CN101974277A - White waterborne wood base coat for medium density fiberboard and preparation technology thereof - Google Patents
White waterborne wood base coat for medium density fiberboard and preparation technology thereof Download PDFInfo
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Abstract
The invention discloses white waterborne wood base coat for a medium density fiberboard and a preparation technology thereof. The preparation technology comprises the processes of: mixing 6.0-8.0 parts of water, 0.2-0.5 part of dispersing agents, 0.2-0.4 part of slurry wetting agents, 0.2-0.4 part of slurry defoaming agents, 18-22 parts of titanium white powder, 5.0-8.0 parts of kaolin, 5.0-8.0 parts of triple superphosphate, 8.0-12.0 parts of talc powder in parts by weight and dispersing to form the slurry, wherein the fineness of the slurry is less than or equal to 50 mu m; mixing 38.0-45.0 parts of resins with the slurry; under the condition of stirring, respectively adding 2.0-4.0 parts of dodecyl acetate, 2.0-4.0 parts of dipropylene glycol methyl ether, 0.3-0.6 part of antifoaming agents, 0.3-0.6 part of wetting agents, 0.3-0.6 part of flatting agents and 0.4-0.8 part of thickening agents, and evenly stirring, discharging and packing. The base coat can control water vapour entering the medium density fiberboard. The paint film has 200-300% of drawing tension, also can not crack, and has good sealing and anti-cracking effects. Besides, the invention has the advantages of quick drying speed and good rubbing property.
Description
[technical field]
The present invention relates to the woodwork coating field, relate in particular to density board edge sealing aqueous wooden ware based white primer and preparation technology thereof.
[technical background]
There is very big defective in existing aqueous wooden ware based white primer on the cross section edge sealing of density board.Mainly be to cause paint film cracking at wet weather.Reason mainly is that density board is a glued board, and under wet weather, steam can enter in the density board, and glue in the density board and xylon bubble are sent out, and it is expanded, thereby cause the paint film cracking on surface.
[summary of the invention]
Purpose of the present invention is exactly in order to solve problems of the prior art, proposes a kind of density board edge sealing aqueous wooden ware based white primer and preparation technology thereof, also the paint film cracking phenomenon can not occur in wet environment.
For achieving the above object, patent of the present invention has proposed a kind of density board edge sealing aqueous wooden ware based white primer, form by slurry, resin and auxiliary agent, described slurry comprises water, dispersion agent, slurry wets agent, slurry defoamer, titanium dioxide, kaolin, coarse whiting and talcum powder, described auxiliary agent comprises lauryl alcohol ester, dipropylene glycol methyl ether, defoamer, wetting agent, flow agent and thickening material, and the mass percent of described each component in based white primer is:
Water: 6.0%～8.0%
Dispersion agent: 0.2%～0.5%
Slurry wets agent: 0.2%～0.4%
Slurry defoamer: 0.2%～0.4%
Titanium dioxide: 18%～22%
Kaolin: 5.0%～8.0%
Coarse whiting: 5.0%～8.0%
Talcum powder: 8.0%～12.0%
Resin: 38.0%～45.0%
Lauryl alcohol ester: 2.0%～4.0%
Dipropylene glycol methyl ether: 2.0%～4.0%
Defoamer: 0.3%～0.6%
Wetting agent: 0.3%～0.6%
Flow agent: 0.3%～0.6%
Thickening material: 0.4%～0.8%.
As preferably, the mass percent of each component in based white primer is:
Water: 7.3%
Dispersion agent: 0.5%
Slurry wets agent: 0.4%
Slurry defoamer: 0.4%
Titanium dioxide: 20.7%
Kaolin: 7.7%
Coarse whiting: 7.7%
Talcum powder: 11%
Resin: 38.0%
Lauryl alcohol ester: 2.3%
Dipropylene glycol methyl ether: 2.3%
Defoamer: 0.4%
Wetting agent: 0.4%
Flow agent: 0.4%
Thickening material: 0.5%.
