CN101836947B - Chinese medicinal freckle-removing facial mask and preparation method thereof - Google Patents
Chinese medicinal freckle-removing facial mask and preparation method thereof Download PDFInfo
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Abstract
The invention provides a Chinese medicinal freckle-removing facial mask. The active ingredient of the facial mask is water extract prepared from 30 to 80 percent of tribulus terrestris, 5 to 25 percent of safflower and 10 to 50 percent of Chinese angelica, wherein the tribulus terrestris can dispel wind and soothe liver, has the effects of washing black skin, removing freckle and washing scar, and is used as a monarch medicament; the Chinese angelica has the effects of moisturizing skin, nourishing the blood and promoting blood circulation and enriching the blood and promoting tissue regeneration; and the safflower has the effects of activating blood circulation, removing blood stasis and improving micro circulation, and is used as a ministerial medicament. The facial mask has the effects of soothing the liver and invigorating blood circulation, dissolving blood stasis and removing freckle and improving skin metabolic capability when the Chinese medicaments are used together. The facial mask can also contain skin nutrients, such as wheat-germ oil, hyaluronic acid, collagen and the like, so the beautifying effect of the facial mask can be further improved.
Description
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of facial film of Chinese medicine compound extract preparation.
Background technology
The generation of most human face's speckle is many slows down with the metabolic function of health, ultraviolet, hormonal imbalance are relevant, and melanin can't normally be mediated, in the old long-pending formation of horny layer.Common speckle is following:
One, freckle: in general to appear at skin on the face whiter for great majority, and summer, over-drastic Exposure to Sunlight meeting increased the weight of to increase, but to winter freckle subtract light.How relevant with heredity.
Two, chloasma: claim butterfly spot again, mainly relevant with the endocrine disturbance.Estrogen can stimulate melanocyte secretion melanin granule, and progestogen can promote the transhipment and the diffusion of melanosome.Discover; In women's patient with chloasma; Serum estradiol (E2), FSH (FSH), lutropin (LH) level are significantly higher than the normal person; Androgen (T) level is low, progestogen (P) and the horizontal no abnormality seen of prolactin antagonist (PRL), and the morbidity of prompting women patient with chloasma changes relevant with sex hormone level.
Three, cyasma: conceived back androgen increases, so the common symmetric chloasma of pregnancy period women denomination portion is recovered normal condition but produce the intravital androgen secretion in back, most people's speckle can alleviate or disappear.
Four: black speck: common people are the caused melanin depositions of sunlight, can drain with the body metabolism, but some human metabolism are slower or older; Can not in time drain; Be mainly in middle-aged women, cause the foreign body embedding people wound that uses cosmetics inferior or wound to cause in addition by the black pathological changes of skin; Perhaps excessive use melanin medicine also can cause black speck.
Five, mottle: reticulate, tend to occur large stretch ofly, skin resistance reduces, and causes atrophy of epidermis.
The product of speckle dispelling mainly contains oral formulations at present, smears unguentum etc.Fructus Atriplicis Sibiricae is traditional beauty treatment Chinese medicine, and Compendium of Material Medica is with regard to " it is black to wash one's face, and speckle dispelling is washed the scar skin ulcer " on the books.Traditional usage of Fructus Atriplicis Sibiricae is to share with Radix Angelicae Sinensis, Fructus Crataegi, Cortex Dictamni to process the oral speckle dispelling that is used for of liniment.Along with the effect that traditional Chinese medicine beauty treatment is improved looks is in modern times admitted by increasing people, the Chinese medicine facial film arises at the historic moment as the ideal skin care item of a kind of skin nursing, and Fructus Atriplicis Sibiricae also begins to be used for by people the making of facial film; The Fructus Atriplicis Sibiricae facial mask powder of processing with Fructus Atriplicis Sibiricae is separately arranged, the compound recipe facial film that is made into other Chinese medicines is also arranged, like the Radix Angelicae Dahuricae of folklore; The Rhizoma Atractylodis Macrocephalae, Fructus Atriplicis Sibiricae, the Pseudobulbus Bletillae (Rhizoma Bletillae); Bombyx Batryticatus is worn into powder and mixes well the facial film of processing with starch and Mel with white Radix Ginseng Rubra, and the effect of whitening and speckle dispelling is arranged.Present existing Chinese medicine facial film is many to be main with facial mask powder.So-called facial mask powder is the powder-product that Chinese crude drug is directly worn into mostly, and water is mixed well and spread upon on the face during use.Though these Chinese medicinal mask powder have certain curative effect, also there are some problems, on the one hand; The dissolution of the Chinese medicinal mask powder effective ingredient that water is mixed well is limited; On the one hand, commercially available Chinese medicinal mask powder exists potential safety hazard, the Radix Angelicae Dahuricae in addition; Rhizoma Typhonii is the banned substance of cosmetics rules regulation, and the use of these materials causes the allergy and the pigmentation of skin easily.In addition; It is not too convenient that this facial film uses, and moistening effect and absorption of nutrient ingredients effect are relatively poor, therefore is necessary to seek safer Chinese medicine; Extract its effective ingredient and improve its utilization rate, and a kind of mask carriers of suitable Chinese medicine promote in the absorption of pharmaceutically active ingredient.
