CN101836946B - Whitening Chinese medicament mask and method for preparing same - Google Patents
Whitening Chinese medicament mask and method for preparing same Download PDFInfo
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Abstract
The invention provides a whitening crystal mask. The mask comprises the active ingredients of aqueous extract prepared by the following raw materials in percentage by weight: 15 to 60 percent of Tribulus terrestris, 10 to 45 percent of red ginseng and 15 to 60 percent of dwarf lilyturf root, wherein the dwarf lilyturf root can nourish yin and moisten the lung and benefit the stomach and increase the body fluid, and according to 'Compendium of Materia Medica', the dwarf lilyturf root has the effect of 'beautifying the skin' and is the monarch, medicament; the Tribulus terrestris can expel wind evil and sooth the liver, and according to 'Compendium of Materia Medica', the Tribulus terrestris has the effects of whitening the facial skin, dispelling freckles and washing away scars and sores, and qi and blood are basic substances of the human body, if qi and blood are sufficient, the complexion is rosy, and if the qi and blood are deficient, the complexion is sallow, the red ginseng can tonify qi and enrich the blood, and the red ginseng and the Tribulus terrestris are both ministerial medicaments; three Chinese medicaments are combined so as to achieve the better whitening effect; and the mask may also contain other whitening materials such as arbutin, vitamin C phosphate magnesium and the like, and skin nutriments such as wheat germ oil, hyaluronic acid and collagen and the like, and the whitening effect of the mask can be further improved.
Description
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of facial film of Chinese medicine compound extract preparation.
Background technology
Facial film is a kind of cosmetics and skincare product that applies on the face, can play the effect of cleaning, fitness and protection face.Along with traditional Chinese medicine beauty treatment is admitted by increasing people in the effect of modern beauty, the Chinese medicine facial film arises at the historic moment as the ideal skin care item of a kind of skin nursing, and has obtained liking of people with its hyposensitivity and low side effect.Present known Chinese medicine facial film is many, especially whitens, the product of speckle dispelling and anti-acne aspect.Fructus Atriplicis Sibiricae is traditional beauty treatment Chinese medicine, and Compendium of Material Medica is with regard to " it is black to wash one's face, and speckle dispelling is washed the scar skin ulcer " on the books.The beauty mask that utilizes this effect of Fructus Atriplicis Sibiricae and develop is many, the Fructus Atriplicis Sibiricae facial mask powder made from Fructus Atriplicis Sibiricae is separately arranged, the compound recipe facial film that is made into other Chinese medicines is also arranged, as the Radix Angelicae Dahuricae of folklore, the Rhizoma Atractylodis Macrocephalae, Fructus Atriplicis Sibiricae, the Radix Paeoniae Alba, the Pseudobulbus Bletillae (Rhizoma Bletillae), Bombyx Batryticatus and white Radix Ginseng Rubra are worn into powder and are mixed well the facial film made from starch and Mel, and the effect of whitening and speckle dispelling is arranged.Present existing Chinese medicine facial film is many based on facial mask powder.So-called facial mask powder is the powder-product that Chinese crude drug is directly worn into mostly, and water is mixed well and spread upon on the face during use.Though these Chinese medicinal mask powder have certain curative effect, but also there are some problems, on the one hand, the dissolution of the Chinese medicinal mask powder effective ingredient that water is mixed well is limited, on the one hand, commercially available Chinese medicinal mask powder exists potential safety hazard, the Radix Angelicae Dahuricae in addition, Rhizoma Typhonii is the banned substance of cosmetics rules regulation, and the use of these materials causes the allergy and the pigmentation of skin easily.In addition, it is not too convenient that this facial film uses, and moistening effect and absorption of nutrient ingredients effect are relatively poor, therefore is necessary to seek safer Chinese medicine, extract its effective ingredient and improve its utilization rate, and a kind of mask carriers of suitable Chinese medicine promote in the absorption of pharmaceutically active ingredient.
Summary of the invention
The technical problem to be solved in the present invention provides a kind of Chinese medicine facial film that skin care is whitened that has.
