CN101657402B - 用于在二氯代醇回收期间减少重质副产物形成的方法和设备 - Google Patents

用于在二氯代醇回收期间减少重质副产物形成的方法和设备 Download PDF

Info

Publication number
CN101657402B
CN101657402B CN200880011714.5A CN200880011714A CN101657402B CN 101657402 B CN101657402 B CN 101657402B CN 200880011714 A CN200880011714 A CN 200880011714A CN 101657402 B CN101657402 B CN 101657402B
Authority
CN
China
Prior art keywords
esters
hydrochlorination
liquid
dichlorohydrins
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN200880011714.5A
Other languages
English (en)
Chinese (zh)
Other versions
CN101657402A (zh
Inventor
阿尼尔·梅赫塔
丹·蒂托维迪奥耶奥
约斯·J·隆戈利亚
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Global Technologies LLC
Blue Cube IP LLC
Original Assignee
Dow Global Technologies LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies LLC filed Critical Dow Global Technologies LLC
Publication of CN101657402A publication Critical patent/CN101657402A/zh
Application granted granted Critical
Publication of CN101657402B publication Critical patent/CN101657402B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C29/82—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by azeotropic distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/146—Multiple effect distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38—Steam distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/34—Halogenated alcohols
    • C07C31/42—Polyhydroxylic acyclic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/80—Phthalic acid esters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN200880011714.5A 2007-04-12 2008-04-11 用于在二氯代醇回收期间减少重质副产物形成的方法和设备 Expired - Fee Related CN101657402B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US92310607P 2007-04-12 2007-04-12
US60/923,106 2007-04-12
PCT/US2008/059969 WO2008128005A1 (en) 2007-04-12 2008-04-11 Process and apparatus for reducing heavy byproduct formation during recovery of dichlorohydrins

Publications (2)

Publication Number Publication Date
CN101657402A CN101657402A (zh) 2010-02-24
CN101657402B true CN101657402B (zh) 2014-05-14

Family

ID=39666073

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200880011714.5A Expired - Fee Related CN101657402B (zh) 2007-04-12 2008-04-11 用于在二氯代醇回收期间减少重质副产物形成的方法和设备

Country Status (7)

Country Link
US (1) US8334415B2 (enExample)
EP (1) EP2137122A1 (enExample)
JP (1) JP2010523699A (enExample)
KR (1) KR20100016453A (enExample)
CN (1) CN101657402B (enExample)
TW (1) TW200906777A (enExample)
WO (1) WO2008128005A1 (enExample)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008128014A1 (en) * 2007-04-12 2008-10-23 Dow Global Technologies Inc. Process and apparatus for vapor phase purification during hydrochlorination of multi-hydroxylated aliphatic hydrocarbon compounds
WO2008128005A1 (en) 2007-04-12 2008-10-23 Dow Global Technologies Inc. Process and apparatus for reducing heavy byproduct formation during recovery of dichlorohydrins
TW200906776A (en) * 2007-04-12 2009-02-16 Dow Global Technologies Inc Conversion of a multihydroxylated-aliphatic hydrocarbon or ester thereof to a chlorohydrin
KR101067494B1 (ko) * 2008-12-31 2011-09-27 삼성정밀화학 주식회사 디클로로프로판올의 선택도가 향상된, 글리세롤을 사용하는디클로로프로판올의 제조방법
CN102471196A (zh) 2009-07-03 2012-05-23 阿克佐诺贝尔化学国际公司 制备二氯丙醇的方法
WO2018175481A1 (en) * 2017-03-20 2018-09-27 Lanzatech, Inc. A process and system for product recovery and cell recycle
CN108059586B (zh) * 2017-12-12 2021-08-17 浙江镇洋发展股份有限公司 一种甘油氯化制备二氯丙醇的方法
CN110652946B (zh) * 2019-09-24 2021-11-09 安徽神剑新材料股份有限公司 一种聚酯树脂生产过程中顶温控制系统及方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1845888A (zh) * 2003-09-01 2006-10-11 化学和冶金生产联合体股份公司 从甘油中制备二氯丙醇的方法
CN1882522A (zh) * 2003-11-20 2006-12-20 索尔维公司 从甘油生产二氯丙醇的方法,甘油最终来自生物柴油生产中动物脂肪的转化
EP1762556A1 (en) * 2005-05-20 2007-03-14 SOLVAY (Société Anonyme) Process for producing dichloropropanol from glycerol

