CN101798760A - Method for applying moisture control agent in fabric dyeing process - Google Patents
Method for applying moisture control agent in fabric dyeing process Download PDFInfo
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- CN101798760A CN101798760A CN 201010124712 CN201010124712A CN101798760A CN 101798760 A CN101798760 A CN 101798760A CN 201010124712 CN201010124712 CN 201010124712 CN 201010124712 A CN201010124712 A CN 201010124712A CN 101798760 A CN101798760 A CN 101798760A
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Abstract
The invention discloses a method for applying a moisture control agent together with dye in the same bath in a fabric dyeing process, which is characterized in that: the dye is added in the fabric dyeing process, and meanwhile the moisture control agent accounting for 0.1 to 5 percent of the weight of the fabric is also added, namely the moisture control agent and the dye are used in the same bath. The moisture control agent comprises the following components in part by weight: 80 to 100 parts of polyethylene glycol, 10 to 15 parts of ethylene glycol, 10 to 14 parts of polyether, 15 to 18 parts of dimethyl terephthalate and 0.2-1 part of metal acetate serving as a catalyst. The method can be widely applied to the dyeing process of the polyester fiber fabric.
Description
Technical field
The present invention relates to the textile dyeing field, especially the application process of moisture control agent in the dyeing of polyester fiber.
Background technology
The moisture absorbing and sweat releasing performance of polyester fiber, antistatic property, easily detergency ability, fluffy flexibility are all relatively poor, the back arrangement is main auxiliary agent with aminosilicone emulsifier, but aminosilicone emulsifier only can improve polyester fiber on feel, easily a static, easy pickup can not improve to some extent to it, and non-refractory, easy breakdown of emulsion floating oil during use can not dye and use with in bathing, printing and dyeing mill in use must increase by one more and put gentle operation, does not meet the state basic policy of current energy-saving and emission-reduction consumption reduction.
Summary of the invention
Technical problem to be solved by this invention is: the application process that will provide a kind of moisture control agent to use with one-bath dyeing in fabric dyeing process.
For solving the problems of the technologies described above, the technical solution used in the present invention is: the application process of described moisture control agent in fabric dyeing process, be characterized in: the stage that adds dyestuff in fabric dyeing process adds the moisture control agent that accounts for fabric weight 0.1%~5% simultaneously, and promptly moisture control agent and one-bath dyeing use; Described moisture control agent comprises following composition by weight: 50~100 parts of polyethylene glycol, 10~80 parts of ethylene glycol, 10~40 parts of polyethers, 10~20 parts of dimethyl terephthalate (DMT)s, 0~50 part of end hydroxy polyether organosilicon and as 0.2~1 part of the acetic acid slaine of catalyst.
The further technical scheme of the present invention is: described polyethers is two end hydroxy polyethers.
In described fabric dyeing process, dyeing temperature adds moisture control agent in the time of 80 ℃~130 ℃.
The processing method of above-mentioned moisture control agent is as follows: the polyethylene glycol, ethylene glycol, polyethers, dimethyl terephthalate (DMT) and the acetic acid slaine that one, take by weighing described weight portion; Two, in reactor, drop into polyethylene glycol, ethylene glycol and polyethers, and reactor heated, when rising to 75~80 ℃, temperature begins to vacuumize, make vacuum in the still reach-0.090~-0.095MPa, continue to be warming up to 90~100 ℃ then, after being incubated 50~60 minutes, be warming up to 102~106 ℃, dimethyl terephthalate (DMT) and catalyst are dropped in the reactor, continue to be warming up to 150~160 ℃, and kept 60~90 minutes, allow the abundant esterification of material in the reactor, then the material after the esterification in the reactor is pressed in the polymeric kettle, be-0.095 in vacuum~-0.1MPa and temperature are under 220~250 ℃ the condition, and under the catalysis of acetic acid slaine, through 40~60 minutes polymerization, the generation molecular weight was 10000~50000 polyester and polyether block copolymer, polyester and polyether/organic silicon block copolymer, blowing after being cooled to 140~160 ℃ then obtains finished product.