The technical scheme that the present invention addresses the above problem is:
A kind of Chinese medicine facial film of whitening, this facial film is made up of effective components of Chinese medicinal and facial film field acceptable auxiliary, it is characterized in that described effective ingredient comprises that concentration is the Chinese medicine extraction liquid of 0.2～2g medical material/mL; Described Chinese medicine extraction liquid is obtained by the Chinese medicine water decocting method extraction of following weight proportion: Fructus Atriplicis Sibiricae 15%～60%, Radix Ginseng Rubra 10%～45%, Radix Ophiopogonis 15%～60%; Every facial film is loaded with described Chinese medicine extraction liquid 80mL.
In the facial film of the present invention, described Chinese medicine extraction liquid is obtained by the Chinese medicine water decocting method extraction of following weight proportion: Fructus Atriplicis Sibiricae 35%～40%, Radix Ginseng Rubra 25%～30%, Radix Ophiopogonis 30%～40%.
In the facial film of the present invention, described effective ingredient also can comprise and occupies the skin-nourishing thing of imitating composition 0.05～6% (W/W) cosmetic result with further raising facial film of the present invention, described skin-nourishing thing is selected from Semen Tritici aestivi germ oil, a kind of or two or more in hyaluronic acid and the collagen protein.
Facial film of the present invention can comprise that also other whitening medicaments of 1～6% (W/W) are to strengthen whitening effect, as arbutin or Magnesium L-Asacorbic Acid 2-O-Phosphate.
The preparation method of facial film of the present invention is made up of following steps:
(1) gets Radix Ophiopogonis, Fructus Atriplicis Sibiricae and Radix Ginseng Rubra, decoct with water twice, add 6～10 times for the first time and decocted 1.5～3 hours, add 6～10 times for the second time and decocted 1.5～3 hours; Merge decocting liquid twice, filter, be concentrated into 0.2～2g medical material/mL, cold preservation was left standstill 10～24 hours, filtered, and adding water adjustment filter liquor concentration is 0.2～2g medical material/mL, gets Chinese medicine extraction liquid;
(2) carry the ratio of the described Chinese medicine extraction liquid of 80mL in every facial film, get Chinese medicine extraction liquid, dispersant and carrier and make facial film according to a conventional method;
In the above-mentioned steps, described facial film adjuvant comprises dispersant and carrier, wherein,
Described dispersant is selected from propylene glycol, glycerol or ethanol, preferred propylene glycol or glycerol;
Described carrier is gel-type vehicle or non-woven fabrics, and wherein, described gel-type vehicle is one or both in soybean fiber, arabic gum, carrageenan, Konjac glucomannan and the gelatin.
In the preparation method of facial film of the present invention, described adjuvant also can comprise one or both in the following adjuvant:
1. antiseptic:, can be selected from chlorobutanol, benzyl alcohol, phenethanol, methyl hydroxybenzoate, ethyl hydroxybenzoate and the propylparaben one or both, preferably ethyl hydroxybenzoate or propylparaben to prolong the shelf-life of facial film of the present invention.
2. solubilizing agent: optional to increase the dissolving of skin-nourishing thing from tween 80, SP-115A (Xin Pu company) or 1264 emulsifying agents (Xin Pu company).
When facial film of the present invention selects for use gel-type vehicle to be carrier, promptly be the quartzy facial film that is commonly called as, concrete method for making is as follows:
(1) scattered dispersant and gel-type vehicle mixture added in the described Chinese medicine extraction liquid by proportioning, be heated to 80～90 ℃ and fully stirred 15 minutes, transfer to pH5.5～6.5 with the pH regulator agent;
(2) film forming (promptly making facial film), packing, sterilization; Wherein said pH regulator agent is hydrochloric acid, citric acid and phosphate buffer solution.
If the effective ingredient in the described quartzy facial film also comprises skin-nourishing thing and/or other material of whitening, then step (2) should be: add skin-nourishing thing and/or other materials of whitening after being cooled to 50 ℃, mixing, film forming, packing, sterilization.
If described quartzy facial film also contains adjuvants such as antiseptic or solubilizing agent, then when the preparation facial film, described adjuvant and gel-type vehicle are disperseed with dispersant, join in the Chinese medicine extraction liquid again.