As preferably, the mass percent of each component in based white primer is:
Water: 7.0%
Dispersion agent: 0.3%
Slurry wets agent: 0.3%
Slurry defoamer: 0.3%
Titanium dioxide: 21.6%
Kaolin: 6.2%
Coarse whiting: 6.2%
Talcum powder: 9.4%
Resin: 41.0%
Lauryl alcohol ester: 3.2%
Dipropylene glycol methyl ether: 3.2%
Defoamer: 0.3%
Wetting agent: 0.3%
Flow agent: 0.3%
Thickening material: 0.4%.
As preferably, the mass percent of each component in based white primer is:
Water: 6.3%
Dispersion agent: 0.2%
Slurry wets agent: 0.2%
Slurry defoamer: 0.2%
Titanium dioxide: 18%
Kaolin: 5.2%
Coarse whiting: 6.7%
Talcum powder: 9.5%
Resin: 45.0%
Lauryl alcohol ester: 3.3%
Dipropylene glycol methyl ether: 3.3%
Defoamer: 0.5%
Wetting agent: 0.5%
Flow agent: 0.5%
Thickening material: 0.6%.
For achieving the above object, patent of the present invention has also proposed a kind of preparation technology of density board edge sealing aqueous wooden ware based white primer, elder generation is 6.0～8.0 parts water by mass, 0.2～0.5 part dispersion agent, 0.2～0.4 part slurry wets agent, 0.2～0.4 part slurry defoamer, 18～22 parts titanium dioxide, 5.0～8.0 parts kaolin, 5.0～8.0 parts coarse whiting, 8.0 be dispersed into the slurry of fineness≤50 μ m after～12.0 parts talcum powder mixes, again 38.0～45.0 parts resin is mixed with above-mentioned slurry, under condition of stirring, the lauryl alcohol ester that adds 2.0～4.0 parts respectively, 2.0～4.0 parts dipropylene glycol methyl ether, 0.3～0.6 part defoamer, 0.3～0.6 part wetting agent, 0.3～0.6 part flow agent, 0.4～0.8 part thickening material can the discharging packing after stirring.
As preferably, the addition of described thickening material is to make the viscosity of lacquer at η
25 ℃=800 centipoises
The beneficial effect of patent of the present invention: after based white primer of the present invention is sprayed at the density board cross section, even under the environment of high humidity, paint film still can effectively be controlled steam and enter in the density board, even there is a spot of steam to enter density board density board is expanded, paint film has 200～300% tensile stress, and paint film can not ftracture yet, the anti-cracking of good sealing effect is arranged, and rate of drying of the present invention is fast, and grinability is good, can effectively improve the utilization ratio of woodworks such as density board.Thoroughly substitute the oil-base paint edge sealing, protection construction workman's is healthy, reduces environmental pollution, better shows the appearance of film effect.
[embodiment]
Embodiment one:
Density board edge sealing aqueous wooden ware based white primer, form by slurry, resin and auxiliary agent, described slurry comprises water, dispersion agent, slurry wets agent, slurry defoamer, titanium dioxide, kaolin, coarse whiting and talcum powder, described auxiliary agent comprises lauryl alcohol ester, dipropylene glycol methyl ether, defoamer, wetting agent, flow agent and thickening material, and the mass percent of described each component in based white primer is: water: 7.3%; Dispersion agent: 0.5%; Slurry wets agent: 0.4%; Slurry defoamer: 0.4%; Titanium dioxide: 20.7%; Kaolin: 7.7%; Coarse whiting: 7.7%; Talcum powder: 11%; Resin: 38.0%; Lauryl alcohol ester: 2.3%; Dipropylene glycol methyl ether: 2.3%; Defoamer: 0.4%; Wetting agent: 0.4%; Flow agent: 0.4%; Thickening material: 0.5%.