Summary of the invention
The technical problem that the present invention will solve provides a kind of Chinese medicine facial film with freckle effect.
The technical scheme that the present invention addresses the above problem is:
A kind of Chinese medicine facial film that is used for speckle dispelling, this facial film is made up of effective components of Chinese medicinal and facial film field acceptable auxiliary, it is characterized in that said effective ingredient comprises that concentration is the Chinese medicine extraction liquid of 0.2～2g medical material/mL; Described Chinese medicine extraction liquid is obtained by the Chinese medicine water decocting method extraction of following weight proportion: Fructus Atriplicis Sibiricae 30%～80%, Flos Carthami 5%～25%, Radix Angelicae Sinensis 10%～50%; Every facial film is loaded with described Chinese medicine extraction liquid 80mL.
In the facial film of the present invention, described Chinese medicine extraction liquid is obtained by the Chinese medicine water decocting method extraction of following weight proportion: Fructus Atriplicis Sibiricae 50%～60%, Flos Carthami 10%～20%, Radix Angelicae Sinensis 25%～35%.
In the facial film of the present invention; Described effective ingredient also can comprise and occupies the skin-nourishing thing of imitating composition 0.5～2.8% (W/W) cosmetic result with further raising facial film of the present invention; Described skin-nourishing thing is selected from Semen Tritici aestivi germ oil, a kind of or two or more in hyaluronic acid and the collagen protein.
Facial film according to the invention is prepared by following method:
(1) adds 6～10 times for the first time and decocted 1.5～3 hours, add 6～10 times for the second time and decocted 1.5～3 hours; Merge decocting liquid twice, filter, be concentrated into 0.2～2g medical material/mL, cold preservation was left standstill 10～24 hours, filtered, and adding water adjustment filter liquor concentration is 0.2～2g medical material/mL, gets Chinese medicine extraction liquid;
(2) carry the ratio of the said Chinese medicine extraction liquid of 80mL in every facial film, get that Chinese medicine is got the gained Chinese medicine extraction liquid and the facial film adjuvant is processed facial film by conventional method;
In the above-mentioned steps, described facial film adjuvant comprises dispersant and carrier, wherein,
Described dispersant is selected from propylene glycol, glycerin or ethanol, preferred propylene glycol or glycerin;
Said carrier is gel-type vehicle or non-woven fabrics, and wherein, described gel-type vehicle is one or both in soybean fiber, arabic gum, carrageenan, Konjac glucomannan and the gelatin.
In the method for preparing of facial film of the present invention, described adjuvant also can comprise one or both in the following adjuvant:
1. antiseptic:, can be selected from chlorobutanol, benzyl alcohol, phenethanol, methyl hydroxybenzoate, ethyl hydroxybenzoate and the propylparaben one or both, preferably ethyl hydroxybenzoate or propylparaben to prolong the shelf-life of facial film of the present invention.
2. solubilizing agent: optional to increase the dissolving of skin-nourishing thing from tween 80, SP-115A (Xin Pu company) or 1264 emulsifying agents (Xin Pu company).
When facial film of the present invention selects for use gel-type vehicle to be carrier, promptly be the quartzy facial film that is commonly called as, concrete method for making is following:
(1) scattered dispersant and gel-type vehicle mixture added in the said Chinese medicine extraction liquid by proportioning, be heated to 80～90 ℃ and fully stirred 15 minutes, transfer to pH5.5～6.5 with the pH regulator agent;
(2) film forming (promptly processing facial film), packing, sterilization;
Wherein said pH regulator agent is hydrochloric acid, citric acid and phosphate buffer solution.