When facial film of the present invention selects for use non-woven fabrics to be carrier, promptly be the non-woven fabrics facial film that is commonly called as, concrete method for making is as follows: dispersant is joined in step (1) the gained Chinese medicine extraction liquid, fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing, radiation sterilization, promptly.If the effective ingredient in the described non-woven fabrics facial film also comprises skin-nourishing thing and/or other material of whitening, then skin-nourishing thing and/or other materials of whitening join Chinese medicine extraction liquid with dispersant in the facial film preparation process, and stirring gets final product.
If described non-woven fabrics facial film also contains adjuvants such as antiseptic or solubilizing agent, then when the preparation facial film, described adjuvant is disperseed with dispersant, join in the Chinese medicine extraction liquid again.
Facial film of the present invention as active component, can play the freckle removing and whitening effect with the effective ingredient of Radix Ophiopogonis, Fructus Atriplicis Sibiricae and Radix Ginseng Rubra.
The traditional Chinese medical science is thought lung governing skin and hair, and lack of lung-YIN, fur lack body fluid and moisten fosterly, and then pachylosis is difficult skin care, and complexion is black dull withered and matt, easily produces wrinkle." element asks that the five internal organs generate ": " the tissue connected with the lung being skin, its flourish hair also." in the facial film of the present invention, Radix Ophiopogonis can nourishing YIN and moistening the lung, reinforcing stomach reg fluid, Compendium of Materia Medica are put down in writing it and are had the effect of " U.S. color is pleased skin ", are monarch drug, and Zhang Xichun says: " cool in nature, body fluid is dense lubricious for Radix Asparagi, the little suffering of sweet in the mouth, kind promoting the production of body fluid to quench thirst.The property of Tianjin dope cunning, can tonneau two just, the circulation blood vessels, fluent meridians, though be the product of YIN nourishing, the real energy tonification edema caused by disorder of QI of holding concurrently." so the Radix Asparagi YIN nourishing and the production of body fluid promoting is moisturized, body fluid is popular in all over the body, moist skin; Fructus Atriplicis Sibiricae can dispel the wind soothing the liver, and Compendium of Material Medica is said: " it is black to wash one's face, and speckle dispelling is washed the scar skin ulcer ", and QI and blood is people's a base substance, the QI and blood abundance is then had rosy cheeks, and deficiency of qi and blood is shallow complexion then, Radix Ginseng Rubra energy vigorate qi and replenish the blood, the two is all ministerial drug.Can whiten Radix Ophiopogonis, and Fructus Atriplicis Sibiricae whitening and speckle dispelling, Radix Ginseng Rubra can make again and have rosy cheeks that three medicines share the whitening effect that reaches preferable.
Modern pharmacology studies have shown that the Radix Asparagi tuber contains multiple Zi body Saponin, fructose and aminoacid, can activate Skin Cell, keep skin wet, smooth and elasticity;
In order to understand the present invention better, will further specify the technique effect that the present invention has by clinical experiment report below.
1, patient data: select black female patient 90 examples of yellow complexion, each 45 example of men and women, 30～45 years old age.Be divided into three groups at random, treatment group (Chinese medicine extraction liquid adds the skin nutrient) 30 examples, each 15 example of men and women, at 37 ± 6 years old age, matched group is (carrageenan adds water) 30 examples 1., each 15 example of men and women, at 35 ± 7 years old age, matched group is (Chinese medicine extraction liquid does not add the skin nutrient) 30 examples 2., each 15 example of men and women, 35 ± 8 years old age.
Respectively organize patient's sex, age, symptom integral before the treatment there are no significant difference (P＞0.05), have comparability.
2, experiment material:
(1) treatment group facial film of the present invention is pressed embodiment 1 preparation:
The treatment group: contain the skin-nourishing thing in the effective ingredient of used facial film, press embodiment 1 preparation, every weight is 80 grams, specification 10*15cm.