Described dispersion agent adopts Shenzhen Hydropatat5040 of Hai Chuan Industry Co.,Ltd main component: poly carboxylic acid sodium; air products company's T G is adopted in the slurry wets agent; the slurry defoamer adopts Degussa Tego Airex902w main component: the polysiloxane polyether copolymer emulsion; titanium dioxide adopts du pont company 902+ main component: TiO2; kaolin adopts the rich kaolin of Shanxi jade pendant 1250 order main component: the SiO2+Al2O3 of company limited; coarse whiting adopts peak, Jiangxi 1250 order main component: the CaCO3 of lime carbonate company limited; talcum powder adopts sea, Yingkou, Liaoning 800 order main component: the AlSiO2 of talcum mining industry company limited, and defoamer adopts Shenzhen Foamstar A of Hai Chuan Industry Co.,Ltd
10Main component: special mineral oil, wetting agent adopts Shenzhen Hydropatat of Hai Chuan Industry Co.,Ltd 140 main components: organic modified polyorganosiloxane, flow agent adopts sea this special Levaslip W-455 of chemical company main component of name: modified polyorganosiloxane, thickening material adopts Hefei Anke Fine Chemicals Co., Ltd., polyurethane associative thickener HUER-A.
The preparation technology of density board edge sealing aqueous wooden ware based white primer, step is as follows:
Making beating: under high shear disperse after earlier water, dispersion agent, slurry wets agent, slurry defoamer, titanium dioxide, kaolin, coarse whiting, talcum powder being mixed, obtain the slurry of fineness≤50 μ m.
Paint: nucleocapsid acrylic resin and above-mentioned slurry that snappiness is suitable are mixed together, under condition of stirring, add lauryl alcohol ester, dipropylene glycol methyl ether, defoamer, wetting agent, flow agent, thickening material respectively, can discharging pack after stirring, the addition of thickening material is to make the viscosity of lacquer at η
25 ℃=800 centipoises.
Resin among the present invention is the nucleocapsid acrylic resin, and is synthetic for making by oneself, and this nucleocapsid acrylic resin is made up of nuclear part, shell part, bottoming liquid, initiator and self-crosslinking sealing monomer.Described nuclear part comprises 20～30 parts butyl methacrylate, 60～66 parts methyl methacrylate, 8～12 parts butyl acrylate in mass; 2～3.5 parts methacrylic acid, but 0.2～0.35 part reactive emulsifier A, but the distilled water of 0.3～0.8 part reactive emulsifier B and 50 parts; Described shell part comprises 25～30 parts butyl methacrylate, 22～25 parts methyl methacrylate, 38～41 parts butyl acrylate in mass; 2～3.5 parts methacrylic acid, 2～4 parts self-cross linking monomer, but 0.2～0.35 part reactive emulsifier A, but the distilled water of 0.3～0.8 part reactive emulsifier B and 50 parts; But bottoming liquid comprises 0.4～0.7 part reactive emulsifier A in mass, but the distilled water of 0.6～1.6 part reactive emulsifier B and 85 parts; Initiator comprises 0.6 part Potassium Persulphate and 10 parts distilled water in mass; Self-crosslinking sealing monomer is 1～2 part in mass.Proportioning between above-mentioned nuclear part, shell part, bottoming liquid, initiator and the self-crosslinking sealing monomer also is in above-mentioned mass fraction, as examine the part be 151.575 parts, then shell partly is 81.325 parts, the bottoming liquid be 86.65 parts, initiator is 10.6 parts, and self-crosslinking sealing monomer is 1.5 parts.
Described self-cross linking monomer adopts diacetone-acryloamide(DAA) (DAAM), and self-crosslinking sealing monomer adopts adipic dihydrazide (ADH).But described reactive emulsifier A adopts DNS-18, is mono succinate stearylamide sulfonate sodium, but reactive emulsifier B adopts DNS-86, is sulfo-succinic acid methyl-isobutyl methyl esters sodium.
