CN101649548A - Batching medium - Google Patents
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- CN101649548A CN101649548A CN 200810044190 CN200810044190A CN101649548A CN 101649548 A CN101649548 A CN 101649548A CN 200810044190 CN200810044190 CN 200810044190 CN 200810044190 A CN200810044190 A CN 200810044190A CN 101649548 A CN101649548 A CN 101649548A
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Abstract
The invention provides a batching medium. The pH value of the batching medium is between 6.5 and 7.5, and the batching medium mainly comprises the following compositions in percentage by weight: 1.3 to 1.7 percent of 18 tertiary amine, 0.85 to 1.15 percent of diethylenetriamine, 1.3 to 1.7 percent of diethanol amine, 1.4 to 1.6 percent of polyethenoxy ether emulsifier, 9 to 12 percent of oleic acid, 1.3 to 1.7 percent of penetrant, 25 to 35 percent of carbamide, 2 to 3 percent of ethanol and 45 to 55 percent of water. The batching medium is used for batching and smoothing raw jute, raw sisal or hemp fiber, does not contain sodium hudroxide component, is fully prepared from organic chemical raw materials, is high-efficiency and environment-friendly, and can facilitate batching production management, reduce production cost, shorten stowing time and improve working environment.
Description
Technical field
The present invention relates to a kind of bast softening agent, it is submissive to be used for that jute raw ramie or sisal hemp raw material or hemp are carried out softening.
Background technology
At present, when jute raw ramie or sisal hemp raw material are carried out softening the traditional soft sesame oil being accustomed to using, exist following shortcoming:
1, use not single auxiliary agent, as multiple auxiliary agents such as use tea oil, rosin, caustic soda now join at the use scene, not only time-consuming but also take a lot of work, the management of unfavorable production technology;
2, traditional linen softening oil production cost is higher;
3, have unpleasant pungent taste, cause work situation abominable;
4, owing to contain caustic soda in this traditional linen softening oil, the operator has the sensation of the hand that burns;
5, the heap storage health after the humidification oil supply carry out machining when the jute raw ramie is carried out softening or to the sisal hemp raw material before, in the fermentation that reaches jute or sisal hemp and soft process, the time of using traditional linen softening oil can make heap storage ferment is quite long.
Summary of the invention
A kind of bast softening agent provided by the invention, it does not contain the caustic soda composition, all uses Organic Chemicals, high-efficiency environment friendly; Use the present invention can make things convenient for the softening production management, reduce production costs, shorten the heap storage time, improve work situation.
In order to achieve the above object, the invention provides a kind of bast softening agent, its pH value is 6.5-7.5, mainly comprises following component:
Weight ratio is 18 tertiary amines of 1.3-1.7%;
Weight ratio is the diethylenetriamine of 0.85-1.15%;
Weight ratio is the diethanol amine of 1.3-1.7%;
Weight ratio is the polyethenoxy ether class emulsifying agent of 1.4-1.6%;
Weight ratio is the vegetable oil acid of 9-12%;
Weight ratio is the bleeding agent of 1.3-1.7%;
Weight ratio is the urea of 25-35%;
Weight ratio is the ethanol of 2-3%; With
Weight ratio is the water of 45-55%.
Wherein, described bleeding agent is the fatty alcohol polyethenoxy ether class bleeding agent.
Further, described bast softening agent also comprises the brightening agent that weight ratio is 0.05-0.15%.
Described brightening agent is the toluylene triazine brightening agent.
Bast softening agent provided by the invention, the heap storage health after the humidification oil supply when can be used for realizing that the jute raw ramie carried out softening reaches fermentation and the softness of jute; Heap storage health after the humidification oil supply before also can be used for realizing the sisal hemp raw material spun reaches fermentation and the softness of sisal hemp; The soft engineering that also can be used for hemp, it is preceding submissive that the hemp realization is spun, and the spinning of favourable hemp improves its spinnability.
Bast softening agent provided by the invention is being used for that jute raw ramie or sisal hemp raw material or hemp are carried out the submissive process of softening, but rapid osmotic and adhere to the bast fiber layer of jute etc.; Can impel pectin and lignin swelling in the bast zone softening effectively; When the organic matter in this bast softening agent with after bast fiber closely contacts, can produce biological bacteria such as saccharomycete, pectin bacterium rapidly effectively, impel the fermentation of bast fiber; Simultaneously, but the regain of this bast softening agent better protect fiber-spinnable, because tossas etc. itself not only contain water but also contain oily composition, so make not static electrification of fiber-spinnable.