(2) the matched group facial film prepares by the following method:
Matched group is 1.:
Prescription: carrageenan 11g, ethyl hydroxybenzoate 2g makes 1000g
Method for making: water adds carrageenan after being heated to 80-90 ℃, and ethyl hydroxybenzoate fully stirred 15 minutes, regulates pH value to 5.5-6.5, film forming, packing, sterilization.Every weight is 80 grams, specification 10*15cm.
The treatment group is 2.: do not contain the skin-nourishing thing in the effective ingredient of used facial film, used facial film is pressed embodiment 19 preparations, and every weight is 80 grams, specification 10*15cm.
3, experimental technique:
The treatment group: the patient lies on the back, and after washing one's face, spreads on face with facial film of the present invention, flush away behind about 15min.3 times weekly, be 2 weeks the course of treatment.
Matched group: the patient lies on the back, and after washing one's face, spreads on face, flush away behind about 15min with matched group facial film (not drug ingredients) and embodiment 19 facial films 1..3 times weekly, be 2 weeks the course of treatment.
4, clinical symptoms standards of grading: yellow complexion is black glossyly to be designated as 2 fens, is designated as 1 fen if shoal after the medication; The black tarnish of yellow complexion is designated as 4 fens; Complexion is withered and yellow dark and gloomyly to be had no gloss and is designated as 8 fens.
5, efficacy assessment standard:
By formula earlier---score value * 100% calculates the improvement rate before clinical symptoms integration score value improvement rate=(symptom integral score value before the treatment-treatment back symptom integral score value)/treatment, adopts following standard rating curative effect then.
Produce effects: symptom integral score value improvement rate 〉=70%;
Effectively: symptom integral score value improvement rate 〉=50%;
Invalid: symptom is not seen obvious improvement or is instead seen deterioration, symptom integral score value improvement rate＜50%.
6, statistical procedures: total data adopts SPSS 13.0 statistics softwares to carry out statistical analysis, and total data adopts SPSS13.0 statistics software to carry out statistical analysis, and measurement data adopts the t check, and enumeration data adopts the x2 check.
7, result of the test
The clinical symptoms scoring relatively sees Table 1 before and after treatment group and the treatment of control group, and curative effect relatively sees Table 2 before and after treatment group and the treatment of control group, and treatment group and the improvement of matched group cardinal symptom sign relatively see Table 3.As known from Table 2, facial film of the present invention is whitened total effective rate up to 83%, and observes nothing through the treatment group and find skin heating, flushing, edema, untoward reaction such as pruritus.
Clinical symptoms scoring before and after table 1 treatment group and the treatment of control group
| Group | n | Before the treatment | After the treatment | Difference |
| The treatment group | 30 | 4.07±1.23 | 2.07±1.14 | 2.00±1.31 |
| Matched group 1. | 30 | 4.27±1.64 | 3.73±1.46 | 0.53±1.17 |
| Matched group 2. | 30 | 4.20±1.42 | 2.43±1.13 | 1.77±1.45 |
Table 2 treatment group and matched group curative effect are relatively
| Group | Case load | Produce effects | Effectively | Invalid | Total effective rate/% |
| The treatment group | 30 | 8 | 17 | 5 | 83.3 |
| Matched group 1. | 30 | 0 | 2 | 28 | 6.7 |
| Matched group 2. | 30 | 6 | 17 | 7 | 76.7 |
1. treatment group and matched group compare, and P＜0.01 illustrates the evident in efficacy of medicine.
2. treatment group and matched group compare P＞0.05, what main therapeutical effect had been described is Chinese medicine extraction liquid, but from the treatment before and after integration difference as can be seen, Chinese medicine extraction liquid adds skin-nourishing thing group (i.e. treatment group) and does not add skin nutrient group (be matched group 2.) and relatively, can play whitening function preferably.
Table 3 treatment group and matched group cardinal symptom sign are improved relatively
Routine number in the last table is two groups of case loads that improve, and percent is the improvement example number/hundreds of proportions by subtraction of treatment precedent of two groups of symptoms.Learn by statistics and handle, the equal difference of symptom is (P＜0.01) significantly.
The specific embodiment
Among the following embodiment 1～19, the recipe quantity of each embodiment is the recipe quantity of 12.5 facial films.
