CN101653149B - Oligosaccharides plant induced-resistance agent effervescent tablet and preparation method thereof - Google Patents
Oligosaccharides plant induced-resistance agent effervescent tablet and preparation method thereof Download PDFInfo
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- CN101653149B CN101653149B CN2009101898590A CN200910189859A CN101653149B CN 101653149 B CN101653149 B CN 101653149B CN 2009101898590 A CN2009101898590 A CN 2009101898590A CN 200910189859 A CN200910189859 A CN 200910189859A CN 101653149 B CN101653149 B CN 101653149B
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- resistance agent
- oligosaccharides
- effervescent tablet
- plant induced
- acid
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Abstract
The invention discloses an oligosaccharides induced-resistance agent effervescent tablet and a preparation method thereof. The oligosaccharides induced-resistance agent effervescent tablet comprises the following raw materials by weight percent: 0.5-40.0 percent of plant induced-resistance agent raw powders, 18.0-30.0 percent of solid organic acid, 30.0-40.0 percent of carbonate, 10.0-15.0 percent of a drier, 1.0-1.5 percent of a glidant and 1.0-13 percent of a promoter. Compared with the prior art, the invention has the advantages of easy dissolution in water, convenient transportation and storage, no agglomeration due to moisture and convenient use.
Description
Technical field
The present invention relates to agricultural biological technical field, particularly a kind of oligosaccharides plant induced-resistance agent effervescent tablet and preparation method thereof.
Background technology
The mutual identification of plant and pathogen depends on the interaction between the two cell surface molecule.During pathogen invasion host plant, through the interaction between the cell surface molecule.During pathogen invasion host plant,, make series reaction takes place in the plant corpus, produce new material in the inducing plant body through the effect between the cell surface molecule.By this molecular recognition mechanism; When no pathogen exists, plant cell wall receive some material as: during the stimulation of mineral salt, organic molecule, large biological molecule and fungal cell wall, in the plant corpus series reaction can take place; Through this series reaction; Produce protective plant protecting agent through this a series of reaction induced plant, make plant obtain disease resistance, the material that these ability inducing plants produce protective plant protecting agent just is called as inducer.
Plant induced resistance agent is the novel agrochemical type of forming with the plant disease-resistant inducible factor, is with a wide range of applications, especially to the unmanageable disease of general chemical pesticide; Like virus disease, fusarium wilt and verticillium wilt etc. good control efficiency is arranged, the plant induced resistance agent of country's registration at present is to be main inducing anti-disease composition with amino-oligosaccharide, but the product of registration all is an aqua product at present; This formulation exists structure and the stability problem in the storage process; Influence its popularization and application, develop solid amino-oligosaccharide product is main direction for this reason, but because the oligosaccharide solid has strong hygroscopicity; Powder product lumps easily, influences dissolubility.
Effervescent tablet is a kind of effervescence medicament form that is grouped into by two kinds of one-tenth of soda acid; In medicine, veterinary drug and plurality kinds of health care article, be applied; Has the dissolving of in water, being easy to; Transportation, storage and multiple advantage such as easy to use have application report in fields such as bactericide, weed killer herbicide, biological insecticides in recent years, but do not appear in the newspapers with the effervescent tablet of oligosaccharides plant induced-resistance agent as its main component.
Summary of the invention
In order to solve the weak point that exists in the above-mentioned prior art, the purpose of this invention is to provide a kind of the have dissolving of in water, being easy to, transportation, storage and oligosaccharides plant induced-resistance agent effervescent tablet easy to use.
Another object of the present invention is to provide the preparation method of above-mentioned oligosaccharides plant induced-resistance agent effervescent tablet.
The object of the invention is realized through following technical proposals: a kind of oligosaccharides plant induced-resistance agent effervescent tablet; It mainly is made up of the former powder of plant induced resistance agent, solid organic acid, carbonate, desiccant, glidant, auxiliary agent; Wherein, The former powder of described plant induced resistance agent is made up of oligosaccharides (acid) series products, mainly comprises: amino-oligosaccharide, oligomerization alginic acid, ligoglucoside and peptone;
The composition and the mass percent of the primary raw material of oligosaccharides plant induced-resistance agent effervescent tablet of the present invention are:
The former powder of plant induced resistance agent: 0.5-40.0%
Solid organic acid: 18.0.-30.0%
Carbonate: 30.0-40.0%
Desiccant: 10.0-15.0%
Glidant: 1.0-1.5%
Auxiliary agent: 1.0-13.0%
Above-described solid organic acid is: any one in citric acid, tartaric acid, the amino acid or two or more mixtures.
Above-described carbonate is: any one in sodium carbonate, sodium bicarbonate, the potash or two or more mixtures.
Described desiccant is: talcum powder, any one in diatomite, starch, aluminium salt, bentonite, the calcium oxide or two or more mixtures.
Described glidant is any or both mixture in dolomol, the calcium stearate.
Described auxiliary agent is: zinc sulphate, boric acid, virazole, Radix Isatidis, soap, any one or two or more mixtures in fulvic acid, salicylic acid, sodium salicylate, the plant growth regulator.
