CN101649548B - Batching medium - Google Patents
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- CN101649548B CN101649548B CN 200810044190 CN200810044190A CN101649548B CN 101649548 B CN101649548 B CN 101649548B CN 200810044190 CN200810044190 CN 200810044190 CN 200810044190 A CN200810044190 A CN 200810044190A CN 101649548 B CN101649548 B CN 101649548B
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Abstract
The invention provides a batching medium. The pH value of the batching medium is between 6.5 and 7.5, and the batching medium mainly comprises the following compositions in percentage by weight: 1.3 to 1.7 percent of 18 tertiary amine, 0.85 to 1.15 percent of diethylenetriamine, 1.3 to 1.7 percent of diethanol amine, 1.4 to 1.6 percent of polyethenoxy ether emulsifier, 9 to 12 percent of oleic acid, 1.3 to 1.7 percent of penetrant, 25 to 35 percent of carbamide, 2 to 3 percent of ethanol, 45 to 55 percent of water and 0.05 to 0.15 percent of brightener, wherein the penetrant is fatty alcohol-polyoxyethylene ether penetrant, the brightener is stilbene triazine brightener. The batching medium is used for batching and smoothing raw jute, raw sisal or hemp fiber, does not contain sodium hudroxide component, is fully prepared from organic chemical raw materials, is high-efficiency and environment-friendly, and can facilitate batching production management, reduce production cost, shorten stowing time and improve working environment.
Description
Technical field
The present invention relates to a kind of bast softening agent, be used for that jute raw ramie or sisal hemp raw material or hemp are carried out softening submissive.
Background technology
At present, when jute raw ramie or sisal hemp raw material are carried out softening the traditional soft sesame oil being accustomed to using, exist following shortcoming:
1, use not single auxiliary agent, as the multiple auxiliary agents such as use tea oil, rosin, caustic soda now join at the use scene, not only time-consuming but also take a lot of work, the management of unfavorable production technology;
2, traditional linen softening oil production cost is higher;
3, have unpleasant pungent taste, cause work situation abominable;
4, owing to containing caustic soda in this traditional linen softening oil, the operator has the sensation of the hand that burns;
5, the heap storage health after the humidification oil supply carry out machining when the jute raw ramie is carried out softening or to the sisal hemp raw material before, in the fermentation that reaches jute or sisal hemp and soft process, the time of using traditional linen softening oil can make heap storage ferment is quite long.
Summary of the invention
A kind of bast softening agent provided by the invention, it does not contain the caustic soda composition, all uses Organic Chemicals, high-efficiency environment friendly; Use the present invention can facilitate the softening production management, reduce production costs, shorten the heap storage time, improve work situation.
In order to achieve the above object, the invention provides a kind of bast softening agent, its pH value is 6.5-7.5, is prepared by following raw material:
Weight ratio is 18 tertiary amines of 1.3-1.7%;
Weight ratio is the diethylenetriamine of 0.85-1.15%;
Weight ratio is the diethanol amine of 1.3-1.7%;
Weight ratio is the polyethenoxy ether class emulsifying agent of 1.4-1.6%;
Weight ratio is the vegetable oil acid of 9-12%;
Weight ratio is the bleeding agent of 1.3-1.7%;
Weight ratio is the urea of 25-35%;
Weight ratio is the ethanol of 2-3%;
Weight ratio is the water of 45-55%; With
Weight ratio is the brightening agent of 0.05-0.15%;
Wherein, described bleeding agent is the fatty alcohol polyethenoxy ether class bleeding agent;
Described brightening agent is the toluylene triazine brightening agent;
The preparation method of described bast softening agent is:
The first step, in reactor, order is injected described water, 18 tertiary amines, ethanol, diethylenetriamine, diethanol amine, polyethenoxy ether class emulsifying agent and vegetable oil acid successively, and polycondensation is 6 hours at the temperature of 95 ℃-100 ℃, cooling rear generation bast softening agent intermediate;
Second step, after first urea being dissolved fully in reactor, the bast softening agent intermediate that reinjects and obtained by first step preparation method, add subsequently fatty alcohol polyethenoxy ether class bleeding agent and toluylene triazine brightening agent, at the temperature of 30 ℃ of left and right, stirred 3 hours, and adjusting pH value is 6.5-7.5, static 2 hours again, obtain described bast softening agent.