If the effective ingredient in the said quartzy facial film also comprises the skin-nourishing thing, then step (2) should be: add the skin-nourishing thing after being cooled to 50 ℃, mixing, film forming, packing, sterilization.
If said quartzy facial film also contains adjuvants such as antiseptic or solubilizing agent, then when the preparation facial film, said adjuvant and gel-type vehicle are disperseed with dispersant, join in the Chinese medicine extraction liquid again.
When facial film of the present invention selects for use non-woven fabrics to be carrier, promptly be the non-woven fabrics facial film that is commonly called as, concrete method for making is following: dispersant is joined in step (1) the gained Chinese medicine extraction liquid, fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing, radiation sterilization.
If the effective ingredient in the said non-woven fabrics facial film also comprises the skin-nourishing thing, then the skin-nourishing thing prepares in the process at facial film and joins Chinese medicine extraction liquid with dispersant, and stirring gets final product.
If said non-woven fabrics facial film also contains adjuvants such as antiseptic or solubilizing agent, then when the preparation facial film, said adjuvant is disperseed with dispersant, join in the Chinese medicine extraction liquid again.
Facial film according to the invention as active component, can play freckle effect with the effective ingredient of Fructus Atriplicis Sibiricae, Radix Angelicae Sinensis and Flos Carthami.
Therefrom medical angle is seen, Fructus Atriplicis Sibiricae can dispel the wind soothing the liver, has the effect of " it is black to wash one's face, and speckle dispelling is washed the scar skin ulcer ", is monarch drug.Radix Angelicae Sinensis, the matter skin of moistening, nourshing blood and promoting blood circulation, tonic blood and growing muscle; Flos Carthami, blood circulation promoting and blood stasis dispelling is ministerial drug altogether.Blood stored in the liver, depression of liver-QI can cause blood stasis, thereby causes speckle to produce, and Fructus Atriplicis Sibiricae can dispel the wind soothing the liver; It is freely suitable to make liver hide mechanism of qi, the nourshing blood and promoting blood circulation of Radix Angelicae Sinensis ability, and Flos Carthami ability blood circulation promoting and blood stasis dispelling distends the blood vessels; Microcirculation improvement makes the timely skin nutrition of nutrient mass-energy in the blood, strengthens the anoxia enduring and the anti-damage ability of skin; Make waste matter be easy to discharge, thereby assist Fructus Atriplicis Sibiricae to make that blood fortune is unobstructed, speckle is not given birth to.Three medicines share, altogether the long memorial liver invigorate blood circulation, the effect of stasis-resolving spot-removing, skin moistening granulation promoting.
In order to understand the present invention better, will further specify the technique effect that the present invention has through clinical experiment report below.
1, patient data: select female patient 90 examples of speckle, each 45 example of men and women, 30～45 years old age.Be divided into three groups at random: treatment group (Chinese medicine extraction liquid adds the skin nutrient) 30 examples, each 15 example of men and women, 36 ± 7 years old age; Matched group is (carrageenan adds water) 30 examples 1., each 15 example of men and women, 38 ± 7 years old age; Matched group is (Chinese medicine extraction liquid 2.; Do not add the skin nutrient) 30 examples, each 15 example of men and women, 38 ± 6 years old age.
Treatment first three groups patient's sex, age, state of an illness weight situation (symptom integral) there are no significant difference (P＞0.05) has comparability.
2, experiment material:
(1) treatment group of the present invention:
The treatment group: contain the skin-nourishing thing in the effective ingredient of used facial film, press embodiment 1 preparation, every weight is 80 grams, specification 10*15cm.
(2) the matched group facial film prepares by following method:
Matched group is 1.:
Prescription: carrageenan 11g, ethyl hydroxybenzoate 2g processes 1000g
Method for making: water adds carrageenan after being heated to 80-90 ℃, and ethyl hydroxybenzoate fully stirred 15 minutes, regulates pH value to 5.5-6.5, film forming, packing, sterilization.Press embodiment 1 preparation, every weight is 80 grams, specification 10*15cm.
Matched group is 2.: do not contain the skin-nourishing thing in the effective ingredient of used facial film, used facial film is pressed embodiment 16 preparations, and every weight is 80 grams, specification 10*15cm.
3, experimental technique:
The treatment group: the patient lies on the back, and after washing one's face, spreads on face with facial film of the present invention, flush away behind about 15min.3 times weekly, be 2 weeks the course of treatment.