Embodiment 1
Prescription:
Fructus Atriplicis Sibiricae 178g, Radix Ginseng Rubra 127g, Radix Ophiopogonis 165g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.5: 1 medicinal liquid (0.5g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes, regulate pH value, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein to 5.5-6.5, mixing, make dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).Because hyaluronic acid than indissoluble, is difficult to homodisperse with medicinal liquid is directly mixed mutually, obtains the hyalomitome acid solution so earlier hyaluronic acid is dissolved in the water, and then mixes with medicinal liquid.
Embodiment 2
Prescription:
Fructus Atriplicis Sibiricae 360g, Radix Ginseng Rubra 60g, Radix Ophiopogonis 240g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, add and add 8 times of water gagings for the first time, for the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid, filter, it is concentrated that (the 0.63g medical material/ml), cold preservation was left standstill 24 hours, filtered into about 0.63: 1 medicinal liquid, adjust filtrate and become 0.63: 1 medicinal liquid (0.63g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add rose essence, 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 3
Prescription:
Fructus Atriplicis Sibiricae 120g, Radix Ginseng Rubra 360g, Radix Ophiopogonis 400g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Semen Ziziphi Spinosae, Semen Platycladi, Poria decocts with water secondary, adds 8 times of water gagings for the first time, for the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid, filter, it is concentrated that (the 0.85g medical material/ml), cold preservation was left standstill 24 hours, filtered into about 0.85: 1 medicinal liquid, adjust filtrate and become 0.85: 1 medicinal liquid (0.85g medical material/ml), add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate gold ethyl ester are heated to 80-90 ℃ and fully stirred 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add rose essence, 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 4
Prescription:
Fructus Atriplicis Sibiricae 282g, Radix Ginseng Rubra 282g, Radix Ophiopogonis 846g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 1.5: 1 medicinal liquids (1.5g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 1.5: 1 medicinal liquid (1.5g medical materials/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes, regulate pH value, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein to 5.5-6.5, mixing, make dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 5
Prescription:
Fructus Atriplicis Sibiricae 760g, Radix Ginseng Rubra 320g, Radix Ophiopogonis 800g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 2: 1 medicinal liquids (2g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 2: 1 medicinal liquid (2g medical materials/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes, regulate pH value, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein to 5.5-6.5, mixing, make dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 6
Prescription:
Fructus Atriplicis Sibiricae 90g, Radix Ginseng Rubra 40g, Radix Ophiopogonis 70g;
Soybean fiber 13g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 1g propylparaben 1g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, be condensed into 0.2: 1 medicinal liquid (0.2g medical material/ml), cold preservation was left standstill 24 hours, filter, moisturizing is adjusted filtrate and is become 0.2: 1 medicinal liquid (0.2g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, propylparaben is heated to 80-90 ℃ and fully stirred 15 minutes, regulates pH value to 5.5-6.5, is cooled to about 50 ℃ and adds 0.5% hyalomitome acid solution and collagen protein, mixing, make dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 7
Prescription:
Fructus Atriplicis Sibiricae 165g, Radix Ginseng Rubra 117g, Radix Ophiopogonis 188g;
Carrageenan 13g, ethanol 50g, hyaluronic acid 0.1g, collagen protein 5g, ethyl hydroxybenzoate 1g propylparaben 1g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.5: 1 medicinal liquid (0.5g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get scattered ethanol, carrageenan, ethyl hydroxybenzoate and the propylparaben of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 8
Prescription:
Fructus Atriplicis Sibiricae 188g, Radix Ginseng Rubra 141g, Radix Ophiopogonis 141g;
Carrageenan 13g, ethanol 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.5: 1 medicinal liquid (0.5g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get scattered ethanol carrageenan of Chinese medicine extraction liquid adding and ethyl hydroxybenzoate and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 9
Prescription:
Fructus Atriplicis Sibiricae 190g, Radix Ginseng Rubra 80g, Radix Ophiopogonis 200g;