Bast softening agent provided by the invention, the heap storage health after the humidification oil supply when can be used for realizing the jute raw ramie is carried out softening reaches fermentation and the softness of jute; Heap storage health after humidification oil supply before also can be used for realizing the sisal hemp raw material is spun reaches fermentation and the softness of sisal hemp; The soft engineering that also can be used for hemp spins the hemp realization front submissive, and the spinning of favourable hemp improves its spinnability.
Bast softening agent provided by the invention is being used for that jute raw ramie or sisal hemp raw material or hemp are carried out the submissive process of softening, but rapid osmotic and adhere to the bast fiber layer of jute etc.; Can effectively impel pectin and lignin swelling in bast zone softening; When the organic matter in this bast softening agent with the bast fiber close contact after, can effectively produce rapidly the biological bacteria such as saccharomycete, pectin bacterium, impel the fermentation of bast fiber; Simultaneously, this bast softening agent can be protected the regain of fiber-spinnable preferably, because tossa etc. itself had not only contained water but also contained the composition of oil, therefore make not static electrification of fiber-spinnable.
The specific embodiment
Below illustrate better embodiment of the present invention.
The invention provides a kind of bast softening agent, its pH value is 6.5-7.5, is prepared by following raw material:
Weight ratio is 18 tertiary amines of 1.3-1.7%;
Weight ratio is the diethylenetriamine of 0.85-1.15%;
Weight ratio is the diethanol amine of 1.3-1.7%;
Weight ratio is the polyethenoxy ether class emulsifying agent of 1.4-1.6%;
Weight ratio is the vegetable oil acid of 9-12%;
Weight ratio is the bleeding agent of 1.3-1.7%;
Weight ratio is the urea of 25-35%;
Weight ratio is the ethanol of 2-3%; With
Weight ratio is the water of 45-55%.
Described bleeding agent is the fatty alcohol polyethenoxy ether class bleeding agent, can be specifically: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Further, the raw material of the described bast softening agent of preparation also comprises the brightening agent of 0.05-0.15%, and it can be used for the brightening of the products such as jute or sisal hemp prevented variable color.
Described brightening agent is the toluylene triazine brightening agent, can be specifically the VBL brightening agent.
Embodiment 1
Bast softening agent provided by the invention, the weight ratio of its raw materials and each raw material is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| 1 | 18 tertiary amines | 1.4 |
| 2 | Diethylenetriamine | 1.05 |
| 3 | Diethanol amine | 1.6 |
| 4 | The polyethenoxy ether class emulsifying agent | 1.4 |
| 5 | Vegetable oil acid | 10 |
| 6 | The fatty alcohol polyethenoxy ether class bleeding agent | 1.4 |
| 7 | Urea | 31.3 |
| 8 | Alcohol (ethanol) | 2.8 |
| 9 | The toluylene triazine brightening agent | 0.05 |
| 10 | Water | 49 |
[0045] Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 2
Bast softening agent provided by the invention, the weight ratio of its raw materials and each raw material is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| 1 | 18 tertiary amines | 1.6 |
| 2 | Diethylenetriamine | 0.95 |
| 3 | Diethanol amine | 1.4 |
| 4 | The polyethenoxy ether class emulsifying agent | 1.55 |
| 5 | Vegetable oil acid | 11 |
| 6 | The fatty alcohol polyethenoxy ether class bleeding agent | 1.65 |
| 7 | Urea | 28.5 |
| 8 | Alcohol (ethanol) | 2.3 |
| 9 | The toluylene triazine brightening agent | 0.08 |
| 10 | Water | 50.93 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 3
Bast softening agent provided by the invention, the weight ratio of its raw materials and each raw material is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| 1 | 18 tertiary amines | 1.55 |
[0057]
| 2 | Diethylenetriamine | 1.1 |
| 3 | Diethanol amine | 1.45 |
| 4 | The polyethenoxy ether class emulsifying agent | 1.45 |
| 5 | Vegetable oil acid | 9.5 |
| 6 | The fatty alcohol polyethenoxy ether class bleeding agent | 1.35 |
| 7 | Urea | 26.5 |
| 8 | Alcohol (ethanol) | 2.1 |
| 9 | The toluylene triazine brightening agent | 0.12 |
