CN1903040A - Fruits protection effervescence tablets, prepn. method and use thereof - Google Patents

Fruits protection effervescence tablets, prepn. method and use thereof Download PDF

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Publication number
CN1903040A
CN1903040A CN 200610036949 CN200610036949A CN1903040A CN 1903040 A CN1903040 A CN 1903040A CN 200610036949 CN200610036949 CN 200610036949 CN 200610036949 A CN200610036949 A CN 200610036949A CN 1903040 A CN1903040 A CN 1903040A
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China
Prior art keywords
effervescence tablets
fruits
protection
surfactant
fruits protection
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CN 200610036949
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Chinese (zh)
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CN100502660C (en
Inventor
冯莉
许平辉
张宝鑫
李敦松
黄少华
冯新霞
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Plant Protection Research Institute Guangdong Academy of Agricultural Sciences
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Plant Protection Research Institute Guangdong Academy of Agricultural Sciences
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Priority to CNB2006100369492A priority Critical patent/CN100502660C/en
Publication of CN1903040A publication Critical patent/CN1903040A/en
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Publication of CN100502660C publication Critical patent/CN100502660C/en
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Abstract

A plant growth regulator 'Baoguo effervescent tablet' for regulating the growth and development, promoting the fruit bearing, improving fruit quality and increasing the yield of fruit tree is prepared from gibberellins, forchlorfenuron, potassium dihydrogen phosphate, boric acid and zinc sulfate through proportional mixing, adding citric acid, sodium dicarbonate, adhesive and surfactant, pulverizing, granulating and die pressing.