Matched group: the patient lies on the back, and after washing one's face, spreads on face, flush away behind about 15min with matched group facial film (not drug ingredients) and embodiment 16 facial films 1..3 times weekly, be 2 weeks the course of treatment.
4, clinical symptoms standards of grading: no speckle is designated as 0; Be main with buccal only, area is no more than more than 30% below 50% of entire face, and paler colour, is filbert, is dispersed in distribution and does not merge in flakes, is designated as 2 fens; Have the brown spot area to surpass more than 50% below 70% of entire face with two cheeks, forehead, but the color of speckle shoal, and is designated as 4 fens; With positions such as forehead, buccal, nose both sides, lip weeks the lighter speckle that is dispersed in is arranged, the 70% above person that area accounts for entire face is designated as 5 fens; With two cheeks, forehead brown spot is arranged, area surpasses 50% or more below 70% of entire face, and the color of speckle is darker, is dark brown, and fusion is designated as 8 fens in flakes; With positions such as forehead, buccal, nose both sides, lip weeks the deep brown spot that is dispersed in is arranged, the 70% above person that area accounts for entire face is designated as 10 fens.
5, efficacy assessment standard:
By formula earlier---score value * 100% calculates the improvement rate before clinical symptoms integration score value improvement rate=(symptom integral score value before the treatment-treatment back symptom integral score value)/treatment, adopts criterion evaluation curative effect then.
Produce effects: symptom integral score value improvement rate >=70%;
Effectively: symptom integral score value improvement rate >=50%;
Invalid: symptom does not see that obvious improvement or counter sees deterioration, symptom integral score value improvement rate＜50%.
6, statistical procedures: total data adopts SPSS 13.0 statistics softwares to carry out statistical analysis, and measurement data adopts the t check, and enumeration data adopts x
2Check.
7, result of the test
Table 1 is relatively seen in the clinical symptoms scoring before and after treatment group and the treatment of control group, and curative effect is relatively seen table 2 before and after treatment group and the treatment of control group, can know from table 2; Facial film speckle dispelling total effective rate of the present invention is up to 83%, and observes through the treatment group and not have the heating of the skin of discovery, flushing; Edema, untoward reaction such as pruritus.
Clinical symptoms scoring before and after table 1 treatment group and the treatment of control group
| Group | n | Before the treatment | After the treatment | Difference |
| The treatment group | 30 | 7.00±2.08 | 3.43±1.59 | 3.57±1.79 |
| Matched group 1. | 30 | 6.73±2.20 | 6.27±2.21 | 0.47±1.25 |
| Matched group 2. | 30 | 6.80±2.07 | 3.50±1.57 | 3.30±1.66 |
Table 2 treatment group and matched group curative effect are relatively
| Group | Case load | Produce effects | Effectively | Invalid | Total effective rate/% |
| The treatment group | 30 | 6 | 19 | 5 | 83.3 |
| Matched group 1. | 30 | 0 | 2 | 28 | 6.7 |
| Matched group 2. | 30 | 5 | 18 | 7 | 76.7 |
1. treatment group and matched group compare, and the evident in efficacy of medicine explained in P＜0.01.
2. treatment group and matched group compare P＞0.05; What main therapeutical effect had been described is Chinese medicine extraction liquid; But the difference of integration can be found out from the treatment front and back; Chinese medicine extraction liquid adds skin-nourishing thing group (i.e. treatment group) and does not add skin nutrient group (be matched group 2.) and relatively, can play effect of dispelling spots preferably.
The specific embodiment
Among the following embodiment 1～16, the recipe quantity of each embodiment is the recipe quantity of 12.5 facial films.
Embodiment 1
Prescription:
Fructus Atriplicis Sibiricae 258g, Flos Carthami 71g, Radix Angelicae Sinensis 141g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.5g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.5: 1 medicinal liquid of written treaty; Filter, 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).Because hyaluronic acid than indissoluble, is difficult to homodisperse with medicinal liquid is directly mixed mutually, obtains the hyalomitome acid solution so earlier hyaluronic acid is dissolved in the water, and then mixes with medicinal liquid.
