CN101731463A - By-pass betaine coated product and preparation method thereof - Google Patents
By-pass betaine coated product and preparation method thereof Download PDFInfo
- Publication number
- CN101731463A CN101731463A CN201010017691A CN201010017691A CN101731463A CN 101731463 A CN101731463 A CN 101731463A CN 201010017691 A CN201010017691 A CN 201010017691A CN 201010017691 A CN201010017691 A CN 201010017691A CN 101731463 A CN101731463 A CN 101731463A
- Authority
- CN
- China
- Prior art keywords
- betaine
- pass
- coated product
- alkali lye
- beet alkali
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Fodder In General (AREA)
Abstract
The invention discloses a by-pass betaine coated product and a preparation method thereof. The by-pass betaine coated product is prepared from betaine liquid white carbon black grains containing 38 to 45 weight percent of betaine liquid through hydroxypropyl methyl cellulose coating, and the betaine liquid white carbon black grains containing 38 to 45 weight percent of betaine liquid are obtained by stirring, mixing, drying and granulating 65 to 70 weight percent of pure betaine liquid and white carbon black. The betaine provided by the invention has comprehensive functions and stable quality, can be widely applied to monogastric animals and ruminants, is easy to be absorbed in animal bodies, and particularly is not easy to degrade when passing through the rumens of the ruminants; and because the betaine is protected in the rumen, the betaine can be successfully absorbed in the true stomach and intestinal tracts of the ruminant so as to play the function. The preparation method for the by-pass betaine coated product provided by the invention has the advantages of reasonable process design, strong operability and low production cost, and can realize industrialized large production.
Description
Technical field
The present invention relates to a kind of feed addictive, be specifically related to the preparation method of a kind of pass betaine coated product and this pass betaine coated product thereof.
Background technology
The betaine range of application is a cultivated animals in the China's name Ministry of Agriculture of republic No. 1126 feed addictive kinds catalogue (2008).It efficiently provides active methyl for animal body, substituting methionine interpolation participation protein and lipid metabolism has the alleviation of the osmotic pressure of adjusting emergent, food calling promotes to search for food, antibacterial bacteriostatic, suppress major physiological effects such as coccidia, extensively utilize betaine as fish in the world, monogastric animal feed additives such as pig, chicken have not yet to see betaine successful Application on ruminant.
Because ruminant microecosystem more complicated.Therefore many additives were as adopting the cud technology,
Degrade in cud, finally not reaching enteron aisle is the purpose that animal absorbs.Have only nutritive additive methionine and unrighted acid to adopt the product of cud technical measures to be applied on the milk cow at present, and methionine to cost an arm and a leg be 3～4 times of betaine, utilized cud technical measures development product---pass betaine, substituting methionine adds, not only save cost, more can bring into play outside the trophic function of betaine, also have functions such as antibacterial bacteriostatic, adjusting osmotic pressure.
Summary of the invention
Goal of the invention: the objective of the invention is to fail and be applied to technical deficiency on the ruminant in order to solve existing betaine, provide a kind of can be applied to ruminant raise in, steady quality, safe and reliable, the pass betaine coated product that production cost is low, another object of the present invention provide the preparation method of this pass betaine coated product.
Technical scheme: in order to realize above purpose, the technical scheme that the present invention takes is:
A kind of pass betaine coated product, it is to be prepared through the hydroxypropyl methylcellulose coating by the beet alkali lye silica particles that contains 38～45% percentage by weight beet alkali lye, the described beet alkali lye silica particles that contains 38～45% percentage by weight beet alkali lye is to be that 65～70% pure beet alkali lye and white carbon mix by percentage by weight, prepares.
Above-described pass betaine coated product, described silica particles are 20～30 orders.Because white carbon is a kind of sorbing material of multi-pore structure, when beet alkali lye and white carbon mixing, white carbon with multi-pore structure can adsorb the effect that beet alkali lye can reach abundant mixing and absorption, and white carbon has good tack, chemical stability, high compactness, anti-ion permeability and has the effect of adsorbing pathogen preferably, and white carbon and coated fertilizer hydroxypropyl methylcellulose have close physicochemical properties, the two can play synergy, can improve the coating rate of beet alkali lye, betaine coated product quality is higher.