The specific embodiment
Below specify better embodiment of the present invention.
The invention provides a kind of bast softening agent, its pH value is 6.5-7.5, mainly comprises following component:
Weight ratio is 18 tertiary amines of 1.3-1.7%;
Weight ratio is the diethylenetriamine of 0.85-1.15%;
Weight ratio is the diethanol amine of 1.3-1.7%;
Weight ratio is the polyethenoxy ether class emulsifying agent of 1.4-1.6%;
Weight ratio is the vegetable oil acid of 9-12%;
Weight ratio is the bleeding agent of 1.3-1.7%;
Weight ratio is the urea of 25-35%;
Weight ratio is the ethanol of 2-3%; With
Weight ratio is the water of 45-55%.
Described bleeding agent is the fatty alcohol polyethenoxy ether class bleeding agent, specifically can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Further, described bast softening agent also comprises the brightening agent of 0.05-0.15%, and it can be used for the brightening of products such as jute or sisal hemp prevented variable color.
Described brightening agent is the toluylene triazine brightening agent, specifically can be the VBL brightening agent.
Embodiment 1
Bast softening agent provided by the invention, the weight ratio of its constituent and each composition is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| ??1 | 18 tertiary amines | ??1.4 |
| ??2 | Diethylenetriamine | ??1.05 |
| ??3 | Diethanol amine | ??1.6 |
| ??4 | The polyethenoxy ether class emulsifying agent | ??1.4 |
| ??5 | Vegetable oil acid | ??10 |
| ??6 | The fatty alcohol polyethenoxy ether class bleeding agent | ??1.4 |
| ??7 | Urea | ??31.3 |
| ??8 | Alcohol (ethanol) | ??2.8 |
| ??9 | The toluylene triazine brightening agent | ??0.05 |
| ??10 | Water | ??49 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 2
Bast softening agent provided by the invention, the weight ratio of its constituent and each composition is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| ??1 | 18 tertiary amines | ??1.6 |
| ??2 | Diethylenetriamine | ??0.95 |
| ??3 | Diethanol amine | ??1.4 |
| ??4 | The polyethenoxy ether class emulsifying agent | ??1.55 |
| ??5 | Vegetable oil acid | ??11 |
| ??6 | The fatty alcohol polyethenoxy ether class bleeding agent | ??1.65 |
| ??7 | Urea | ??28.5 |
| ??8 | Alcohol (ethanol) | ??2.3 |
| ??9 | The toluylene triazine brightening agent | ??0.08 |
| ??10 | Water | ??50.93 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 3
Bast softening agent provided by the invention, the weight ratio of its constituent and each composition is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| ??1 | 18 tertiary amines | ??1.55 |
| ??2 | Diethylenetriamine | ??1.1 |
| ??3 | Diethanol amine | ??1.45 |
| ??4 | The polyethenoxy ether class emulsifying agent | ??1.45 |
| ??5 | Vegetable oil acid | ??9.5 |
| ??6 | The fatty alcohol polyethenoxy ether class bleeding agent | ??1.35 |
| ??7 | Urea | ??26.5 |
| ??8 | Alcohol (ethanol) | ??2.1 |
| ??9 | The toluylene triazine brightening agent | ??0.12 |
| ??10 | Water | ??54.88 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 4
Bast softening agent provided by the invention, the weight ratio of its constituent and each composition is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| ??1 | 18 tertiary amines | ??1.35 |
| ??2 | Diethylenetriamine | ??0.9 |
| ??3 | Diethanol amine | ??1.55 |
| ??4 | The polyethenoxy ether class emulsifying agent | ??1.55 |
| ??5 | Vegetable oil acid | ??11.5 |
| ??6 | The fatty alcohol polyethenoxy ether class bleeding agent | ??1.55 |
| ??7 | Urea | ??33.5 |
| ??8 | Alcohol (ethanol) | ??2.6 |
| ??9 | The toluylene triazine brightening agent | ??0.14 |
| ??10 | Water | ??45.36 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 5
Bast softening agent provided by the invention, the weight ratio of its constituent and each composition is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| ??1 | 18 tertiary amines | ??1.35 |
| ??2 | Diethylenetriamine | ??0.9 |
| ??3 | Diethanol amine | ??1.55 |