The preparation technology of nucleocapsid acrylic resin, step is as follows:
A) pre-emulsification: will examine the pre-emulsification 0.5h of part and obtain examining pre-emulsion, the pre-emulsification 0.5h of shell part obtains the shell pre-emulsion;
B) bottoming liquid adds: the liquid that will feel secure adds the reactor reaction, and is warmed up to 78～82 ℃;
C) the nuclear pre-emulsion adds: all nuclear pre-emulsions are evenly splashed in 2.5h in the reactor, drip initiator simultaneously;
D) first insulation reaction: be incubated 30 minutes down at 80 ℃;
E) the shell pre-emulsion adds: all shell pre-emulsions are evenly splashed in 2h in the reactor, drip initiator simultaneously;
F) second insulation reaction: stopped reaction when insulation 3-4h mensuration transformation efficiency reaches 96-98%;
G) cooling: cool to 50 ℃, transfer Ph=8.5-9.0, stir 0.5h;
H) self-crosslinking sealing monomer adds: self-crosslinking is sealed monomer add after reactor stirs, filter and packing gets final product.
The present invention introduces self-cross linking monomer in the system of conventional acrylic emulsion, this monomer can keep relative stability when routine stores, when film forming, behind the condition changing of system, can realize intermolecular being cross-linked with each other, and form a kind of hard-packed reticulated structure.This reticulated structure is arranged closely, has certain rule, can effectively hinder the motion of water molecules or little branch alcohol, thereby reach purpose water-fast, anti-alcohol.Owing to there is reticulated structure, physicalies such as its antiblocking, tensile strength are improved greatly, so make whole paint film have more excellent performance simultaneously.
Vinylformic acid self-crossing emulsion of the present invention belongs to a kind of hud typed emulsion, its nuclear is made up of the monomer of some high glass transition temperatures, its average T g 〉=60 ℃ (Tg is meant all monomeric average glass transition temperatures), the purpose of doing like this is to make it have extremely strong hardness, improves the resistance to blocking of filming.Its shell is made up of average T g=15 ℃ monomer, wherein contains self-cross linking monomer, can reduce the film-forming temperature MFFT (MFFT is meant the minimum film-forming temperature of paint film) of whole paint film like this, makes it be easy to film forming, and is easy to crosslinked.
The present invention has improved the performance of vinylformic acid paint film, has abandoned traditional emulsifying agent, and adopts the reactable emulsifying agent, and this emulsifying agent can participate in reaction with monomer, has formed the part of paint film.When forming paint film, can as conventional emulsifier, not move the surface of paint film, thereby influence performances such as its water-fast, anti-alcohol, antiblocking.
This prescription has the good characteristics of opacifying power.
Embodiment two:
Density board edge sealing aqueous wooden ware based white primer, form by slurry, resin and auxiliary agent, described slurry comprises water, dispersion agent, slurry wets agent, slurry defoamer, titanium dioxide, kaolin, coarse whiting and talcum powder, described auxiliary agent comprises lauryl alcohol ester, dipropylene glycol methyl ether, defoamer, wetting agent, flow agent and thickening material, and the mass percent of described each component in based white primer is: water: 7.0%; Dispersion agent: 0.3%; Slurry wets agent: 0.3%; Slurry defoamer: 0.3%; Titanium dioxide: 21.6%; Kaolin: 6.2%; Coarse whiting: 6.2%; Talcum powder: 9.4%; Resin: 41.0%; Lauryl alcohol ester: 3.2%; Dipropylene glycol methyl ether: 3.2%; Defoamer: 0.3%; Wetting agent: 0.3%; Flow agent: 0.3%; Thickening material: 0.4%.Preparation process is identical with embodiment one.
This prescription has opacifying power and all good characteristics of anti-cracking behavior.