As preferably, above-described pass betaine coated product, after described silica particles and hydroxypropyl methylcellulose packaging material mix, prepare through vaporific spraying coating, preparing coated product sieves through 0.84～0.59mm sieve and obtains pass betaine coated product, the present invention prepares the betaine coated product by vaporific spraying coating process and has high coating rate, and coating rate can reach 80%-90%.
The coated product particle diameter is controlled at 0.84～0.59mm, is difficult for degraded when the betaine coated product is by cud like this, and betaine is protected in cud, and in abomasum, enteron aisle higher absorptivity is arranged, thereby can give full play to the function of betaine.
Pass betaine coated product of the present invention, wherein the percentage by weight of moisture is controlled lower amount of moisture in the betaine coated product less than 5%, the long term storage of betaine coated product energy, stability strengthens.
The preparation method of pass betaine coated product provided by the invention specifically may further comprise the steps:
1. get percentage by weight and be 65～70% pure beet alkali lye portion, be heated to 80～82 ℃, join in the mixer, the white carbon that adds 0.89～1.05 part again, mix, stir into solid, again through the granulator back drying of granulating, obtain beet alkali lye weight percentage and be 38～45% beet alkali lye silica particles, standby;
2. getting 5～6 parts of hydroxypropyl methylcelluloses, is the dissolving of 70～75% ethanol with 95～98 parts of concentration, obtains packaging material, standby;
3. get 1 part of the beet alkali lye silica particles that 1. step obtain, the packaging material that 2. obtains 0.75～0.9 part with step carries out vaporific spraying coating at bag in by machine, and preparing sieves through the 0.84-0.59mm sieve behind the coated product again obtains pass betaine coated product.
As preferably, the particle diameter of the preparation method of above-described pass betaine coated product, step used white carbon in 1. is 20～30 orders.And the weight percentage of beet alkali lye is 40% in the beet alkali lye silica particles that step obtains in 1..
As another preferred version, the preparation method of pass betaine coated product, step 2. in hydroxypropyl methylcellulose be to be that 7 concentration are that 70% ethanol dissolves that to prepare coated fertilizer standby with pH value.
The preparation method of pass betaine coated product of the present invention, wherein step 1. the granulator granulating process can adopt conventional granulator to prepare.
The preparation method of pass betaine coated product of the present invention, wherein the 3. vaporific spraying coating process of step is: 40% betaine particle is dropped in the end spray dressing bed, being preheated to 35～40 ℃ and air inducing (5mmH2O post) makes it to be suspended in the bed, regulate atomisation pressure about 0.3MPa, make coating buffer form the vaporific quilt that wraps, 40～45 ℃ of temperature controls.Spraying finishes to 60～80 ℃ of oven dry, and sieving detection is qualified, promptly gets betaine coated product of the present invention.
Beneficial effect: pass betaine coated product provided by the invention and preparation method thereof is compared with prior art and is had the following advantages:
1, pass betaine coated product provided by the invention, at first beet alkali lye and white carbon mixing granulation are obtained beet alkali lye silica particles, pass through hydroxypropyl methylcellulose bag quilt again, because white carbon has the effect that multi-pore structure can reach abundant mixing and absorption beet alkali lye, and white carbon and hydroxypropyl methylcellulose have similar physicochemical property, can improve the coating rate of beet alkali lye greatly.
2, pass betaine coated product provided by the invention; complete function; steady quality; can be widely used in nonruminant and the ruminant; absorptivity height in animal body; be difficult for degraded during especially by ruminant tumor gastric; beet alkali lye is protected in cud; and can absorb the function of bringing into play betaine smoothly in ruminant abomasum, enteron aisle, and experiment shows that pass betaine coated product provided by the invention also has antibacterial anti-inflammatory and the effect that promotes cow producing milk preferably.
3, the preparation method of pass betaine coated product provided by the invention, technological design is reasonable, and is workable, and production cost is low, can realize industrialized production.
The specific embodiment
Further illustrate the present invention below in conjunction with specific embodiment, should understand these embodiment only is used for the present invention and is not used in the restriction scope of the invention, after having read the present invention, those skilled in the art all fall within the application's claims institute restricted portion to the modification of the various equivalent form of values of invention.