Soybean fiber 11g, glycerol 50g, hyaluronic acid 0.1g, collagen protein 50g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.54: 1 medicinal liquid (0.54g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.54: 1 medicinal liquid (0.54g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get scattered glycerol, carrageenan and the ethyl hydroxybenzoate of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 10
Prescription:
Fructus Atriplicis Sibiricae 190g, Radix Ginseng Rubra 80g, Radix Ophiopogonis 200g;
Carrageenan 10g, arabic gum 3g, propylene glycol 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 10 times of water gagings for the first time, add 8 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.53: 1 medicinal liquid (0.53g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.53: 1 medicinal liquid (0.53g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get scattered propylene glycol, carrageenan, arabic gum and the ethyl hydroxybenzoate of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 11
Prescription:
Fructus Atriplicis Sibiricae 190g, Radix Ginseng Rubra 80g, Radix Ophiopogonis 200g;
Carrageenan 11g, arbutin 60g, propylene glycol 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 10 times of water gagings for the first time, add 10 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.57: 1 medicinal liquid (0.57g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.57: 1 medicinal liquid (0.57g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get scattered propylene glycol, carrageenan and the ethyl hydroxybenzoate of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution, collagen protein and arbutin, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 12
Prescription:
Fructus Atriplicis Sibiricae 190g, Radix Ginseng Rubra 80g, Radix Ophiopogonis 200g;
Carrageenan 11g, arbutin 10g, propylene glycol 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 8 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.53: 1 medicinal liquid (0.53g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.53: 1 medicinal liquid (0.53g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get scattered propylene glycol, carrageenan and the ethyl hydroxybenzoate of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution, collagen protein and arbutin, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 13
Prescription:
Fructus Atriplicis Sibiricae 190g, Radix Ginseng Rubra 80g, Radix Ophiopogonis 200g;
Carrageenan 11g, Magnesium L-Asacorbic Acid 2-O-Phosphate 10g, propylene glycol 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.54: 1 medicinal liquid (0.54g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.54: 1 medicinal liquid (0.54g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get scattered propylene glycol, carrageenan and the ethyl hydroxybenzoate of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add former albumen of 0.5% hyaluronic acid sol and Magnesium L-Asacorbic Acid 2-O-Phosphate, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 14
Prescription:
Fructus Atriplicis Sibiricae 190g, Radix Ginseng Rubra 80g, Radix Ophiopogonis 200g;
Carrageenan 11g, Magnesium L-Asacorbic Acid 2-O-Phosphate 60g, propylene glycol 50g, hyaluronic acid 0.25g, collagen protein 10g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.57: 1 medicinal liquid (0.57g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.57: 1 medicinal liquid (0.57g medical material/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, get scattered propylene glycol, carrageenan and the ethyl hydroxybenzoate of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add 0.5% hyalomitome acid solution and collagen protein, Magnesium L-Asacorbic Acid 2-O-Phosphate, mixing, make dissolving fully, film forming, packing, sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 15
Prescription:
Fructus Atriplicis Sibiricae 543g, Radix Ginseng Rubra 229g, Radix Ophiopogonis 571g;
Hyaluronic acid 0.36g, collagen protein 18g, propylene glycol 180g.
Method for making: Radix Codonopsis, the Radix Astragali, Poria, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 1.74: 1 medicinal liquids (1.74g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 1.74: 1 medicinal liquid 1.74g medical materials/ml), Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with 1% scattered hyalomitome acid solution and collagen protein of propylene glycol, fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing, sterilization, promptly.
In the above-mentioned steps, described 1% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 1% (w/w).
Embodiment 16
Prescription:
Fructus Atriplicis Sibiricae 500g, Radix Ginseng Rubra 180g, Radix Ophiopogonis 550g;
Hyaluronic acid 0.1g, collagen protein 5g, Semen Tritici aestivi germ oil 20g, propylene glycol 50g, 1264 emulsifying agents (Xin Pu company) 4g.