Description

A kind of fruits protection effervescence tablets and its production and application
Technical field
The invention belongs to agricultural biological technical field, particularly a kind of fruits protection effervescence tablets of forming by gibberellin of plant growth regulator, CPPU and multiple mineral nutrient element and its production and application.
Background technology
The fruit of granulated sugar tangerine is seeds abortion mostly, therefore causes the fruit percentage of fertile fruit low, and young fruit comes off seriously; Seedless wampee equally also is that abscisic acid content raises because the solid endogenous hormones that causes of no seed is out of proportion, and percentage of fertile fruit is extremely low under the self-sow state.Therefore, two planting fruit-trees must use fruit preservative, just can reach the purpose that promotes setting, improves output.
Granulated sugar tangerine and seedless wampee do not have fruit preservative special at present, though also there is the single gibberellin of plant growth regulator of use to use in the production as fruit preservative, but having to impel, gibberellin takes out the prosperous length of the tip, elongate fruit ear and to shortcomings such as fruit quality improvement effect are not obvious, and gibberellin is when using as commodity, its formulation is generally 85% former powder or 4% missible oil at present, its Central Plains powder is water insoluble, will be before using earlier with after a small amount of alcohol dissolving, thin up is to required concentration again, and the aqueous solution can not be put for a long time, therefore using to the peasant makes troubles, and missible oil contains a large amount of organic solvents, cost height not only, but also can cause environmental pollution, therefore press for the environment amenable environment friendly agricultural preparation of exploitation.
Effervescent tablet is a kind ofly to be grouped into effervescent agent by two kinds of one-tenth of soda acid, in medicine, veterinary drug and plurality kinds of health care product, be applied, has easily dissolving in water, transportation, storage and multiple advantage such as easy to use, at pesticide fields such as bactericide, weed killer herbicide, biological insecticides application report is arranged in recent years, but the compound fruits protection effervescence tablets of forming with gibberellin, CPPU and various plants nutritive element does not appear in the newspapers.
Summary of the invention
In order to solve above-mentioned the deficiencies in the prior art part, primary and foremost purpose of the present invention is to provide a kind of can improve percentage of fertile fruit, improve fruit quality and easy to use and formulation environmental protection---fruits protection effervescence tablets, this effervescent tablet has and promotes setting, improves advantages such as fruit quality and volume increase, also have simultaneously efficient, low toxicity, environmental protection, easy to use, be convenient to characteristics such as accumulating.
Another object of the present invention is to provide the preparation method of above-mentioned fruits protection effervescence tablets.
A further object of the present invention is to provide the application of above-mentioned fruits protection effervescence tablets.
Purpose of the present invention is achieved through the following technical solutions: a kind of fruits protection effervescence tablets, this effervescent tablet is after mixing in proportion with gibberellin of plant growth regulator, CPPU and multiple mineral nutrient element potassium dihydrogen phosphate, boric acid, zinc sulphate, with effervescent agent citric acid, effervescent agent sodium bicarbonate and adhesive, surfactant etc., make effervescent tablet through operations such as pulverizing, granulation, compressing tablets, described effervescent tablet is become to be grouped into by following by mass percentage:
Active ingredient gibberellin 5%~20%, CPPU 2.5%~10%, potassium dihydrogen phosphate 5%~20%, boric acid 5%~10%, zinc sulphate 5%~10%, effervescent agent citric acid 15%~35%, effervescent agent sodium bicarbonate 10%~30%, adhesive dextrin 5~10%, surfactant 1%~5%.
Described surfactant is lauryl sodium sulfate or carboxymethyl cellulose.
A kind of preparation method of fruits protection effervescence tablets, comprise following processing step and process: press above-mentioned quality proportioning with active ingredient gibberellin, CPPU, potassium dihydrogen phosphate, boric acid and zinc sulphate, mix behind the crushing screening respectively, add through difference crushing screening effervescent agent citric acid and sodium bicarbonate, adhesive dextrin again, reach surfactant, abundant mixing, granulation, dry back compressing tablet promptly get fruits protection effervescence tablets.
Described sieving to crossing 80~120 mesh sieves.Described baking temperature is 50~70 ℃.
Above-mentioned fruits protection effervescence tablets is used on the solid fruit trees of no seed such as granulated sugar tangerine, seedless wampee or currant, all can improve percentage of fertile fruit, reaches the fruit retention purpose.This fruits protection effervescence tablets is specifically designed to the fruit retention of the solid fruit trees of no seed such as granulated sugar tangerine or seedless wampee, can improve granulated sugar tangerine and seedless wampee percentage of fertile fruit, improves fruit quality, and easy to use and environmental protection.
Every heavy 4~5g of this effervescent tablet gets a slice and puts into 20~25 kg of water during use, can be dissolved as uniform liquid rapidly, promptly can be used for granulated sugar tangerine or seedless wampee full-bloom stage, thanks florescence and young fruit period foliar spray fruit retention.
The present invention compared with prior art, have following advantage and beneficial effect: formulation advanced person of the present invention is novel, scientific formulation is tight, easy to use, particularly for plant growth regulator, usage amount is few, can reach coordinate plant growth and grow, promote setting, improve quality, improve the purpose of output, and safety and environmental protection.Fruits protection effervescence tablets of the present invention can be specifically designed to the fruit retention of granulated sugar tangerine or seedless wampee fruit tree, can improve granulated sugar tangerine and seedless wampee percentage of fertile fruit, improves fruit quality.
Embodiment
Below in conjunction with embodiment the present invention is described in further detail, but embodiment is not limited in this.
Embodiment one
Fruits protection effervescence tablets of the present invention is grouped into by following one-tenth:
Gibberellin 200g (5%)
CPPU 400g (10%)
Potassium dihydrogen phosphate 200g (5%)
Boric acid 200g (5%)
Zinc sulphate 200g (5%)
Citric acid 1300 (33%)
Sodium bicarbonate 1200g (30%)
Lauryl sodium sulfate 100g (3%)
With above-mentioned each raw material pulverizing, sieve after (cross 80~120 mesh sieves), by after the above-mentioned formula ratio weighing, mix, add adhesive dextrin 200g (5%), mix, granulate in (14~16 order), dry (50~70 ℃ of dryings make water content≤2.5%) back compressing tablet, promptly get fruits protection effervescence tablets, make 1000 altogether, the every heavy 4g of sheet, getting a slice during use is dissolved in the 20Kg water, be dissolved as uniform liquid rapidly, at the seedless wampee full-bloom stage, thank and spend spend spray in 2 weeks of back blade faces and flower fringes latter stage, can significantly promote setting with thanking, do not compare with spraying fruits protection effervescence tablets, percentage of fertile fruit has improved 42.2%.
Embodiment two
Fruits protection effervescence tablets of the present invention is grouped into by following one-tenth:
Gibberellin 800g (18%)
CPPU 100g (2%)
Potassium dihydrogen phosphate 800g (18%)
Boric acid 400g (9%)
Zinc sulphate 400g (9%)
Citric acid 700g (16%)
Sodium bicarbonate 600g (13%)
Lauryl sodium sulfate 200g (4%)
With above-mentioned each raw material pulverizing, (cross 80~120 mesh sieves) after sieving, by after the above-mentioned formula ratio weighing, mix, add adhesive dextrin 450g (10%), granulate in (14~16 order), dry (50~70 ℃ of dryings make water content≤2.5%) back compressing tablet promptly gets fruits protection effervescence tablets, make 1000 altogether, the every heavy 4.5g of sheet gets a slice and is dissolved in the 20Kg water during use, be dissolved as uniform liquid rapidly, thank in seedless wampee and to spend latter stage and thanking and spend 2 week of back spraying blade face and fruit ears, can significantly promote setting, not compare that percentage of fertile fruit has improved 94.0% with spraying fruits protection effervescence tablets.
Embodiment three
Fruits protection effervescence tablets of the present invention is grouped into by following one-tenth:
Gibberellin 600g (12%)
CPPU 350g (7%)
Potassium dihydrogen phosphate 500g (10%)
Boric acid 350g (7%)
Zinc sulphate 350g (7%)
Citric acid 1200g (24%)
Sodium bicarbonate 1200g (24%)
Carboxymethyl cellulose 50g (1%)
With above-mentioned each raw material pulverizing, (cross 80~120 mesh sieves) after sieving, by after the above-mentioned formula ratio weighing, mix, add adhesive dextrin 400g (8%), granulate in (14~16 order), dry (50~70 ℃ of dryings make water content≤2.5%) back compressing tablet promptly gets fruits protection effervescence tablets, makes 1000 altogether, the every heavy 5g of sheet, get a slice during use and be dissolved in the 20Kg water, thank the granulated sugar tangerine and spend 2/3 and thank and spend back 2 week spraying blade face and fruits, can significantly promote setting, do not compare with spraying fruits protection effervescence tablets, percentage of fertile fruit has improved 87.6%.
As mentioned above, can realize the present invention preferably.