The invention has the beneficial effects as follows: moisture control agent and one-bath dyeing are used, can not increase operation in addition, meet the development trend of current energy-saving and emission-reduction; And make the polyester fiber of treated mistake have good moisture absorbing and sweat releasing, antistatic behaviour, fluffy flexibility and easy detergency ability.
The specific embodiment
The present invention is described in further detail below by specific embodiment, but the present invention should not only limit to these embodiment.
Embodiment 1
In the dacron fabric dyeing, moisture control agent and DISPERSE DYES red [C.I.Disperse red60 (60756)] and levelling agent are added together, the addition of moisture control agent is 0.3% of a fabric weight, described moisture control agent comprises following composition by weight: 50 parts of polyethylene glycol, 10 parts of ethylene glycol, 10 parts of polyethers, 10 parts of dimethyl terephthalate (DMT)s, 0 part of end hydroxy polyether organosilicon and as 0.2 part of the acetic acid slaine of catalyst.Dyeing temperature uses in the time of 130 ℃.Polyester fiber after the use not only has fluffy flexibility, also has good antistatic property simultaneously.
Embodiment 2
Yellow and levelling agent adds together with moisture control agent and DISPERSE DYES in the dacron fabric dyeing, the addition of moisture control agent is 0.1% of a fabric weight, described moisture control agent comprises following composition by weight: 50~100 parts of polyethylene glycol, 10~80 parts of ethylene glycol, 30 parts of polyethers, 15 parts of dimethyl terephthalate (DMT)s, 25 parts of end hydroxy polyether organosilicons and as 0.6 part of the acetic acid slaine of catalyst.Dyeing temperature uses in the time of 110 ℃.Polyester fiber after the use not only has fluffy flexibility, also has well easily detergency ability simultaneously.
Embodiment 3
Black and levelling agent adds together with moisture control agent and DISPERSE DYES in the dacron fabric dyeing, the addition of moisture control agent is 4% of a fabric weight, described moisture control agent comprises following composition by weight: 100 parts of polyethylene glycol, 80 parts of ethylene glycol, 40 parts of polyethers, 20 parts of dimethyl terephthalate (DMT)s, 50 parts of end hydroxy polyether organosilicons and as 1 part of the acetic acid slaine of catalyst.Dyeing temperature uses in the time of 95 ℃.Polyester fiber after the use not only has moisture absorbing and sweat releasing, also has well antistatic, flexibility simultaneously.
Claims (3)
1. the application process of moisture control agent in fabric dyeing process is characterized in that: the stage that adds dyestuff in fabric dyeing process adds the moisture control agent that accounts for fabric weight 0.1%~5% simultaneously; Described moisture control agent comprises following composition by weight: 50~100 parts of polyethylene glycol, 10~80 parts of ethylene glycol, 10~40 parts of polyethers, 10~20 parts of dimethyl terephthalate (DMT)s, 0~50 part of end hydroxy polyether organosilicon and as 0.2~1 part of the acetic acid slaine of catalyst.
2. the application process of moisture control agent according to claim 1 in fabric dyeing process is characterized in that: described polyethers is two end hydroxy polyethers.
3. the application process of moisture control agent according to claim 1 and 2 in fabric dyeing process is characterized in that: in described fabric dyeing process, dyeing temperature adds moisture control agent in the time of 80 ℃~130 ℃.