A kind of preparation method of oligosaccharides plant induced-resistance agent effervescent tablet comprises following processing step and process: with said solid organic acid, carbonate and desiccant are dry respectively by above-mentioned quality proportioning; Be crushed to the 50-100 order; Mix, add alcohols furnishing pasty state, alcohol is removed in vacuum drying; Cross the 20-60 mesh sieve, for expecting 1;
And then will expect 1 with mix by former powder auxiliary agent of the plant induced resistance agent of above-mentioned quality proportioning and glidant, compressing tablet gets final product.
The alcohols of the adding among the said preparation method is ethanol or propyl alcohol.
The present invention compared with prior art has following advantage: in water, be easy to dissolving, be convenient to transportation, store, can not lump because of humidity, use very convenient simultaneously.
Embodiment
Below in conjunction with embodiment the present invention is done to specify further, but embodiment is not limited to this.
Embodiment 1
In the present embodiment, the former powder of plant induced resistance agent adopts amino-oligosacchride, and solid organic acid adopts citric acid, and carbonate adopts sodium carbonate, and desiccant adopts calcium oxide and starch, and glidant adopts dolomol, and auxiliary agent adopts boric acid.
1 kilogram of this kind oligosaccharides plant induced-resistance agent effervescent tablet comprises: 5 gram amino-oligosaccharide powder, 400 gram sodium carbonate, 300 gram citric acids, 100 gram calcium oxide, 50 gram starch, 15 gram dolomols, boric acid 100 grams; With citric acid, sodium carbonate, calcium oxide and starch difference drying and crushing, cross the 50-100 mesh sieve, then with sodium carbonate, citric acid, calcium oxide, starch mixing; Add 80 milliliters of absolute ethyl alcohols, reconcile into pasty state, vacuum is removed alcohol; Add component at last respectively: the amino-oligosaccharide powder; Boric acid and dolomol mix the back compressing tablet, promptly obtain containing the effervescent tablet of 0.5% oligosaccharides plant induced-resistance agent.
Embodiment 2
In the present embodiment, the former powder of plant induced resistance agent adopts amino-oligosacchride, and solid organic acid adopts citric acid, and carbonate adopts sodium carbonate, and desiccant adopts calcium oxide and starch, and glidant adopts dolomol, and auxiliary agent adopts boric acid.
1 kilogram of this kind oligosaccharides plant induced-resistance agent effervescent tablet comprises: 400 gram amino-oligosaccharide powder, 300 gram sodium carbonate, 180 gram citric acids, 100 gram starch; 10 gram dolomols, boric acid 10 grams are with citric acid, sodium carbonate, calcium oxide and starch difference drying and crushing; Cross the 50-100 mesh sieve,, add 80 milliliters of absolute ethyl alcohols sodium carbonate, citric acid, starch mixing; Reconcile into pasty state, vacuum is removed alcohol, is adding the amino-oligosaccharide powder respectively; Boric acid and dolomol mix the back compressing tablet, promptly obtain containing the effervescent tablet of 40% oligosaccharides plant induced-resistance agent.
Embodiment 3
In the present embodiment, the former powder of plant induced resistance agent adopts amino-oligosacchride, and solid organic acid adopts citric acid, and carbonate adopts sodium carbonate, and desiccant adopts calcium oxide and starch, and glidant adopts dolomol.
1 kilogram of this kind oligosaccharides plant induced-resistance agent effervescent tablet comprises: 300 gram amino-oligosaccharide powder, 300 gram sodium carbonate, 200 gram citric acids, 100 gram calcium oxide; 50 gram starch, 10 gram dolomols, 40 gram peptones are with citric acid, sodium carbonate, calcium oxide and starch difference drying and crushing; Cross the 50-100 mesh sieve,, add 80 milliliters of absolute ethyl alcohols sodium carbonate, citric acid, calcium oxide, starch mixing; Reconcile into pasty state, vacuum is removed alcohol, is adding the amino-oligosaccharide powder respectively; Peptone and dolomol mix the back compressing tablet, promptly obtain containing the effervescent tablet of 30% oligosaccharides plant induced-resistance agent.
Embodiment 4
In the present embodiment, the former powder of plant induced resistance agent adopts amino-oligosacchride, and solid organic acid adopts tartaric acid, and carbonate adopts sodium bicarbonate, and desiccant adopts starch, and glidant adopts dolomol.
1 kilogram of this kind oligosaccharides plant induced-resistance agent effervescent tablet comprises: 100 gram amino-oligosaccharide powder, 400 gram sodium bicarbonates, 300 gram tartaric acid, 100 gram starch, 50 gram peptones, 15 gram dolomols, 35 gram sodium salicylates.With tartaric acid, sodium bicarbonate, starch difference drying and crushing, cross the 50-100 mesh sieve, with sodium bicarbonate, tartaric acid, starch mixing; Add 100-150 milliliter absolute ethyl alcohol, reconcile into pasty state, vacuum is removed alcohol; Pulverized 60 mesh sieves; Add amino-oligosaccharide powder, peptone and dolomol respectively, the mixing compressing tablet promptly obtains containing the effervescent tablet of 10% oligosaccharides plant induced-resistance agent.