Embodiment three:
Density board edge sealing aqueous wooden ware based white primer, form by slurry, resin and auxiliary agent, described slurry comprises water, dispersion agent, slurry wets agent, slurry defoamer, titanium dioxide, kaolin, coarse whiting and talcum powder, described auxiliary agent comprises lauryl alcohol ester, dipropylene glycol methyl ether, defoamer, wetting agent, flow agent and thickening material, and the mass percent of described each component in based white primer is: water: 6.3%; Dispersion agent: 0.2%; Slurry wets agent: 0.2%; Slurry defoamer: 0.2%; Titanium dioxide: 18%; Kaolin: 5.2%; Coarse whiting: 6.7%; Talcum powder: 9.5%; Resin: 45.0%; Lauryl alcohol ester: 3.3%; Dipropylene glycol methyl ether: 3.3%; Defoamer: 0.5%; Wetting agent: 0.5%; Flow agent: 0.5%; Thickening material: 0.6%.Preparation process is identical with embodiment one.
This prescription has the characteristics of anti-cracking best results.
The foregoing description is to explanation of the present invention, is not limitation of the invention, any scheme after the simple transformation of the present invention is all belonged to protection scope of the present invention.
Claims (6)
1. density board edge sealing aqueous wooden ware based white primer, it is characterized in that: form by slurry, resin and auxiliary agent, described slurry comprises water, dispersion agent, slurry wets agent, slurry defoamer, titanium dioxide, kaolin, coarse whiting and talcum powder, described auxiliary agent comprises lauryl alcohol ester, dipropylene glycol methyl ether, defoamer, wetting agent, flow agent and thickening material, and the mass percent of described each component in based white primer is:
Water: 6.0%～8.0%
Dispersion agent: 0.2%～0.5%
Slurry wets agent: 0.2%～0.4%
Slurry defoamer: 0.2%～0.4%
Titanium dioxide: 18%～22%
Kaolin: 5.0%～8.0%
Coarse whiting: 5.0%～8.0%
Talcum powder: 8.0%～12.0%
Resin: 38.0%～45.0%
Lauryl alcohol ester: 2.0%～4.0%
Dipropylene glycol methyl ether: 2.0%～4.0%
Defoamer: 0.3%～0.6%
Wetting agent: 0.3%～0.6%
Flow agent: 0.3%～0.6%
Thickening material: 0.4%～0.8%.
2. density board edge sealing aqueous wooden ware based white primer as claimed in claim 1, it is characterized in that: the mass percent of each component in based white primer is:
Water: 7.3%
Dispersion agent: 0.5%
Slurry wets agent: 0.4%
Slurry defoamer: 0.4%
Titanium dioxide: 20.7%
Kaolin: 7.7%
Coarse whiting: 7.7%
Talcum powder: 11%
Resin: 38.0%
Lauryl alcohol ester: 2.3%
Dipropylene glycol methyl ether: 2.3%
Defoamer: 0.4%
Wetting agent: 0.4%
Flow agent: 0.4%
Thickening material: 0.5%.
3. density board edge sealing aqueous wooden ware based white primer as claimed in claim 1, it is characterized in that: the mass percent of each component in based white primer is:
Water: 7.0%
Dispersion agent: 0.3%
Slurry wets agent: 0.3%
Slurry defoamer: 0.3%
Titanium dioxide: 21.6%
Kaolin: 6.2%
Coarse whiting: 6.2%
Talcum powder: 9.4%
Resin: 41.0%
Lauryl alcohol ester: 3.2%
Dipropylene glycol methyl ether: 3.2%
Defoamer: 0.3%
Wetting agent: 0.3%
Flow agent: 0.3%
Thickening material: 0.4%.
4. density board edge sealing aqueous wooden ware based white primer as claimed in claim 1, it is characterized in that: the mass percent of each component in based white primer is:
Water: 6.3%
Dispersion agent: 0.2%
Slurry wets agent: 0.2%
Slurry defoamer: 0.2%
Titanium dioxide: 18%
Kaolin: 5.2%
Coarse whiting: 6.7%
Talcum powder: 9.5%
Resin: 45.0%
Lauryl alcohol ester: 3.3%
Dipropylene glycol methyl ether: 3.3%
Defoamer: 0.5%
Wetting agent: 0.5%
Flow agent: 0.5%
Thickening material: 0.6%.