| 10 | Water | 54.88 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 4
Bast softening agent provided by the invention, the weight ratio of its raw materials and each raw material is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| 1 | 18 tertiary amines | 1.35 |
| 2 | Diethylenetriamine | 0.9 |
| 3 | Diethanol amine | 1.55 |
| 4 | The polyethenoxy ether class emulsifying agent | 1.55 |
| 5 | Vegetable oil acid | 11.5 |
| 6 | The fatty alcohol polyethenoxy ether class bleeding agent | 1.55 |
| 7 | Urea | 33.5 |
| 8 | Alcohol (ethanol) | 2.6 |
| 9 | The toluylene triazine brightening agent | 0.14 |
| 10 | Water | 45.36 |
[0064] Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 5
Bast softening agent provided by the invention, the weight ratio of its raw materials and each raw material is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| 1 | 18 tertiary amines | 1.35 |
| 2 | Diethylenetriamine | 0.9 |
| 3 | Diethanol amine | 1.55 |
| 4 | The polyethenoxy ether class emulsifying agent | 1.5 |
| 5 | Vegetable oil acid | 9.3 |
| 6 | The fatty alcohol polyethenoxy ether class bleeding agent | 1.6 |
| 7 | Urea | 33.84 |
| 8 | Alcohol (ethanol) | 2.9 |
| 9 | The toluylene triazine brightening agent | 0.06 |
| 10 | Water | 47 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 6
Bast softening agent provided by the invention, the weight ratio of its preparation and each raw material is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| 1 | 18 tertiary amines | 1.65 |
[0076]
| 2 | Diethylenetriamine | 1 |
| 3 | Diethanol amine | 1.65 |
| 4 | The polyethenoxy ether class emulsifying agent | 1.42 |
| 5 | Vegetable oil acid | 11.8 |
| 6 | The fatty alcohol polyethenoxy ether class bleeding agent | 1.38 |
| 7 | Urea | 26.1 |
| 8 | Alcohol (ethanol) | 2.4 |
| 9 | The toluylene triazine brightening agent | 0.1 |
| 10 | Water | 52.5 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
The bast softening agent that the invention described above provides, the equipment of its preparation are chemical reaction kettle, and concrete preparation method is:
The first step: in reactor, order Jiang Shui, 18 tertiary amines, alcohol, diethylenetriamine, diethanol amine, polyethenoxy ether class emulsifying agent be (for example successively to press operation requirements, the TX-10 emulsifying agent) and vegetable oil acid inject, polycondensation is about 6 hours at the temperature of 95 ℃-100 ℃, the intermediate of the described bast softening agent of cooling rear generation;
second step: after first urea being dissolved fully in reactor, the bast softening agent intermediate that reinjects and obtained by first step preparation method, (for example add subsequently the fatty alcohol polyethenoxy ether class bleeding agent, the AEO-9 high-efficient penetrant, or SHT high-efficient penetrant, or JFC high-efficient penetrant) and the toluylene triazine brightening agent (for example, the VBL brightening agent) after, at the temperature of 30 ℃ of left and right, stirred 3 hours, use simultaneously oily acid for adjusting pH, static 2 hours again, obtain bast softening agent of the present invention, it is that Acidity of Aikalinity pH value is the liquid of the Sandy (or faint yellow) of 6.5-7.5, last discharging barrelling warehouse-in.
The bast softening agent that the invention described above provides, the heap storage health after the humidification oil supply when can be used for realizing the jute raw ramie is carried out softening reaches fermentation and the softness of jute; Concrete using method is:
The first step, the liquid bast softening agent that is Sandy (or faint yellow) that will prepare through the chemical process of science are directly allocated the softening liquid of making the emulsification shape, i.e. humidification healthy liquid with water; The proportioning of described softening liquid (humidification healthy liquid) by as make decision: the proportioning of bast softening agent provided by the invention and water is 8%:92%;
Second step, the resulting softening liquid of use (humidification healthy liquid) spray jute on jute softener, the humidification amount of concrete spray should be controlled in 20%-30%, and namely the softening liquid of the jute raw ramie of 100 kilograms spray is 20 kilograms to 30 kilograms left and right.