Embodiment 1
A kind of pass betaine coated product is prepared by following preparation method:
1. get percentage by weight and be 65% pure beet alkali lye double centner, be heated to 80 ℃, join in the mixer, add 89 kilogram of 20～30 purpose white carbon again, mix, stir into solid, again through the granulator back drying of granulating, obtain beet alkali lye weight percentage and be 162 kilograms of 40% beet alkali lye silica particles, standby;
2. get 5 kilograms of hydroxypropyl methylcelluloses, with the pH value be 7 and concentration be the dissolving of 70% alcohol 95 kilogram, obtain the packaging material double centner, standby;
3. get the beet alkali lye silica particles double centner that 1. step obtains, 2. 75 kilograms the packaging material that obtains with step carries out vaporific spraying coating in wrapping by machine, sieve through 0.84～0.59mm sieve again after preparing coated product, obtain 105 kilograms of pass betaine coated products.
Embodiment 2
A kind of pass betaine coated product is prepared by following preparation method:
1. get percentage by weight and be 68% pure beet alkali lye double centner, be heated to 82 ℃, join in the mixer, add 102 kilogram of 20～30 purpose white carbon again, mix, stir into solid, again through the granulator back drying of granulating, obtain beet alkali lye weight percentage and be 170 kilograms of 40% beet alkali lye silica particles, standby;
2. get 5 kilograms of hydroxypropyl methylcelluloses, with the pH value be 7 and concentration be 75% alcohol 95 kilogram heating for dissolving, obtain the packaging material double centner, standby;
3. get the beet alkali lye silica particles double centner that 1. step obtains, 2. 80 kilograms the packaging material that obtains with step carries out vaporific spraying coating in wrapping by machine, sieve through 0.84～0.59mm sieve again after preparing coated product, obtain 110 kilograms of pass betaine coated products.
Embodiment 3
A kind of pass betaine coated product is prepared by following preparation method:
1. get percentage by weight and be 200 kilograms of 65% pure beet alkali lye, be heated to 82 ℃, join in the mixer, add 178 kilogram of 20～30 purpose white carbon again, mix, stir into solid, again through the granulator back drying of granulating, obtain beet alkali lye weight percentage and be 324 kilograms of 40% beet alkali lye silica particles, standby;
2. get 10 kilograms of hydroxypropyl methylcelluloses, with the pH value be 7 and concentration be 190 kilograms of heating for dissolving of ethanol of 75%, obtain 200 kilograms of packaging materials, standby;
3. get 200 kilograms of the beet alkali lye silica particles that 1. step obtain, 2. 150 kilograms the packaging material that obtains with step carries out vaporific spraying coating in wrapping by machine, sieve through 0.84～0.59mm sieve again after preparing coated product, obtain 210 kilograms of pass betaine coated products.
Embodiment 4
A kind of pass betaine coated product is prepared by following preparation method:
1. get percentage by weight and be 200 kilograms of 70% pure beet alkali lye, be heated to 80 ℃, join in the mixer, add 204 kilogram of 20～30 purpose white carbon again, mix, stir into solid, again through the granulator back drying of granulating, obtain beet alkali lye weight percentage and be 340 kilograms of 40% beet alkali lye silica particles, standby;
2. get 10 kilograms of hydroxypropyl methylcelluloses, with the pH value be 7 and concentration be 200 kilograms of heating for dissolving of ethanol of 70%, obtain 210 kilograms of packaging materials, standby;
3. get 200 kilograms of the beet alkali lye silica particles that 1. step obtain, 2. 150 kilograms the packaging material that obtains with step carries out vaporific spraying coating in wrapping by machine, sieve through 0.84～0.59mm sieve again after preparing coated product, obtain 220 kilograms of pass betaine coated products.
Embodiment 5
A kind of pass betaine coated product is prepared by following preparation method:
1. get percentage by weight and be 70% pure beet alkali lye double centner, be heated to 80 ℃, join in the mixer, add 105 kilogram of 20～30 purpose white carbon again, mix, stir into solid, again through the granulator back drying of granulating, obtain beet alkali lye weight percentage and be 172 kilograms of 40% beet alkali lye silica particles, standby;
2. get 12 kilograms of hydroxypropyl methylcelluloses, with the pH value be 7 and concentration be 98 kilograms of heating for dissolving of ethanol of 70%, obtain 110 kilograms of packaging materials, standby;
3. get the beet alkali lye silica particles double centner that 1. step obtains, 2. 90 kilograms the packaging material that obtains with step carries out vaporific spraying coating in wrapping by machine, sieve through 0.84～0.59mm sieve again after preparing coated product, obtain 115 kilograms of pass betaine coated products.