5. the preparation technology of density board edge sealing aqueous wooden ware based white primer, it is characterized in that: elder generation is 6.0～8.0 parts water by mass, 0.2～0.5 part dispersion agent, 0.2～0.4 part slurry wets agent, 0.2～0.4 part slurry defoamer, 18～22 parts titanium dioxide, 5.0～8.0 parts kaolin, 5.0～8.0 parts coarse whiting, 8.0 be dispersed into the slurry of fineness≤50 μ m after～12.0 parts talcum powder mixes, again 38.0～45.0 parts resin is mixed with above-mentioned slurry, under condition of stirring, the lauryl alcohol ester that adds 2.0～4.0 parts respectively, 2.0～4.0 parts dipropylene glycol methyl ether, 0.3～0.6 part defoamer, 0.3～0.6 part wetting agent, 0.3～0.6 part flow agent, 0.4～0.8 part thickening material can the discharging packing after stirring.
6. the preparation technology of density board edge sealing aqueous wooden ware based white primer as claimed in claim 5 is characterized in that: the addition of described thickening material is to make the viscosity of lacquer at η
25 ℃=80 ± 5ku.
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| CN 201010529886 CN101974277B (en) | 2010-10-29 | 2010-10-29 | White waterborne wood base coat for medium density fiberboard and preparation technology thereof |
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|---|---|---|---|
| CN 201010529886 CN101974277B (en) | 2010-10-29 | 2010-10-29 | White waterborne wood base coat for medium density fiberboard and preparation technology thereof |
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| CN101974277A true CN101974277A (en) | 2011-02-16 |
| CN101974277B CN101974277B (en) | 2013-01-16 |
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| CN102241941B (en) * | 2011-06-27 | 2013-10-09 | 广东巴德士化工有限公司 | Water-soluble polyurethane-based quick-drying base coat with ultrahigh solid content |
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| CN103131284B (en) * | 2013-03-21 | 2015-02-25 | 叶氏化工研发（上海）有限公司 | Water-based wood white primer as well as preparation method and use method thereof |
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| CN105111909A (en) * | 2015-09-14 | 2015-12-02 | 广东朗法博涂装新材料科技有限公司 | Water-based rib-expansion-prevention seal primer for carpentry |
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| CN105505064A (en) * | 2016-01-19 | 2016-04-20 | 卓达新材料科技集团有限公司 | White water-based alkali-resistant sealing primer and preparation method thereof |
| CN106833096A (en) * | 2017-01-18 | 2017-06-13 | 广西贺州市金海乐器有限公司 | A kind of woodenware oil paint additive and its preparation, application method |
| CN107057445A (en) * | 2017-01-18 | 2017-08-18 | 广西贺州市金海乐器有限公司 | Oil paint additive composition and its preparation, application method |
| CN109337474A (en) * | 2018-07-25 | 2019-02-15 | 河北晨阳工贸集团有限公司 | A kind of woodenware sealing wax and preparation method thereof |
| CN112646443A (en) * | 2020-12-24 | 2021-04-13 | 华南理工大学 | Thermal transfer printing roller coating woodware coating composition and preparation method thereof |
| CN112646443B (en) * | 2020-12-24 | 2022-04-22 | 华南理工大学 | Thermal transfer printing roller coating woodware coating composition and preparation method thereof |
| CN114085576A (en) * | 2021-12-22 | 2022-02-25 | 东莞市涂芭新材料有限公司 | Water-based yellow-sealing coating and preparation method thereof |
| CN114958125A (en) * | 2022-06-07 | 2022-08-30 | 上海展辰涂料有限公司 | Water-based high-filling hot-air-drying white primer for MDF (medium density fiberboard) board |
| CN115477880A (en) * | 2022-08-02 | 2022-12-16 | 广州冠志新材料科技有限公司 | Water-based high-solid-content quick-drying edge sealing paint and preparation method thereof |
| CN115477880B (en) * | 2022-08-02 | 2023-08-29 | 广州冠志新材料科技有限公司 | Water-based high-solid-content quick-drying edge sealing paint and preparation method thereof |
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