CN101652463B - 利用超临界流体从羊毛中提取内部脂质的方法 - Google Patents
利用超临界流体从羊毛中提取内部脂质的方法 Download PDFInfo
- Publication number
- CN101652463B CN101652463B CN2008800063802A CN200880006380A CN101652463B CN 101652463 B CN101652463 B CN 101652463B CN 2008800063802 A CN2008800063802 A CN 2008800063802A CN 200880006380 A CN200880006380 A CN 200880006380A CN 101652463 B CN101652463 B CN 101652463B
- Authority
- CN
- China
- Prior art keywords
- wool
- extraction
- under
- polar modifier
- methyl alcohol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/16—Emollients or protectives, e.g. against radiation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0203—Solvent extraction of solids with a supercritical fluid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0288—Applications, solvents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B11/00—Recovery or refining of other fatty substances, e.g. lanolin or waxes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B11/00—Recovery or refining of other fatty substances, e.g. lanolin or waxes
- C11B11/005—Lanolin; Woolfat
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Pharmacology & Pharmacy (AREA)
- Dermatology (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Toxicology (AREA)
- Extraction Or Liquid Replacement (AREA)
- Medicines Containing Plant Substances (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Cosmetics (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Fats And Perfumes (AREA)
Abstract
Description
试验 | 羊毛 | 压力(bar) | T(℃) | 助溶剂 | 助溶剂的%(v/v) | 总脂质相对于该羊毛重量的% |
1 | R-NZ | 360 | 60 | 甲醇 | 10 | 0.143 |
2 | R-NZ | 360 | 100 | 甲醇 | 10 | 0.226 |
3 | R-NZ | 360 | 160 | 甲醇 | 10 | 0.188 |
4 | R-NZ | 360 | 100 | 甲醇 | 20 | 0.125 |
5 | M-ES | 360 | 60 | 甲醇 | 10 | 0.147 |
6 | M-ES | 360 | 100 | 甲醇 | 10 | 0.202 |
7 | M-ES | 100 | 60 | 乙醇 | 20 | 0.881 |
8 | M-ES | 360 | 60 | 乙醇 | 20 | 0.564 |
实施例 | T(℃) | P(bars) | 极性调节剂(%,类型) | 总体积(mL) | IWL(%) | 神经酰胺(%) |
3 | 40 | 162 | 5,甲醇 | 200 | 0.624 | 0.226 |
4 | 40 | 253 | 10,甲醇 | 300 | 0.556 | 0.230 |
5 | 50 | 253 | 7.5,甲醇 | 200 | 0.600 | 0.227 |
6 | 60 | 233 | 10,甲醇 | 350 | 0.704 | 0.296 |
7 | 60 | 304 | 10,甲醇 | 250 | 0.858 | 0.296 |
8 | 75 | 304 | 10,甲醇 | 150 | 0.851 | 0.356 |
9 | 90 | 233 | 10,甲醇 | 350 | 0.803 | 0.297 |
10 | 90 | 304 | 10,甲醇 | 250 | 0.818 | 0.278 |
11 | 75 | 304 | 10,甲醇 | 350 | 0.823 | 0.297 |
12 | 60 | 162 | 7.5,甲醇 | 300 | 0.560 | 0.233 |
13 | 40 | 202 | 7.5,甲醇 | 250 | 0.550 | 0.232 |
14 | 60 | 162 | 10,乙醇 | 350 | 0.618 | 0.249 |
Claims (10)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ES200700543A ES2304213B1 (es) | 2007-03-01 | 2007-03-01 | Procedimiento para la extraccion de los lipidos internos de la lana con fluidos supercriticos. |
ESP200700543 | 2007-03-01 | ||
PCT/ES2008/070033 WO2008104630A1 (es) | 2007-03-01 | 2008-02-27 | Procedimiento para la extracción de los lípidos internos de la lana con fluidos supercriticos |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101652463A CN101652463A (zh) | 2010-02-17 |
CN101652463B true CN101652463B (zh) | 2012-08-22 |
Family
ID=39720868