Method for making: Radix Codonopsis, the Radix Astragali, Poria, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 1.36: 1 medicinal liquids (1.36g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 1.36: 1 medicinal liquid (1.36g medical materials/ml), get Chinese medicine extraction liquid; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film, getting Chinese medicine extraction liquid adds with scattered 1264 emulsifying agents, Oleum menthae, Semen Tritici aestivi germ oil, 0.5% hyalomitome acid solution and the collagen protein of propylene glycol, fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing, radiation sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 17
Prescription:
Fructus Atriplicis Sibiricae 543g, Radix Ginseng Rubra 229g, Radix Ophiopogonis 571g;
Hyaluronic acid 0.1g, collagen protein 5g, Semen Tritici aestivi germ oil 20g, propylene glycol 50g, SP-115A (Xin Pu company) 4g.
Method for making: Radix Codonopsis, the Radix Astragali, Poria, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 1.74: 1 medicinal liquids (1.74g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 1.74: 1 medicinal liquid 1.74g medical materials/ml), Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with scattered SP-115A, Semen Tritici aestivi germ oil, 0.5% hyalomitome acid solution and the collagen protein of propylene glycol, fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing, radiation sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 18
Prescription:
Fructus Atriplicis Sibiricae 250g, Radix Ginseng Rubra 150g, Radix Ophiopogonis 300g;
Hyaluronic acid 0.1g, collagen protein 5g, Semen Tritici aestivi germ oil 20g, propylene glycol 50g, tween 80 10g.
Method for making: Radix Codonopsis, the Radix Astragali, Poria, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.79: 1 medicinal liquid (0.79g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.79: 1 medicinal liquid (0.79g medical material/ml), get Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with scattered tween 80, Semen Tritici aestivi germ oil, 0.5% hyalomitome acid solution and the collagen protein of propylene glycol, fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing, radiation sterilization, promptly.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 19
Prescription:
Fructus Atriplicis Sibiricae 190g, Radix Ginseng Rubra 80g, Radix Ophiopogonis 200g;
Carrageenan 11g, propylene glycol 50g, ethyl hydroxybenzoate 2g.
Method for making:
Get Fructus Atriplicis Sibiricae, Radix Ginseng Rubra and Radix Ophiopogonis, decoct with water secondary, add 8 times of water gagings for the first time, add 6 times of water gagings for the second time, each 3 hours, merge the secondary decocting liquid, filter, concentrate into about 0.5: 1 medicinal liquid (0.5g medical material/ml), cold preservation was left standstill 24 hours, filter, adjust filtrate and become 0.5: 1 medicinal liquid (0.5g medical material/ml), get Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes, regulate pH value to 5.5-6.5, mixing makes dissolving fully, film forming, packing, sterilization, promptly.
Claims (10)
1. Chinese medicine facial film of whitening, this facial film is made up of effective components of Chinese medicinal and facial film field acceptable auxiliary, it is characterized in that described effective ingredient comprises that concentration is the Chinese medicine extraction liquid of 0.2～2g medical material/mL; Described Chinese medicine extraction liquid is obtained by the Chinese medicine water decocting method extraction of following weight proportion: Fructus Atriplicis Sibiricae 15%～60%, Radix Ginseng Rubra 10%～45%, Radix Ophiopogonis 15%～60%; Every facial film is loaded with described Chinese medicine extraction liquid 80mL.
2. facial film according to claim 1 is characterized in that described Chinese medicine extraction liquid is extracted by the Chinese medicine water decocting method of following weight proportion to obtain: Fructus Atriplicis Sibiricae 35%～40%, Radix Ginseng Rubra 25%～30%, Radix Ophiopogonis 30%～40%.
3. facial film according to claim 1, it is characterized in that described effective ingredient also comprises occupies the skin-nourishing thing of imitating composition 0.05～6% (W/W), and described skin-nourishing thing is selected from Semen Tritici aestivi germ oil, a kind of or two or more in hyaluronic acid and the collagen protein.
4. as facial film as described in the claim 3, the described effective ingredient of its feature is also to comprise other whitening medicaments of 1～6% (W/W), and described other whitening medicaments are arbutin or Magnesium L-Asacorbic Acid 2-O-Phosphate.