| ??4 | The polyethenoxy ether class emulsifying agent | ??1.5 |
| ??5 | Vegetable oil acid | ??9.3 |
| ??6 | The fatty alcohol polyethenoxy ether class bleeding agent | ??1.6 |
| ??7 | Urea | ??33.84 |
| ??8 | Alcohol (ethanol) | ??2.9 |
| ??9 | The toluylene triazine brightening agent | ??0.06 |
| ??10 | Water | ??47 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
Embodiment 6
Bast softening agent provided by the invention, the weight ratio of its constituent and each composition is as follows:
| Sequence number | Constituent | Mass ratio (%) |
| ??1 | 18 tertiary amines | ??1.65 |
| ??2 | Diethylenetriamine | ??1 |
| ??3 | Diethanol amine | ??1.65 |
| ??4 | The polyethenoxy ether class emulsifying agent | ??1.42 |
| ??5 | Vegetable oil acid | ??11.8 |
| ??6 | The fatty alcohol polyethenoxy ether class bleeding agent | ??1.38 |
| ??7 | Urea | ??26.1 |
| ??8 | Alcohol (ethanol) | ??2.4 |
| ??9 | The toluylene triazine brightening agent | ??0.1 |
| ??10 | Water | ??52.5 |
Wherein, described fatty alcohol polyethenoxy ether class bleeding agent can be: AEO-9 high-efficient penetrant or SHT high-efficient penetrant or JFC high-efficient penetrant.
Described polyethenoxy ether class emulsifying agent can be the TX-10 emulsifying agent.
Described toluylene triazine brightening agent can be the VBL brightening agent.
The bast softening agent that the invention described above provided, the equipment of its preparation are chemical reaction kettle, and concrete preparation method is:
The first step: in reactor, by operation requirement preface Jiang Shui successively, 18 tertiary amines, alcohol, diethylenetriamine, diethanol amine, polyethenoxy ether class emulsifying agent (for example, the TX-10 emulsifying agent) and vegetable oil acid inject, polycondensation is about 6 hours under 95 ℃-100 ℃ temperature, and the cooling back generates the intermediate of described bast softening agent;
Second step: after in reactor, earlier urea being dissolved fully, the bast softening agent intermediate that reinjects and obtain by first step preparation method, (for example add the fatty alcohol polyethenoxy ether class bleeding agent subsequently, the AEO-9 high-efficient penetrant, or SHT high-efficient penetrant, or JFC high-efficient penetrant) and the toluylene triazine brightening agent (for example, the VBL brightening agent) after, under the temperature about 30 ℃, stirred 3 hours, regulate PH with oleic acid simultaneously, static again 2 hours, obtain bast softening agent of the present invention, it is that the Acidity of Aikalinity pH value is the liquid of the Sandy (or faint yellow) of 6.5-7.5, last discharging barrelling warehouse-in.
The bast softening agent that the invention described above provided, the heap storage health after the humidification oil supply when can be used for realizing that the jute raw ramie carried out softening reaches fermentation and the softness of jute; Concrete using method is:
The first step, the liquid bast softening agent that is Sandy (or faint yellow) that will prepare through the chemical process of science are directly allocated the softening liquid of making the emulsification shape, i.e. humidification healthy liquid with water; The proportioning of described softening liquid (humidification healthy liquid) by as make decision: the proportioning of bast softening agent provided by the invention and water is 8%:92%;
Second step, the resulting softening liquid of use (humidification healthy liquid) spray jute on jute softener, and the humidification amount of concrete spray should be controlled in the 20%-30%, and promptly the softening liquid of 100 kilograms jute raw ramie spray is about 20 kilograms to 30 kilograms.
Adopt bast softening agent provided by the invention, the jute raw ramie carried out having the following advantages after softening handles:
1, can quicken jute raw ramie fermentation, heap storage after 1 day numb stack temperature obviously raise, after 72 hours, can reach 50 ℃.