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2008800063802A Expired - Fee Related CN101652463B (zh) | 2007-03-01 | 2008-02-27 | 利用超临界流体从羊毛中提取内部脂质的方法 |
Country Status (7)
Country | Link |
---|---|
US (1) | US8138362B2 (zh) |
EP (1) | EP2119763B1 (zh) |
JP (1) | JP2010520378A (zh) |
CN (1) | CN101652463B (zh) |
AT (1) | ATE518942T1 (zh) |
ES (2) | ES2304213B1 (zh) |
WO (1) | WO2008104630A1 (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6202270B2 (ja) * | 2011-01-17 | 2017-09-27 | インディア グリコルズ リミテッド | コウオウソウ属種−マリーゴールド花粗粉からの単段式ルテインエステル抽出 |
CN108251219A (zh) * | 2018-01-16 | 2018-07-06 | 西藏自治区农牧科学院农产品开发与食品科学研究所 | 一种羊毛脂提取方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001004244A1 (es) * | 1999-07-09 | 2001-01-18 | Consejo Superior De Investigaciones Cientificas | Composiciones y uso de extracto de lipidos internos de la lana en la preparacion de productos para el tratamiento y cuidado de la piel |
WO2002100990A1 (es) * | 2001-06-11 | 2002-12-19 | Consejo Superior De Investigaciones Científicas | Procedimiento de obtención de fracciones de lípidos con dióxido de carbono presurizado a partir de lana o lanolina |
CN1772856A (zh) * | 2004-11-08 | 2006-05-17 | 浙江霸力(鞋业)集团有限公司 | 从未脱脂羊毛中萃取回收羊毛脂的工艺方法 |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3619116A (en) | 1969-04-02 | 1971-11-09 | Thomas Burnley & Sons Ltd | Method for scouring wool |
DE3207914A1 (de) * | 1982-03-04 | 1983-09-15 | Skw Trostberg Ag, 8223 Trostberg | Verfahren zur extraktiven gewinnung von hochwertigen natuerlichen wachsen |
JPH08291228A (ja) * | 1995-04-21 | 1996-11-05 | Nok Corp | 加硫フッ素ゴムの再生方法 |
CN1059003C (zh) * | 1995-10-16 | 2000-11-29 | 克鲁普犹德有限公司 | 以超临界流体染色纺织基质的方法与装置 |
ES2161611B1 (es) | 1999-06-18 | 2003-04-01 | Consejo Superior Investigacion | Procedimiento de obtencion de lanolina y lana exentas de plaguicidas. |
NL1014395C2 (nl) * | 2000-02-16 | 2001-08-20 | Stork Brabant Bv | Werkwijze voor het verven van textielmaterialen in een superkritisch flu´dum. |
ES2186485B1 (es) | 2000-10-05 | 2004-08-16 | Universitat Politecnica De Catalunya | Procedimiento para la extraccion de lanolina de la lana y planta para la realizacion de dicho procedimiento. |
NL1021142C2 (nl) * | 2002-07-24 | 2004-01-27 | Stork Prints Bv | Inrichting en werkwijze voor het stuksgewijs of partij-gewijs onder hoge druk veredelen van stukken substraat, in het bijzonder textiel substraat. |
JP2004076190A (ja) * | 2002-08-15 | 2004-03-11 | Kobe Steel Ltd | 繊維処理方法 |
JP2004143613A (ja) * | 2002-10-23 | 2004-05-20 | Howa Kk | 含浸処理方法及び含浸処理された繊維製品 |
JP2006036638A (ja) * | 2004-07-22 | 2006-02-09 | Terumo Corp | 微細炭素繊維への親水性物質付着方法 |
-
2007
- 2007-03-01 ES ES200700543A patent/ES2304213B1/es not_active Expired - Fee Related
-
2008
- 2008-02-27 ES ES08736731T patent/ES2371130T3/es active Active
- 2008-02-27 US US12/529,453 patent/US8138362B2/en not_active Expired - Fee Related
- 2008-02-27 WO PCT/ES2008/070033 patent/WO2008104630A1/es active Application Filing
- 2008-02-27 CN CN2008800063802A patent/CN101652463B/zh not_active Expired - Fee Related
- 2008-02-27 JP JP2009551232A patent/JP2010520378A/ja active Pending