Embodiment 5
1 kilogram of this kind oligosaccharides plant induced-resistance agent effervescent tablet comprises: 50 gram amino-oligosaccharide powder, 30 gram oligomerization alginic acid powder, 20 gram oligomerization powdered glucoses, 350 gram sodium carbonate, 350 gram citric acids, 50 gram calcium oxide, 50 gram starch, 50 gram peptones, 35 gram fulvic acids; 15 gram dolomols with mentioned component difference drying and crushing, are crossed the 50-100 mesh sieve; With sodium carbonate, citric acid, calcium oxide, starch mixing, add 100-150 milliliter absolute ethyl alcohol, reconcile into pasty state; Vacuum is removed alcohol; Pulverize 60 orders and sieve, add amino-oligosaccharide powder, oligomerization alginic acid powder, ligoglucoside powder, peptone and dolomol respectively, the mixing compressing tablet; Be 5% amino-oligosaccharide effervescent tablet, promptly obtain containing the effervescent tablet of 5% oligosaccharides plant induced-resistance agent.
The above is merely the preferred embodiment of invention, not in order to restriction the present invention, all any modifications of within spirit of the present invention and principle, being done, is equal to and replaces and improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. oligosaccharides plant induced-resistance agent effervescent tablet; It mainly is made up of the former powder of plant induced resistance agent, solid organic acid, carbonate, desiccant, glidant, auxiliary agent; Wherein, The former powder of described plant induced resistance agent is made up of the oligosaccharides series products, mainly comprises: amino-oligosaccharide, oligomerization alginic acid, ligoglucoside and peptone; The composition and the mass percent of the primary raw material of described oligosaccharides plant induced-resistance agent effervescent tablet are:
The former powder of plant induced resistance agent: 0.5-40.0%
Solid organic acid: 18.0.-30.0%
Carbonate: 30.0-40.0%
Desiccant: 10.0-15.0%
Glidant: 1.0-1.5%
Auxiliary agent: 1.0-13.0%
It is characterized in that: described solid organic acid is: any one in citric acid, tartaric acid, the amino acid or two or more mixtures;
Described glidant is any or both mixture in dolomol, the calcium stearate;
Described auxiliary agent is: zinc sulphate, boric acid, virazole, Radix Isatidis, soap, any one or two or more mixtures in fulvic acid, salicylic acid, sodium salicylate, the plant growth regulator.
2. oligosaccharides plant induced-resistance agent effervescent tablet according to claim 1 is characterized in that: described carbonate is: any one in sodium carbonate, sodium bicarbonate, the potash or two or more mixtures.
3. oligosaccharides plant induced-resistance agent effervescent tablet according to claim 1 is characterized in that: described desiccant is: talcum powder, any one in diatomite, starch, aluminium salt, bentonite, the calcium oxide or two or more mixtures.
4. the preparation method of an oligosaccharides plant induced-resistance agent effervescent tablet is characterized in that, comprises following processing step and process: press the said quality proportioning of claim 1 with described solid organic acid; Carbonate and desiccant are dry respectively, are crushed to the 50-100 order, mix; Add alcohols furnishing pasty state; Alcohol is removed in vacuum drying, crosses the 20-60 mesh sieve, for expecting 1;
And then will expect 1 with mix by the former powder of plant induced resistance agent, auxiliary agent and the glidant of the said quality proportioning of claim 1, compressing tablet gets final product.
5. the preparation method of oligosaccharides plant induced-resistance agent effervescent tablet as claimed in claim 4, it is characterized in that: the alcohols of the adding among the said preparation method is ethanol or propyl alcohol.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2009101898590A CN101653149B (en) | 2009-09-02 | 2009-09-02 | Oligosaccharides plant induced-resistance agent effervescent tablet and preparation method thereof |
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| CN2009101898590A CN101653149B (en) | 2009-09-02 | 2009-09-02 | Oligosaccharides plant induced-resistance agent effervescent tablet and preparation method thereof |
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| CN101653149B true CN101653149B (en) | 2012-07-04 |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102273486A (en) * | 2011-06-28 | 2011-12-14 | 深圳诺普信农化股份有限公司 | Amino-oligosaccharin containing composition and application thereof |
| CN103483057A (en) * | 2013-08-30 | 2014-01-01 | 南京农业大学 | Plant growth-promoting and resistance-inducing agent, and preparation and application method thereof |
| CN104920472B (en) * | 2015-06-08 | 2017-09-19 | 中国农业科学院油料作物研究所 | A kind of crop physiological inducer and preparation method thereof |
| CN111449062B (en) * | 2020-05-12 | 2022-08-19 | 侨昌现代农业有限公司 | Production and preparation process of pesticide effervescent |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1903040A (en) * | 2006-08-04 | 2007-01-31 | 广东省农业科学院植物保护研究所 | Fruits protection effervescence tablets, prepn. method and use thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1903040A (en) * | 2006-08-04 | 2007-01-31 | 广东省农业科学院植物保护研究所 | Fruits protection effervescence tablets, prepn. method and use thereof |
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