Embodiment 2
Prescription:
Fructus Atriplicis Sibiricae 480g, Flos Carthami 60g, Radix Angelicae Sinensis 60g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.63g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.63: 1 medicinal liquid of written treaty; Filter, 0.63: 1 medicinal liquid (0.63g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 3
Prescription:
Fructus Atriplicis Sibiricae 520g, Flos Carthami 200g, Radix Angelicae Sinensis 80g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.85g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.85: 1 medicinal liquid of written treaty; Filter, 0.85: 1 medicinal liquid (0.85g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 4
Prescription:
Fructus Atriplicis Sibiricae 423g, Flos Carthami 71g, Radix Angelicae Sinensis 916g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 8 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 1.5g medical material/ml), cold preservation was left standstill 24 hours to concentrate 1.5: 1 medicinal liquids of written treaty; Filter, 1.5: 1 medicinal liquid (1.5g medical materials/ml), get Chinese medicine extraction liquid are filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 5
Prescription:
Fructus Atriplicis Sibiricae 1000g, Flos Carthami 200g, Radix Angelicae Sinensis 680g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 10 times of water gagings for the first time; For the second time add 10 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 2g medical material/ml), cold preservation was left standstill 24 hours to concentrate 2: 1 medicinal liquids of written treaty; Filter, 2: 1 medicinal liquid (2g medical materials/ml), get Chinese medicine extraction liquid are filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 6
Prescription:
Fructus Atriplicis Sibiricae 120g, Flos Carthami 15g, Radix Angelicae Sinensis 65g;
Soybean fiber 13g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 1g propylparaben 1g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.2g medical material/ml), cold preservation was left standstill 24 hours to be condensed into 0.2: 1 medicinal liquid; Filter, 0.2: 1 medicinal liquid (0.2g medical material/ml), get Chinese medicine extraction liquid is filtrated in the moisturizing adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, to get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, propylparaben is heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 7
Prescription:
Fructus Atriplicis Sibiricae 235g, Flos Carthami 94g, Radix Angelicae Sinensis 141g;
Carrageenan 13g, ethanol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 1g, propylparaben 1g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.5g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.5: 1 medicinal liquid of written treaty; Filter, 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get scattered ethanol, carrageenan, ethyl hydroxybenzoate and the propylparaben of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5; Be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully; Film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 8
Prescription:
Fructus Atriplicis Sibiricae 282g, Flos Carthami 71g, Radix Angelicae Sinensis 117g;
Carrageenan 13g, ethanol 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 1g, benzyl alcohol 5g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.5g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.5: 1 medicinal liquid of written treaty; Filter, 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get scattered ethanol, carrageenan, ethyl hydroxybenzoate and the benzyl alcohol of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5; Be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully; Film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 9
Prescription:
Fructus Atriplicis Sibiricae 250g, Flos Carthami 50g, Radix Angelicae Sinensis 170g;
Carrageenan 13g, glycerin 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.5g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.5: 1 medicinal liquid of written treaty; Filter, 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get scattered glycerin, carrageenan and the ethyl hydroxybenzoate of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5; Be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully; Film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 10
Prescription:
Fructus Atriplicis Sibiricae 250g, Flos Carthami 50g, Radix Angelicae Sinensis 170g;
Carrageenan 10g, arabic gum 3g, propylene glycol 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.5g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.5: 1 medicinal liquid of written treaty; Filter, 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan, arabic gum; Ethyl hydroxybenzoate is heated to 80-90 ℃ and fully stirred 15 minutes, regulates pH value to 5.5-6.5, is cooled to about 50 ℃ and adds 0.5% hyalomitome acid solution and collagen protein; Mixing makes dissolving fully, film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 11
Prescription:
Fructus Atriplicis Sibiricae 250g, Flos Carthami 50g, Radix Angelicae Sinensis 170g;
Carrageenan 11g, Magnesium L-Asacorbic Acid 2-O-Phosphate 50g, propylene glycol 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.5g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.5: 1 medicinal liquid of written treaty; Filter, 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan; Ethyl hydroxybenzoate is heated to 80-90 ℃ and fully stirred 15 minutes, regulates pH value to 5.5-6.5, is cooled to about 50 ℃ and adds 0.5% hyalomitome acid solution, collagen protein and Magnesium L-Asacorbic Acid 2-O-Phosphate; Mixing makes dissolving fully, film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 12
Prescription:
Fructus Atriplicis Sibiricae 714g, Flos Carthami 143g, Radix Angelicae Sinensis 486g;
Hyaluronic acid 0.36g, collagen protein 18g, propylene glycol 180g.