5. the preparation method of claim 1 or 2 described facial films, this method is made up of following steps:
(1) gets Radix Ophiopogonis, Fructus Atriplicis Sibiricae and Radix Ginseng Rubra, decoct with water twice, add 6～10 times for the first time and decocted 1.5～3 hours, add 6～10 times for the second time and decocted 1.5～3 hours; Merge decocting liquid twice, filter, be concentrated into 0.2～2g medical material/mL, cold preservation was left standstill 10～24 hours, filtered, and adding water adjustment filter liquor concentration is 0.2～2g medical material/mL, gets Chinese medicine extraction liquid;
(2) carry the ratio of the described Chinese medicine extraction liquid of 80mL in every facial film, get Chinese medicine extraction liquid and the facial film adjuvant is made facial film according to a conventional method;
In the above-mentioned steps, described facial film adjuvant comprises dispersant and carrier, wherein,
Described dispersant is selected from propylene glycol, glycerol or ethanol;
Described carrier is gel-type vehicle or non-woven fabrics, and wherein, described gel-type vehicle is one or both in soybean fiber, arabic gum, carrageenan, Konjac glucomannan and the gelatin.
6. as method as described in the claim 5, it is characterized in that described dispersant is propylene glycol or glycerol.
7. as method as described in the claim 5, it is characterized in that described facial film adjuvant also comprises antiseptic, described antiseptic is one or both in chlorobutanol, benzyl alcohol, phenethanol, methyl hydroxybenzoate, ethyl hydroxybenzoate and the propylparaben.
8. as method as described in the claim 7, it is characterized in that described antiseptic is ethyl hydroxybenzoate or propylparaben.
9. as method as described in the claim 5, it is characterized in that described facial film adjuvant also comprises solubilizing agent, described solubilizing agent is a tween 80.
10. as method as described in the claim 6, it is characterized in that described facial film adjuvant also comprises solubilizing agent, described solubilizing agent is a tween 80.
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| CN102475658A (en) * | 2010-11-29 | 2012-05-30 | 吴克 | Crystal mask |
| CN102657780B (en) * | 2012-05-31 | 2013-11-06 | 王孟理 | Freckle-dispelling Chinese medicinal beautifying cream and preparation method thereof |
| CN103655369A (en) * | 2013-12-23 | 2014-03-26 | 青岛安信医疗器械有限公司 | Mask essence |
| CN106726915A (en) * | 2016-12-15 | 2017-05-31 | 孟炜 | Crystal mask |
| CN109998948A (en) * | 2017-12-29 | 2019-07-12 | 辽宁上药好护士健康科技有限公司 | A kind of preparation method of red ginseng sleep mask |
| CN112870143A (en) * | 2021-04-19 | 2021-06-01 | 湖南中医药大学 | Traditional Chinese medicine mask for nourishing yin and promoting blood circulation and preparation method thereof |
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| CN1059554C (en) * | 1994-10-13 | 2000-12-20 | 赖晓梅 | Paper beautifying face mask and its preparing method thereof |
| CN1212111C (en) * | 2002-12-24 | 2005-07-27 | 于璟玲 | Chinese medicinal skin-beautifying honey and preparing method thereof |
| CN101606899A (en) * | 2009-07-28 | 2009-12-23 | 李芸 | A kind of Chinese medicine freckle whitening makeup |
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Effective date of registration: 20160119 Address after: 510660 Tianhe District, Guangzhou, Huang Village Road, No. 55, building No. 3, No. Patentee after: Gao Kang Cosmetics Manufacturing Co.,Ltd. Address before: 510665, No. two, 30, Xinzhuang Road, Yonghe street, Guangzhou, Guangdong, Luogang District Patentee before: Guangdong Yangmei Medicine Investment Co.,Ltd. |
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Address after: 510660 Tianhe District, Guangzhou, Huang Village Road, No. 55, building No. 3, No. Patentee after: GAOKANG DAILY CHEMICAL GROUP Co.,Ltd. Address before: 510660 Tianhe District, Guangzhou, Huang Village Road, No. 55, building No. 3, No. Patentee before: Gao Kang Cosmetics Manufacturing Co.,Ltd. |
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Granted publication date: 20111005 |