Embodiment 6 pass betaine coated product functional experiments
With control group? are and what dosage? with pass betaine coated product provided by the invention is experimental group, two density components are set not for to test the I group 6g/ days and to test the II group 12g/ days, feed milk cow, observe the output of milk, fat of milk cow rate, lactoprotein of milk cow, to the milk bovine somatic cells with to the influence of the stealthy mammitis incidence of disease of milk cow.Concrete experimental result as table 1 to shown in the table 4:
Table 1 pass betaine coated product is to the influence (kg/d) of milk production of cow
| Before the test? | Before the test? | |
| Control group | ??32.8 | ??28.39±1.8 |
| Test I group (6g/d) | ??32.8 | ??29.37±2.17 |
| Test II group (12g/d) | ??32.8 | ??28.85±2.6 |
Show by table 1 experimental result, compare that feed with pass betaine coated product 6g/d provided by the invention and 12g/d, milk cow output of milk every day has improved 098kg and 0.46kg respectively with control group.
Table 2 pass betaine coated product is to the influence (%) of fat of milk cow rate and lactoprotein
| Butterfat percnetage | Lactoprotein | |
| Control group | ??4.07±0.8 | ??3.04±0.2 |
| Test I group (6g/d) | ??4.16±0.55 | ??3.05±0.2 |
Show by table 2 experimental result, feed pass betaine coated product 6g/d provided by the invention, fat of milk cow rate and lactoprotein have improved 0.09 and 0.01 percentage point respectively, feed the 12g/d pass betaine coated product, the milk cow's milk protein has improved 0.02 percentage point, but butterfat percnetage slightly reduces (P＞0.05).
Table 3 pass betaine coated product is to the influence of milk cow somatic number
| Somatic number (ten thousand/ml) | |
| Control group | ??47.63±88.46 |
| Test I group (6g/d) | ??21.15±24.82 |
| Test II group (12g/d) | ??28.83±59.44 |
Show by table 3 experimental result, at experimental session, the big rise and fall of control group milk cow somatic number, feed pass betaine coated product 6g/d provided by the invention, somatic number presents slow ascendant trend, feed pass betaine coated product 12g/d provided by the invention, somatic number presents downward trend.
Table 4 pass betaine coated product is to the influence of the stealthy mammitis incidence of disease of milk cow
| The incidence of disease (%) | |
| Control group | ??21.43±3.78B |
| Test I group (6g/d) | ??8.57±3.78A |
| Test II group (12g/d) | ??12.86±4.88A |
Show by table 4 experimental result; after feeding pass betaine coated product 6g/d provided by the invention and 12g/d; the stealthy mammitis incidence of disease of milk cow 60% and 39.99% (P＜0.01) that descended respectively; show that pass betaine coated product can improve the milk cow immunity of organisms; reduce somatic number in the milk, reduce the generation of mastitis for milk cows.
Claims (8)
1. pass betaine coated product, it is characterized in that, it is to be prepared through the hydroxypropyl methylcellulose coating by the beet alkali lye silica particles that contains 38～45% percentage by weight beet alkali lye, the described beet alkali lye silica particles that contains 38～45% percentage by weight beet alkali lye is to be that 65～70% pure beet alkali lye and white carbon mix by percentage by weight, and drying and granulating obtains.
2. pass betaine coated product according to claim 1 is characterized in that, described silica particles is 20～30 orders.
3. pass betaine coated product according to claim 1 is characterized in that, described silica particles and hydroxypropyl methylcellulose packaging material prepare through vaporific spraying coating after mixing.
4. pass betaine coated product according to claim 1 is characterized in that the percentage by weight of moisture is less than 5% in the pass betaine coated product for preparing.
5. method for preparing each described pass betaine coated product of claim 1 to 4 is characterized in that may further comprise the steps:
1. get percentage by weight and be 65～70% pure beet alkali lye portion, be heated to 80～82 ℃, join in the mixer, the white carbon that adds 0.89～1.05 part again, mix, stir into solid, again through the granulator back drying of granulating, obtain beet alkali lye weight percentage and be 38～45% beet alkali lye silica particles, standby;
2. getting 5～6 parts of hydroxypropyl methylcelluloses, is the dissolving of 70～75% ethanol with 95～98 parts of concentration, obtains packaging material, standby;
3. get 1 part of the beet alkali lye silica particles that 1. step obtain, the packaging material that 2. obtains 0.7～0.9 part with step carries out vaporific spraying coating at bag in by machine, and preparing sieves through the 0.84-0.59mm sieve behind the coated product again obtains pass betaine coated product.