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CN 201010124712 CN101798760A (en) | 2010-03-08 | 2010-03-08 | Method for applying moisture control agent in fabric dyeing process |
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CN 201010124712 CN101798760A (en) | 2010-03-08 | 2010-03-08 | Method for applying moisture control agent in fabric dyeing process |
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Cited By (17)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103114440A (en) * | 2013-03-14 | 2013-05-22 | 浙江金三发非织造布有限公司 | Production technology of full terylene non-woven fabric with hydrophilic function |
CN103321054A (en) * | 2013-06-07 | 2013-09-25 | 张家港市德宝化工有限公司 | Fluffy and soft finishing agent used for polyester fiber, and preparation method thereof |
CN103321049A (en) * | 2013-06-07 | 2013-09-25 | 张家港市德宝化工有限公司 | Washing-resistant agent used for polyester fiber, and preparation method thereof |
CN103321038A (en) * | 2013-06-07 | 2013-09-25 | 张家港市德宝化工有限公司 | Decontamination finishing agent used for polyester fiber, and preparation method thereof |
CN104060428A (en) * | 2014-05-30 | 2014-09-24 | 浙江圣山科纺有限公司 | Moisture-absorption sweat-releasing or antistatic gray fabric dyeing and after-finishing method |
CN105401433A (en) * | 2015-12-16 | 2016-03-16 | 张家港市德宝化工有限公司 | Moisture-absorbing sweat-releasing finishing agent used for polyester fiber materials and having no influence on color fastness and preparation method thereof |
CN106192264A (en) * | 2016-07-27 | 2016-12-07 | 江苏新凯盛企业发展有限公司 | A kind of method for sorting improving brocade ammonia knitted fabric moisture absorbing and sweat releasing performance |
WO2017063849A1 (en) * | 2015-10-12 | 2017-04-20 | Sabic Global Technologies B.V. | Polyether ester block copolymers |
CN106835718A (en) * | 2017-01-09 | 2017-06-13 | 佛山市广嘉纺织科技有限公司 | A kind of method for sorting and pure cotton fabric of pure cotton fabric moisture absorbing and sweat releasing quick-drying |
CN107574666A (en) * | 2017-09-04 | 2018-01-12 | 上海维胜化工有限公司 | A kind of durable antistatic agent and its preparation method and application |
CN107938354A (en) * | 2017-11-30 | 2018-04-20 | 英泰时尚服饰(苏州)有限公司 | A kind of preparation method of moisture absorbing and sweat releasing deodorization finishing agent |
CN107938367A (en) * | 2017-11-30 | 2018-04-20 | 英泰时尚服饰(苏州)有限公司 | A kind of moisture absorbing and sweat releasing microcapsule dressing agent and preparation method thereof |
CN109056389A (en) * | 2018-07-03 | 2018-12-21 | 常州旭荣针织印染有限公司 | With uvioresistant, absorbing fast-drying, crease-resistant complex function the CDP fabrics/polyester fibre/spandex fabric dyeing and finishing process |
CN111172781A (en) * | 2020-01-20 | 2020-05-19 | 宁波萌恒线业有限公司 | High-temperature leveling agent and preparation method thereof |
CN111945440A (en) * | 2020-07-15 | 2020-11-17 | 纳派化学(上海)有限公司 | Polyester textile fabric with single-side moisture-conducting function and preparation method thereof |
CN114737397A (en) * | 2022-05-17 | 2022-07-12 | 广东德美精细化工集团股份有限公司 | Preparation method of moisture-absorbing and sweat-releasing finishing agent for polyester fabric containing anthracene structure |
CN116263032A (en) * | 2022-11-29 | 2023-06-16 | 浙江科峰有机硅股份有限公司 | Dyeing one-bath moisture-absorbing sweat-releasing agent, preparation method and application thereof |
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CN101424046A (en) * | 2008-11-21 | 2009-05-06 | 张家港市德宝化工有限公司 | Polyester fiber modifying agent as well as preparation method and use thereof |
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Cited By (25)
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CN103114440A (en) * | 2013-03-14 | 2013-05-22 | 浙江金三发非织造布有限公司 | Production technology of full terylene non-woven fabric with hydrophilic function |
CN103114440B (en) * | 2013-03-14 | 2014-09-03 | 浙江金三发非织造布有限公司 | Production technology of full terylene non-woven fabric with hydrophilic function |