- 2008-02-27 EP EP08736731A patent/EP2119763B1/en not_active Not-in-force
- 2008-02-27 AT AT08736731T patent/ATE518942T1/de not_active IP Right Cessation
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001004244A1 (es) * | 1999-07-09 | 2001-01-18 | Consejo Superior De Investigaciones Cientificas | Composiciones y uso de extracto de lipidos internos de la lana en la preparacion de productos para el tratamiento y cuidado de la piel |
EP1201736A1 (en) * | 1999-07-09 | 2002-05-02 | Consejo Superior De Investigaciones Cientificas | Compositions of internal lipid extract of wool and use thereof in the preparation of products for skin care and treatment |
WO2002100990A1 (es) * | 2001-06-11 | 2002-12-19 | Consejo Superior De Investigaciones Científicas | Procedimiento de obtención de fracciones de lípidos con dióxido de carbono presurizado a partir de lana o lanolina |
CN1772856A (zh) * | 2004-11-08 | 2006-05-17 | 浙江霸力(鞋业)集团有限公司 | 从未脱脂羊毛中萃取回收羊毛脂的工艺方法 |
Non-Patent Citations (2)
Title |
---|
C.Dominguez et al..Characterization of Supercritical Fluid Extracts from Raw Wool by TLC-FID and GC-MS.《Journal of the American Oil Chemists" Society》.2003,第80卷(第7期),717. * |
L. Coderch et al..Extraction and Analysis of Ceramides from Internal Wool Lipids.《Journal of the American Oil Chemists" Society》.2002,第79卷(第12期),全文. * |
Also Published As
Publication number | Publication date |
---|---|
ES2304213B1 (es) | 2009-10-20 |
ES2371130T3 (es) | 2011-12-27 |
JP2010520378A (ja) | 2010-06-10 |
WO2008104630A1 (es) | 2008-09-04 |
ES2304213A1 (es) | 2008-09-16 |
EP2119763B1 (en) | 2011-08-03 |
US8138362B2 (en) | 2012-03-20 |
US20100099899A1 (en) | 2010-04-22 |
EP2119763A4 (en) | 2010-05-26 |
ATE518942T1 (de) | 2011-08-15 |
CN101652463A (zh) | 2010-02-17 |
EP2119763A1 (en) | 2009-11-18 |
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CI01 | Publication of corrected invention patent application |
Correction item: Inventor Correct: Coderch Negra Ma Luisa|Ramirez Mileo Raquel|Marti Gelabert Meritxell|Parra Juez Jose Luis|Garay Peral Iratxe|Salas Vaquero Oscar|Alvarez Alcega Jorge False: Coderch Negra Ma Luisa|Ramirez Mileo Raquel|Marti Gelabert Meritxell|Parra Juez Jose Luis|Garay Peral Iratxe|Salas Vaquero Oscar|Alvarez Alcega Jorge Number: 07 Volume: 26 |
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CI02 | Correction of invention patent application |
Correction item: Inventor Correct: Alvarez Alcega Jorge False: Alvarez Alcega Jorge Number: 07 Page: The title page Volume: 26 |
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Owner name: GAIKER CENTRO TECNOLOGICO Free format text: FORMER OWNER: SPAIN HIGHER RESEARCH COUNCIL Effective date: 20120216 Free format text: FORMER OWNER: GAIKER CENTRO TECNOLOGICO Effective date: 20120216 |
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Effective date of registration: 20120216 Address after: Zamudio Spain Applicant after: Consejo Superior Investigacion (ES) Address before: Madrid Applicant before: Consejo Superior De Investigaciones Cientificas Co-applicant before: Consejo Superior Investigacion (ES) |
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