2, bast softening agent of the present invention can not produce peculiar smell in jute softening processing procedure, and the bright feel of operating personnel, and the jute after the heap storage simultaneously produces the fiber crops ash in spinning process few, favourable labour protection and production environment improvement.
3, the tossa after bast softening agent of the present invention carries out the softening processing, static electrification is produced smoothly spinning, does not twine roller, does not twine roller, the few broken end.
4, the jute yarn that obtains after utilization bast softening agent of the present invention is handled, its uniformity, intensity, pliability, glossiness and filoplume situation all are better than the jute yarn of traditional handicraft.
5, utilization bast softening agent of the present invention carries out after softening handles the jute raw ramie, can improve the spinnability of tossa, when using traditional bast softening agent, generally can spin the jute raw materials of 3.5 public jute yarns, after using the present invention, can spin 5 public jute yarns.
The bast softening agent that the invention described above provided, the heap storage health after the humidification oil supply before also can be used for realizing the sisal hemp raw material spun reaches fermentation and the softness of sisal hemp; Concrete using method is:
The first step, the liquid bast softening agent that is Sandy (or faint yellow) that will prepare through the chemical process of science are directly allocated the softening liquid of making the emulsification shape, i.e. humidification healthy liquid with water; The proportioning of described softening liquid (humidification healthy liquid) by as make decision: the proportioning of bast softening agent provided by the invention and water is 8%:92%;
Second step, the humidification amount of using resulting softening liquid (humidification healthy liquid) that sisal hemp is spun preceding humidification health are no more than 20%, and promptly the added softening liquid of 100 kilograms sisal hemp raw ramie is no more than 20 kilograms.
The bast softening agent that the invention described above provided also can be used for the soft treatment of hemp, and submissive before making hemp realize spinning, the spinning of favourable hemp improves its spinnability; Concrete using method is:
The first step, the liquid bast softening agent that is Sandy (or faint yellow) that will prepare through the chemical process of science are directly allocated the softening liquid of making the emulsification shape, i.e. humidification healthy liquid with water; The proportioning of described softening liquid (humidification healthy liquid) by as make decision: the consumption of bast softening agent provided by the invention fits into the windrow storehouse and (presses the humidification amount with water by 8% of hemp amount, be that the water yield is allocated) or carry out kiering (calculate the water yield by bath raio and allocate, general bath raio is 7-8);
Second step, the resulting softening liquid of use (humidification healthy liquid) are about 15% to the humidification amount of the heap storage soft treatment of hemp, and promptly the added softening liquid of 100 kilograms hemp is about 15 kilograms.
Bast softening agent provided by the invention is being used for that jute raw ramie or sisal hemp raw material or hemp are carried out the submissive process of softening, but rapid osmotic and adhere to the bast fiber layer of jute etc.; Can impel pectin and lignin swelling in the bast zone softening effectively; When the organic matter in this bast softening agent with after bast fiber closely contacts, can produce biological bacteria such as saccharomycete, pectin bacterium rapidly effectively, impel the fermentation of bast fiber; Simultaneously, but the regain of this bast softening agent better protect fiber-spinnable, because tossas etc. itself not only contain water but also contain oily composition, so make not static electrification of fiber-spinnable.
Bast softening agent provided by the invention does not contain the caustic soda composition, all uses Organic Chemicals, high-efficiency environment friendly; Use the present invention can make things convenient for the softening production management, reduce production costs, shorten the heap storage time, improve work situation.
Claims (4)
1. a bast softening agent is characterized in that, the pH value of this bast softening agent is 6.5-7.5, mainly comprises following component:
Weight ratio is 18 tertiary amines of 1.3-1.7%;
Weight ratio is the diethylenetriamine of 0.85-1.15%;
Weight ratio is the diethanol amine of 1.3-1.7%;
Weight ratio is the polyethenoxy ether class emulsifying agent of 1.4-1.6%;
Weight ratio is the vegetable oil acid of 9-12%;
Weight ratio is the bleeding agent of 1.3-1.7%;
Weight ratio is the urea of 25-35%;
Weight ratio is the ethanol of 2-3%; With
Weight ratio is the water of 45-55%.
2. bast softening agent as claimed in claim 1 is characterized in that, described bleeding agent is the fatty alcohol polyethenoxy ether class bleeding agent.