Adopt bast softening agent provided by the invention, after the jute raw ramie is carried out the softening processing, have the following advantages:
1, can accelerate jute raw ramie fermentation, heap storage after 1 day numb stack temperature obviously raise, can reach 50 ℃ after 72 hours.
2, bast softening agent of the present invention in jute softening processing procedure, can not produce peculiar smell, and the bright feel of operating personnel, and the jute after heap storage simultaneously produces the fiber crops ash in spinning process few, favourable labour protection and production environment improvement.
3, the tossa after bast softening agent of the present invention carries out the softening processing, static electrification, do not make Spinning process smooth, do not twine roller, do not twine roller, few broken end.
4, use the jute yarn that obtains after bast softening agent processing of the present invention, its uniformity, intensity, pliability, glossiness and filoplume situation all are better than the jute yarn of traditional handicraft.
5, after utilization bast softening agent of the present invention carries out the softening processing to the jute raw ramie, can improve the spinnability of tossa, during the traditional bast softening agent of use, generally can spin the jute raw materials of 3.5 public jute yarns, after use the present invention, can spin the jute yarns that 5 public affairs are propped up.
The bast softening agent that the invention described above provides, the heap storage health after the humidification oil supply before also can be used for realizing the sisal hemp raw material is spun reaches fermentation and the softness of sisal hemp; Concrete using method is:
The first step, the liquid bast softening agent that is Sandy (or faint yellow) that will prepare through the chemical process of science are directly allocated the softening liquid of making the emulsification shape, i.e. humidification healthy liquid with water; The proportioning of described softening liquid (humidification healthy liquid) by as make decision: the proportioning of bast softening agent provided by the invention and water is 8%:92%;
Second step, the humidification amount of using resulting softening liquid (humidification healthy liquid) to spin front humidification health to sisal hemp are no more than 20%, and namely the added softening liquid of the sisal hemp raw ramie of 100 kilograms is no more than 20 kilograms.
The bast softening agent that the invention described above provides also can be used for the soft treatment of hemp, makes hemp realize spinning front submissive, and the spinning of favourable hemp improves its spinnability; Concrete using method is:
The first step, the liquid bast softening agent that is Sandy (or faint yellow) that will prepare through the chemical process of science are directly allocated the softening liquid of making the emulsification shape, i.e. humidification healthy liquid with water; The proportioning of described softening liquid (humidification healthy liquid) by as make decision: the consumption of bast softening agent provided by the invention coordinates with water by 8% of hemp amount and carries out heap storage and (press the humidification amount, be that the water yield is allocated) or carry out kiering (calculate the water yield by bath raio and allocate, general bath raio is 7-8);
Second step, the resulting softening liquid of use (humidification healthy liquid) are 15% left and right to the humidification amount of the heap storage soft treatment of hemp, and namely the added softening liquid of the hemp of 100 kilograms is 15 kilograms of left and right.
Bast softening agent provided by the invention is being used for that jute raw ramie or sisal hemp raw material or hemp are carried out the submissive process of softening, but rapid osmotic and adhere to the bast fiber layer of jute etc.; Can effectively impel pectin and lignin swelling in bast zone softening; When the organic matter in this bast softening agent with the bast fiber close contact after, can effectively produce rapidly the biological bacteria such as saccharomycete, pectin bacterium, impel the fermentation of bast fiber; Simultaneously, this bast softening agent can be protected the regain of fiber-spinnable preferably, because tossa etc. itself had not only contained water but also contained the composition of oil, therefore make not static electrification of fiber-spinnable.
Bast softening agent provided by the invention does not contain the caustic soda composition, all uses Organic Chemicals, high-efficiency environment friendly; Use the present invention can facilitate the softening production management, reduce production costs, shorten the heap storage time, improve work situation.