Claims (6)

1, a kind of fruits protection effervescence tablets, this effervescent tablet is after mixing by the quality proportioning with gibberellin of plant growth regulator, CPPU and mineral nutrient element potassium dihydrogen phosphate, boric acid, zinc sulphate, with effervescent agent citric acid and sodium bicarbonate and adhesive, surfactant, make effervescent tablet through pulverizing, granulation, compressing tablet, it is characterized in that described effervescent tablet is become to be grouped into by following by mass percentage:
Active ingredient gibberellin 5%~20%, CPPU 2.5%~10%, potassium dihydrogen phosphate 5%~20%, boric acid 5%~10%, zinc sulphate 5%~10%, effervescent agent citric acid 15%~35%, effervescent agent sodium bicarbonate 10%~30%, adhesive dextrin 5~10%, surfactant 1%~5%.
2, a kind of fruits protection effervescence tablets according to claim 1 is characterized in that: described surfactant is lauryl sodium sulfate or carboxymethyl cellulose.
3, the preparation method of the described a kind of fruits protection effervescence tablets of claim 1, it is characterized in that comprising following processing step and process: press above-mentioned quality proportioning with active ingredient gibberellin, CPPU, potassium dihydrogen phosphate, boric acid and zinc sulphate, mix behind the crushing screening respectively, add again through the effervescent agent citric acid of crushing screening respectively and sodium bicarbonate, adhesive dextrin, and surfactant, fully behind the mixing, granulation, dry back compressing tablet promptly get fruits protection effervescence tablets; Described surfactant is lauryl sodium sulfate or carboxymethyl cellulose.
4, the preparation method of a kind of fruits protection effervescence tablets according to claim 3 is characterized in that: described sieving to crossing 80~120 mesh sieves.
5, the preparation method of a kind of fruits protection effervescence tablets according to claim 3 is characterized in that: described baking temperature is 50~70 ℃.
6, the described fruits protection effervescence tablets of claim 1 does not have application in the solid fruit tree of seed granulated sugar tangerine, seedless wampee or currant.
CNB2006100369492A 2006-08-04 2006-08-04 Fruits protection effervescence tablets, preparation method and use thereof Expired - Fee Related CN100502660C (en)