Method for making: Radix Codonopsis, the Radix Astragali, Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 1.74g medical material/ml), cold preservation was left standstill 24 hours to concentrate 1.74: 1 medicinal liquids of written treaty; Filter, 1.74: 1 medicinal liquid (1.74g medical materials/ml), get Chinese medicine extraction liquid are filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with 1% scattered hyalomitome acid solution and collagen protein of propylene glycol, fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing, and sterilization promptly gets.
In the above-mentioned steps, described 1% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 1% (w/w).
Embodiment 13
Prescription:
Fructus Atriplicis Sibiricae 650g, Flos Carthami 100g, Radix Angelicae Sinensis 350g;
Hyaluronic acid 0.1g, collagen protein 5g, Semen Tritici aestivi germ oil 20g, propylene glycol 50g, 1264 emulsifying agents (Xin Pu company) 4g.
Method for making: Radix Codonopsis, the Radix Astragali, Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 1.22g medical material/ml), cold preservation was left standstill 24 hours to concentrate 1.22: 1 medicinal liquids of written treaty; Filter, 1.22: 1 medicinal liquid (1.22g medical materials/ml), get Chinese medicine extraction liquid are filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with 1264 scattered emulsifying agents of propylene glycol, Semen Tritici aestivi germ oil, hyalomitome acid solution and collagen protein, fully mix; Stir; The non-woven fabrics that high-temperature sterilization is good absorbs, packing, and radiation sterilization promptly gets.
Embodiment 14
Prescription:
Fructus Atriplicis Sibiricae 650g, Flos Carthami 100g, Radix Angelicae Sinensis 350g;
Hyaluronic acid 0.1g, collagen protein 5g, Semen Tritici aestivi germ oil 20g, propylene glycol 50g, SP-115A (Xin Pu company) 4g.
Method for making: Radix Codonopsis, the Radix Astragali, Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 1.22g medical material/ml), cold preservation was left standstill 24 hours to concentrate 1.22: 1 medicinal liquids of written treaty; Filter, 1.22: 1 medicinal liquid (1.22g medical materials/ml), get Chinese medicine extraction liquid are filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with the scattered SP-115A Semen Tritici aestivi germ oil of propylene glycol, 0.5% hyalomitome acid solution and collagen protein, fully mix; Stir; The non-woven fabrics that high-temperature sterilization is good absorbs, packing, and radiation sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 15
Prescription:
Fructus Atriplicis Sibiricae 500g, Flos Carthami 100g, Radix Angelicae Sinensis 200g;
Hyaluronic acid 0.1g, collagen protein 5g, Semen Tritici aestivi germ oil 20g, propylene glycol 50g, tween 80 10g.
Method for making: get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.89g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.89: 1 medicinal liquid of written treaty; Filter, 0.89: 1 medicinal liquid (0.89g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with the scattered tween 80 of propylene glycol, Semen Tritici aestivi germ oil, 0.5% hyalomitome acid solution and collagen protein, fully mix; Stir; The non-woven fabrics that high-temperature sterilization is good absorbs, packing, and radiation sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 16
Prescription:
Fructus Atriplicis Sibiricae 250g, Flos Carthami 50g, Radix Angelicae Sinensis 170g;
Carrageenan 11g, propylene glycol 50g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Flos Carthami and Radix Angelicae Sinensis, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.5g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.5: 1 medicinal liquid of written treaty; Filter, 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes, regulate pH value to 5.5-6.5; Mixing makes dissolving fully, film forming; Packing, sterilization promptly gets.
Claims (9)
1. Chinese medicine facial film that is used for speckle dispelling, this facial film is made up of effective components of Chinese medicinal and facial film field acceptable auxiliary, it is characterized in that said effective ingredient comprises that concentration is the Chinese medicine extraction liquid of 0.2～2g medical material/mL; Described Chinese medicine extraction liquid is obtained by the Chinese medicine water decocting method extraction of following weight proportion: Fructus Atriplicis Sibiricae 30%～80%, Flos Carthami 5%～25%, Radix Angelicae Sinensis 10%～50%; Every facial film is loaded with described Chinese medicine extraction liquid 80mL.
2. facial film according to claim 1 is characterized in that described Chinese medicine extraction liquid is extracted by the Chinese medicine water decocting method of following weight proportion to obtain: Fructus Atriplicis Sibiricae 50%～60%, Flos Carthami 10%～20%, Radix Angelicae Sinensis 25%～35%.