Claims (1)
1. a bast softening agent, is characterized in that, the pH value of this bast softening agent is 6.5-7.5, is prepared by following raw material:
Weight ratio is 18 tertiary amines of 1.3-1.7%;
Weight ratio is the diethylenetriamine of 0.85-1.15%;
Weight ratio is the diethanol amine of 1.3-1.7%;
Weight ratio is the polyethenoxy ether class emulsifying agent of 1.4-1.6%;
Weight ratio is the vegetable oil acid of 9-12%;
Weight ratio is the bleeding agent of 1.3-1.7%;
Weight ratio is the urea of 25-35%;
Weight ratio is the ethanol of 2-3%;
Weight ratio is the water of 45-55%; With
Weight ratio is the brightening agent of 0.05-0.15%;
Wherein, described bleeding agent is the fatty alcohol polyethenoxy ether class bleeding agent;
Described brightening agent is the toluylene triazine brightening agent;
The preparation method of described bast softening agent is:
The first step, in reactor, order is injected described water, 18 tertiary amines, ethanol, diethylenetriamine, diethanol amine, polyethenoxy ether class emulsifying agent and vegetable oil acid successively, and polycondensation is 6 hours at the temperature of 95 ℃-100 ℃, cooling rear generation bast softening agent intermediate;
Second step, after first urea being dissolved fully in reactor, the bast softening agent intermediate that reinjects and obtained by first step preparation method, add subsequently fatty alcohol polyethenoxy ether class bleeding agent and toluylene triazine brightening agent, at the temperature of 30 ℃ of left and right, stirred 3 hours, and adjusting pH value is 6.5-7.5, static 2 hours again, obtain described bast softening agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810044190 CN101649548B (en) | 2008-12-25 | 2008-12-25 | Batching medium |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810044190 CN101649548B (en) | 2008-12-25 | 2008-12-25 | Batching medium |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101649548A CN101649548A (en) | 2010-02-17 |
| CN101649548B true CN101649548B (en) | 2013-05-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN 200810044190 Active CN101649548B (en) | 2008-12-25 | 2008-12-25 | Batching medium |
Country Status (1)
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| CN (1) | CN101649548B (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101979734B (en) * | 2010-11-24 | 2011-08-31 | 郴州湘南麻业有限公司 | Jute spinning method |
| CN102677447B (en) * | 2011-03-15 | 2014-06-18 | 上海奇克氟硅材料有限公司 | Special organic scouring agent for flax and hemp and preparation method of scouring liquid thereof |
| CN106676896A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening agent |
| CN106676895A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Batching medium |
| CN106676885A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Hemp softening agent |
| CN106676886A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening oil |
| CN106676884A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening agent |
| CN109322154B (en) * | 2018-11-07 | 2021-12-07 | 青岛奥洛思新材料有限公司 | Lubricant for processing hemp roving and preparation method thereof |
| CN110230192A (en) * | 2019-06-27 | 2019-09-13 | 重庆市晶苎纺织品有限公司 | A kind of preparation method for expecting high-quality softening liquid for softening fiber crops |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1050231A (en) * | 1990-08-16 | 1991-03-27 | 江汉油田日用化工厂 | Bast softening agent |
| CN101319409A (en) * | 2008-07-17 | 2008-12-10 | 上海新浦化工厂有限公司 | YDM-T type organic retting agent and preparation method thereof |
| CN101319463A (en) * | 2008-07-17 | 2008-12-10 | 上海新浦化工厂有限公司 | YDM-J type organic composite slurry for bast fibre spinning industry and its preparation method |
| JP4468685B2 (en) * | 2003-12-12 | 2010-05-26 | 三洋化成工業株式会社 | Softener composition |
-
2008
- 2008-12-25 CN CN 200810044190 patent/CN101649548B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1050231A (en) * | 1990-08-16 | 1991-03-27 | 江汉油田日用化工厂 | Bast softening agent |
| JP4468685B2 (en) * | 2003-12-12 | 2010-05-26 | 三洋化成工業株式会社 | Softener composition |
| CN101319409A (en) * | 2008-07-17 | 2008-12-10 | 上海新浦化工厂有限公司 | YDM-T type organic retting agent and preparation method thereof |
| CN101319463A (en) * | 2008-07-17 | 2008-12-10 | 上海新浦化工厂有限公司 | YDM-J type organic composite slurry for bast fibre spinning industry and its preparation method |
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Address after: 200137, Jiangdong Road 1585, Shanghai, Pudong New Area Patentee after: Shanghai Sinpo special assistant Co., Ltd. Address before: 200137, Jiangdong Road 1585, Shanghai, Pudong New Area Patentee before: Shanghai Sepal Chemical Co., Ltd. |