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Application Number Priority Date Filing Date Title
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CN1903040A true CN1903040A (en) 2007-01-31
CN100502660C CN100502660C (en) 2009-06-24

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102258058A (en) * 2010-08-03 2011-11-30 重庆大学 Preparation method of citrus maturing regulator
CN102283248A (en) * 2011-08-09 2011-12-21 孔祥军 Grape bunch shaft drawing softening agent
CN102450255A (en) * 2011-11-08 2012-05-16 安阳市全丰农药化工有限责任公司 Forchlorfenuron effervescent granules/or effervescent tablets and preparation method thereof
CN101653149B (en) * 2009-09-02 2012-07-04 深圳市沃科生物工程有限公司 Oligosaccharides plant induced-resistance agent effervescent tablet and preparation method thereof
CN103250580A (en) * 2013-05-06 2013-08-21 丁在喜 Method for softening hard pomegranate seeds
CN107267322A (en) * 2017-07-09 2017-10-20 深圳市美益洁生物科技有限公司 Degerming cleaning effervescent tablet of feeding bottle biology enzyme and its preparation method and application
CN111213512A (en) * 2020-01-13 2020-06-02 广东省农业科学院果树研究所 Planting method for improving total flavone content and antioxidant activity of wampee fruits
CN113575922A (en) * 2021-08-06 2021-11-02 四川轻化工大学 Phosphate additive and preparation method thereof

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1555690A (en) * 2003-12-30 2004-12-22 上海交通大学 European Asia variety grape seedless treatment method
CN1964624B (en) * 2004-05-24 2010-10-27 瓦伦特生物科学公司 Stable and water-soluble plant growth regulator liquid compositions and methods for use of same

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101653149B (en) * 2009-09-02 2012-07-04 深圳市沃科生物工程有限公司 Oligosaccharides plant induced-resistance agent effervescent tablet and preparation method thereof
CN102258058A (en) * 2010-08-03 2011-11-30 重庆大学 Preparation method of citrus maturing regulator
CN102283248A (en) * 2011-08-09 2011-12-21 孔祥军 Grape bunch shaft drawing softening agent
CN102450255A (en) * 2011-11-08 2012-05-16 安阳市全丰农药化工有限责任公司 Forchlorfenuron effervescent granules/or effervescent tablets and preparation method thereof
CN103250580A (en) * 2013-05-06 2013-08-21 丁在喜 Method for softening hard pomegranate seeds
CN103250580B (en) * 2013-05-06 2015-04-22 丁在喜 Method for softening hard pomegranate seeds
CN107267322A (en) * 2017-07-09 2017-10-20 深圳市美益洁生物科技有限公司 Degerming cleaning effervescent tablet of feeding bottle biology enzyme and its preparation method and application
CN111213512A (en) * 2020-01-13 2020-06-02 广东省农业科学院果树研究所 Planting method for improving total flavone content and antioxidant activity of wampee fruits
CN111213512B (en) * 2020-01-13 2021-10-12 广东省农业科学院果树研究所 Planting method for improving total flavone content and antioxidant activity of wampee fruits
CN113575922A (en) * 2021-08-06 2021-11-02 四川轻化工大学 Phosphate additive and preparation method thereof

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EE01 Entry into force of recordation of patent licensing contract

Assignee: Guangdong Dafeng Plant Protection Technology Co., Ltd.

Assignor: Inst. of Plant Protection, Guangdong Prov. Academy of Agricultural Sciences

Contract record no.: 2011440000816

Denomination of invention: Fruits protection effervescence tablets, prepn. method and use thereof

Granted publication date: 20090624

License type: Exclusive License

Open date: 20070131

Record date: 20110805

C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20090624

Termination date: 20110804