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2144612A (en) * 1936-09-10 1939-01-24 Dow Chemical Co Preparation of glycerol dichlorohydrin
EP0162556B1 (en) * 1984-04-13 1991-11-06 FISONS plc Novels forms and formulations of nedocromil sodium
JPS60258171A (ja) * 1984-06-04 1985-12-20 Showa Denko Kk エピクロルヒドリンの製造方法
JP4080553B2 (ja) * 1994-12-01 2008-04-23 三菱化学株式会社 ブチルアルデヒドの製造方法
EP0931054B2 (de) * 1996-09-10 2012-07-11 Basf Se Verfahren zur abtrennung von 2-aminomethylcyclopentylamin aus einer mischung enthaltend hexamethylendiamin und 2-aminomethylcyclopentylamin
US6171449B1 (en) * 1998-06-19 2001-01-09 Washington Group International, Inc. Cascade reboiling of ethylbenzene/styrene columns
DE10056841A1 (de) 2000-11-16 2002-05-23 Basf Ag Verfahren und Vorrichtung zur destillativen Gewinnung von 1,3-Reinbutadien aus 1,3-Rohbutadien
JP4091766B2 (ja) * 2001-12-27 2008-05-28 三菱レイヨン株式会社 メタクロレインの製造方法
US20040104108A1 (en) * 2002-12-03 2004-06-03 Mason Robert Michael High capacity purification of thermally unstable compounds
EA200800129A1 (ru) 2003-11-20 2008-04-28 Солвей (Сосьете Аноним) Псевдоазеотропная композиция, содержащая дихлорпропанол, и способ ее получения
JP2005336122A (ja) * 2004-05-28 2005-12-08 Mitsubishi Chemicals Corp （メタ）アクリル酸又は（メタ）アクリル酸エステルの製造方法
CN102516205B (zh) 2004-07-21 2016-05-04 兰科知识产权有限责任公司 多羟基化脂族烃或其酯向氯醇的转化
US7381971B2 (en) * 2004-07-28 2008-06-03 Omniprobe, Inc. Method and apparatus for in-situ probe tip replacement inside a charged particle beam microscope
CN100509726C (zh) 2007-01-26 2009-07-08 江苏工业学院 一种从甘油制备二氯丙醇的方法
WO2008128005A1 (en) 2007-04-12 2008-10-23 Dow Global Technologies Inc. Process and apparatus for reducing heavy byproduct formation during recovery of dichlorohydrins

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1845888A (zh) * 2003-09-01 2006-10-11 化学和冶金生产联合体股份公司 从甘油中制备二氯丙醇的方法
CN1882522A (zh) * 2003-11-20 2006-12-20 索尔维公司 从甘油生产二氯丙醇的方法,甘油最终来自生物柴油生产中动物脂肪的转化
EP1762556A1 (en) * 2005-05-20 2007-03-14 SOLVAY (Société Anonyme) Process for producing dichloropropanol from glycerol

Also Published As

Publication number Publication date
KR20100016453A (ko) 2010-02-12
CN101657402A (zh) 2010-02-24
EP2137122A1 (en) 2009-12-30
TW200906777A (en) 2009-02-16
US20100137621A1 (en) 2010-06-03
WO2008128005A1 (en) 2008-10-23
US8334415B2 (en) 2012-12-18
JP2010523699A (ja) 2010-07-15

Similar Documents

Publication Publication Date Title
CN101657403B (zh) 用于回收二氯代醇的多级方法和设备
CN101998945B (zh) 用于有效回收二氯代醇的方法和设备
CN101657402B (zh) 用于在二氯代醇回收期间减少重质副产物形成的方法和设备
US8629305B2 (en) Process and apparatus for azeotropic recovery of dichlorohydrins
US8926916B2 (en) Process and apparatus for recovery of dichlorohydrins via codistillation
US8586802B2 (en) Multi-stage process and apparatus for recovering dichlorohydrins

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C41 Transfer of patent application or patent right or utility model
C56 Change in the name or address of the patentee
CP01 Change in the name or title of a patent holder

Address after: American Michigan

Patentee after: Dow Global Technologies Llc

Address before: American Michigan

Patentee before: Dow Global Technologies Inc.

TR01 Transfer of patent right

Effective date of registration: 20151221

Address after: American Michigan

Patentee after: BLUE CUBE IP LLC

Address before: American Michigan

Patentee before: Dow Global Technologies Llc

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140514

Termination date: 20170411

CF01 Termination of patent right due to non-payment of annual fee