3. bast softening agent as claimed in claim 1 is characterized in that, described bast softening agent also comprises the brightening agent that weight ratio is 0.05-0.15%.
4. bast softening agent as claimed in claim 3 is characterized in that, described brightening agent is the toluylene triazine brightening agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810044190 CN101649548B (en) | 2008-12-25 | 2008-12-25 | Batching medium |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810044190 CN101649548B (en) | 2008-12-25 | 2008-12-25 | Batching medium |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101649548A true CN101649548A (en) | 2010-02-17 |
| CN101649548B CN101649548B (en) | 2013-05-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200810044190 Active CN101649548B (en) | 2008-12-25 | 2008-12-25 | Batching medium |
Country Status (1)
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| CN (1) | CN101649548B (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101979734A (en) * | 2010-11-24 | 2011-02-23 | 郴州湘南麻业有限公司 | Jute spinning method |
| CN102677447A (en) * | 2011-03-15 | 2012-09-19 | 上海奇克氟硅材料有限公司 | Special organic scouring agent for flax and hemp and preparation method of scouring liquid thereof |
| CN106676885A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Hemp softening agent |
| CN106676886A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening oil |
| CN106676896A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening agent |
| CN106676895A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Batching medium |
| CN106676884A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening agent |
| CN109322154A (en) * | 2018-11-07 | 2019-02-12 | 青岛奥洛思新材料有限公司 | It is a kind of for handling the lubricant and preparation method thereof of crudefiber crop rove |
| CN110230192A (en) * | 2019-06-27 | 2019-09-13 | 重庆市晶苎纺织品有限公司 | A kind of preparation method for expecting high-quality softening liquid for softening fiber crops |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1050231A (en) * | 1990-08-16 | 1991-03-27 | 江汉油田日用化工厂 | Bast softening agent |
| JP4468685B2 (en) * | 2003-12-12 | 2010-05-26 | 三洋化成工業株式会社 | Softener composition |
| CN101319409B (en) * | 2008-07-17 | 2010-12-08 | 上海新浦化工厂有限公司 | Ydm-t type organic retting agent and preparation method thereof |
| CN101319463B (en) * | 2008-07-17 | 2010-11-17 | 上海新浦化工厂有限公司 | YDM-J type organic composite slurry for bast fibre spinning industry and its preparation method |
-
2008
- 2008-12-25 CN CN 200810044190 patent/CN101649548B/en active Active
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101979734A (en) * | 2010-11-24 | 2011-02-23 | 郴州湘南麻业有限公司 | Jute spinning method |
| CN101979734B (en) * | 2010-11-24 | 2011-08-31 | 郴州湘南麻业有限公司 | Jute spinning method |
| CN102677447A (en) * | 2011-03-15 | 2012-09-19 | 上海奇克氟硅材料有限公司 | Special organic scouring agent for flax and hemp and preparation method of scouring liquid thereof |
| CN102677447B (en) * | 2011-03-15 | 2014-06-18 | 上海奇克氟硅材料有限公司 | Special organic scouring agent for flax and hemp and preparation method of scouring liquid thereof |
| CN106676885A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Hemp softening agent |
| CN106676886A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening oil |
| CN106676896A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening agent |
| CN106676895A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Batching medium |
| CN106676884A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening agent |
| CN109322154A (en) * | 2018-11-07 | 2019-02-12 | 青岛奥洛思新材料有限公司 | It is a kind of for handling the lubricant and preparation method thereof of crudefiber crop rove |
| CN109322154B (en) * | 2018-11-07 | 2021-12-07 | 青岛奥洛思新材料有限公司 | Lubricant for processing hemp roving and preparation method thereof |
| CN110230192A (en) * | 2019-06-27 | 2019-09-13 | 重庆市晶苎纺织品有限公司 | A kind of preparation method for expecting high-quality softening liquid for softening fiber crops |
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| CN101649548B (en) | 2013-05-08 |
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Address after: 200137, Jiangdong Road 1585, Shanghai, Pudong New Area Patentee after: Shanghai Sinpo special assistant Co., Ltd. Address before: 200137, Jiangdong Road 1585, Shanghai, Pudong New Area Patentee before: Shanghai Sepal Chemical Co., Ltd. |