CN103321054A (en) * | 2013-06-07 | 2013-09-25 | 张家港市德宝化工有限公司 | Fluffy and soft finishing agent used for polyester fiber, and preparation method thereof |
CN103321049A (en) * | 2013-06-07 | 2013-09-25 | 张家港市德宝化工有限公司 | Washing-resistant agent used for polyester fiber, and preparation method thereof |
CN103321038A (en) * | 2013-06-07 | 2013-09-25 | 张家港市德宝化工有限公司 | Decontamination finishing agent used for polyester fiber, and preparation method thereof |
CN103321038B (en) * | 2013-06-07 | 2015-08-05 | 张家港市德宝化工有限公司 | For the soil release finishing agent and preparation method thereof of polyester fiber |
CN103321049B (en) * | 2013-06-07 | 2015-08-05 | 张家港市德宝化工有限公司 | For the resistance to lotion and preparation method thereof of polyester fiber |
CN103321054B (en) * | 2013-06-07 | 2016-01-13 | 张家港市德宝化工有限公司 | A kind of polyester fiber fluffy soft finishing agent and preparation method thereof |
CN104060428A (en) * | 2014-05-30 | 2014-09-24 | 浙江圣山科纺有限公司 | Moisture-absorption sweat-releasing or antistatic gray fabric dyeing and after-finishing method |
WO2017063849A1 (en) * | 2015-10-12 | 2017-04-20 | Sabic Global Technologies B.V. | Polyether ester block copolymers |
CN105401433A (en) * | 2015-12-16 | 2016-03-16 | 张家港市德宝化工有限公司 | Moisture-absorbing sweat-releasing finishing agent used for polyester fiber materials and having no influence on color fastness and preparation method thereof |
CN106192264A (en) * | 2016-07-27 | 2016-12-07 | 江苏新凯盛企业发展有限公司 | A kind of method for sorting improving brocade ammonia knitted fabric moisture absorbing and sweat releasing performance |
CN106835718A (en) * | 2017-01-09 | 2017-06-13 | 佛山市广嘉纺织科技有限公司 | A kind of method for sorting and pure cotton fabric of pure cotton fabric moisture absorbing and sweat releasing quick-drying |
CN106835718B (en) * | 2017-01-09 | 2018-09-28 | 佛山市广嘉纺织科技有限公司 | A kind of method for sorting and pure cotton fabric of pure cotton fabric moisture absorbing and sweat releasing quick-drying |
CN107574666A (en) * | 2017-09-04 | 2018-01-12 | 上海维胜化工有限公司 | A kind of durable antistatic agent and its preparation method and application |
CN107938354A (en) * | 2017-11-30 | 2018-04-20 | 英泰时尚服饰(苏州)有限公司 | A kind of preparation method of moisture absorbing and sweat releasing deodorization finishing agent |
CN107938367A (en) * | 2017-11-30 | 2018-04-20 | 英泰时尚服饰(苏州)有限公司 | A kind of moisture absorbing and sweat releasing microcapsule dressing agent and preparation method thereof |
CN109056389A (en) * | 2018-07-03 | 2018-12-21 | 常州旭荣针织印染有限公司 | With uvioresistant, absorbing fast-drying, crease-resistant complex function the CDP fabrics/polyester fibre/spandex fabric dyeing and finishing process |
CN109056389B (en) * | 2018-07-03 | 2021-03-16 | 常州旭荣针织印染有限公司 | Dyeing and finishing process of cationic dyeable terylene/spandex fabric with ultraviolet-resistant, moisture-absorbing, quick-drying and crease-resistant composite functions |
CN111172781A (en) * | 2020-01-20 | 2020-05-19 | 宁波萌恒线业有限公司 | High-temperature leveling agent and preparation method thereof |
CN111172781B (en) * | 2020-01-20 | 2022-12-06 | 宁波萌恒线业有限公司 | High-temperature leveling agent and preparation method thereof |
CN111945440A (en) * | 2020-07-15 | 2020-11-17 | 纳派化学(上海)有限公司 | Polyester textile fabric with single-side moisture-conducting function and preparation method thereof |
CN114737397A (en) * | 2022-05-17 | 2022-07-12 | 广东德美精细化工集团股份有限公司 | Preparation method of moisture-absorbing and sweat-releasing finishing agent for polyester fabric containing anthracene structure |
CN114737397B (en) * | 2022-05-17 | 2024-02-06 | 广东德美精细化工集团股份有限公司 | Preparation method of anthracene structure-containing polyester fabric moisture-absorbing and sweat-releasing finishing agent |
CN116263032A (en) * | 2022-11-29 | 2023-06-16 | 浙江科峰有机硅股份有限公司 | Dyeing one-bath moisture-absorbing sweat-releasing agent, preparation method and application thereof |
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Application publication date: 20100811 |