6. the preparation method of pass betaine coated product according to claim 5 is characterized in that, the particle diameter of step used white carbon in 1. is 20～30 orders.
7. the preparation method of pass betaine coated product according to claim 5 is characterized in that, the weight percentage of beet alkali lye is 40% in the beet alkali lye silica particles of step described in 1..
8. the preparation method of pass betaine coated product according to claim 5 is characterized in that, step 2. in hydroxypropyl methylcellulose be to be that 7 concentration are that 70% ethanol dissolves with pH value.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010017691A CN101731463A (en) | 2010-01-12 | 2010-01-12 | By-pass betaine coated product and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010017691A CN101731463A (en) | 2010-01-12 | 2010-01-12 | By-pass betaine coated product and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101731463A true CN101731463A (en) | 2010-06-16 |
Family
ID=42455879
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201010017691A Pending CN101731463A (en) | 2010-01-12 | 2010-01-12 | By-pass betaine coated product and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101731463A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103689239A (en) * | 2013-12-23 | 2014-04-02 | 宜兴市天石饲料有限公司 | Preparation method of rumen-through double-layer coated betaine |
| CN113317396A (en) * | 2021-06-17 | 2021-08-31 | 安徽东方天合生物技术有限责任公司 | Preparation method of novel rumen-bypass betaine |
-
2010
- 2010-01-12 CN CN201010017691A patent/CN101731463A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103689239A (en) * | 2013-12-23 | 2014-04-02 | 宜兴市天石饲料有限公司 | Preparation method of rumen-through double-layer coated betaine |
| CN113317396A (en) * | 2021-06-17 | 2021-08-31 | 安徽东方天合生物技术有限责任公司 | Preparation method of novel rumen-bypass betaine |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102578387B (en) | A kind of slowly-releasing compound acidulant for animal and fowl fodder and preparation method thereof and feed | |
| CN101715898B (en) | Acidating agent for newborn piglet feed and preparation method thereof | |
| CN110771742B (en) | Feed additive for reducing methane emission of rumen of cattle and preparation method thereof | |
| CN104397349A (en) | Feeding intestinal tract sustained-release type compound acidifier and preparation method thereof | |
| CN104996737B (en) | A kind of coating preparation method of fodder acidulant | |
| CN103504137A (en) | Enteric coated fodder acidifying agent and preparation method thereof | |
| CN102688220B (en) | Tilmicosin micro-capsule preparation and preparation method thereof | |
| CN104938791A (en) | Fodder baking soda stomach-pass sustained-release agent and preparation method thereof | |
| CA2431250A1 (en) | Composition for regulating animal growth, method of manufacture and use thereof | |
| KR20160045073A (en) | Solid dietary compositions for ruminants and methods of making and using the same | |
| JP2023531098A (en) | Preparation of complex rumen-bypassing polyunsaturated fatty acid powder and its application | |
| CN106721055B (en) | Feeding coated compound acidifier and preparation method thereof | |
| JP5802662B2 (en) | Cashew nut shell oil with improved stability | |
| CN106490345A (en) | A kind of acidulant preparation method and its prepared acidulant | |
| CN108651725A (en) | A kind of palm oil for the Lactation of Dairy Cow phase is coated with rumen bypass lysine | |
| WO2019080155A1 (en) | Conjugate acid salt of n,n-dimethylglycine and organic acid, and composition and application thereof | |
| CN105053557B (en) | A kind of coating preparation method of phosphoric acid micropore acidulant particulate material | |
| CN103239422B (en) | Preparation method of smellless coated enrofloxacin preparation | |
| CN101731463A (en) | By-pass betaine coated product and preparation method thereof | |
| CN109329610A (en) | A kind of feed addictive and preparation method thereof for pig | |
| CN102077905B (en) | Method for producing enteric cysteamine hydrochloride coated granules | |
| CN101715886A (en) | Stabilized cysteamine growth promoting agent used for aquatic feeds and production method thereof | |
| NZ542437A (en) | Composition comprising cysteamine for improving lactation in dairy animals | |
| CN112970942A (en) | Compound acidifier for slow-release feed and production method thereof | |
| CN1592608A (en) | Micropherules containing a pleuromutilin derivative |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C12 | Rejection of a patent application after its publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20100616 |