3. facial film according to claim 1, it is characterized in that said effective ingredient also comprises occupies the skin-nourishing thing of imitating composition 0.5～2.8% (W/W), and described skin-nourishing thing is selected from Semen Tritici aestivi germ oil, a kind of in hyaluronic acid and the collagen protein or two kinds.
4. the method for preparing of claim 1 or 2 said facial films, this method is made up of following steps:
(1) adds 6～10 times for the first time and decocted 1.5～3 hours, add 6～10 times for the second time and decocted 1.5～3 hours; Merge decocting liquid twice, filter, be concentrated into 0.2～2g medical material/mL, cold preservation was left standstill 10～24 hours, filtered, and adding water adjustment filter liquor concentration is 0.2～2g medical material/mL, gets Chinese medicine extraction liquid;
(2) carry the ratio of the said Chinese medicine extraction liquid of 80mL in every facial film, get Chinese medicine extraction liquid and the facial film adjuvant is processed facial film by conventional method;
In the above-mentioned steps, described facial film adjuvant comprises dispersant and carrier, wherein,
Described dispersant is selected from propylene glycol, glycerin or ethanol;
Said carrier is gel-type vehicle or non-woven fabrics, and wherein, described gel-type vehicle is one or both in soybean fiber, arabic gum, carrageenan, Konjac glucomannan and the gelatin.
5. like the said method of claim 4, it is characterized in that described dispersant is propylene glycol or glycerin.
6. like the said method of claim 4, it is characterized in that said facial film adjuvant also comprises antiseptic, said antiseptic is one or both in chlorobutanol, benzyl alcohol, phenethanol, methyl hydroxybenzoate, ethyl hydroxybenzoate and the propylparaben.
7. like the said method of claim 6, it is characterized in that described antiseptic is ethyl hydroxybenzoate or propylparaben.
8. like the said method of claim 4, it is characterized in that said facial film adjuvant also comprises solubilizing agent, described solubilizing agent is a tween 80.
9. like the said method of claim 6, it is characterized in that said facial film adjuvant also comprises solubilizing agent, described solubilizing agent is a tween 80.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2010101796602A CN101836947B (en) | 2010-05-17 | 2010-05-17 | Chinese medicinal freckle-removing facial mask and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2010101796602A CN101836947B (en) | 2010-05-17 | 2010-05-17 | Chinese medicinal freckle-removing facial mask and preparation method thereof |
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| Publication Number | Publication Date |
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| CN101836947A CN101836947A (en) | 2010-09-22 |
| CN101836947B true CN101836947B (en) | 2012-01-25 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102144960B (en) * | 2011-03-30 | 2012-09-26 | 解筱羚 | Anti-aging facial mask |
| CN110227047B (en) * | 2019-06-26 | 2022-05-13 | 广州三广生物科技有限公司 | Skin care composition with effect of removing red blood streak and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1099867C (en) * | 1997-08-18 | 2003-01-29 | 陈利华 | Face-care prepn. contg. natural ingredients |
| JP2001240555A (en) * | 2000-03-01 | 2001-09-04 | Kenji Nakamura | External agent for beautifying |
| CN101536972B (en) * | 2009-04-08 | 2012-02-08 | 刘伟琳 | Traditional Chinese medicine mask powder |
| CN101606899A (en) * | 2009-07-28 | 2009-12-23 | 李芸 | A kind of Chinese medicine freckle whitening makeup |
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Address after: 510660 Tianhe District, Guangzhou, Huang Village Road, No. 55, building No. 3, No. Patentee after: GAOKANG DAILY CHEMICAL GROUP Co.,Ltd. Address before: 510660 Tianhe District, Guangzhou, Huang Village Road, No. 55, building No. 3, No. Patentee before: Gao Kang Cosmetics Manufacturing Co.,Ltd. |
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Effective date of registration: 20220624 Address after: 510000 a8016, block a, Tianrui Plaza, 397 Jianpeng Road, Jiahe street, Baiyun District, Guangzhou City, Guangdong Province Patentee after: Guangzhou Wanqian vermicelli Cosmetics Co.,Ltd. Address before: 510660 3rd floor, 55 Huangcun Road, Tianhe District, Guangzhou City, Guangdong Province Patentee before: GAOKANG DAILY CHEMICAL GROUP CO.,LTD. |