CN101647872A - Peony essential oil soft capsule and preparation method thereof - Google Patents
Peony essential oil soft capsule and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a peony essential oil soft capsule which is prepared by using peony seed oil, peony essential oil and vitamin E as raw materials according to a proportion of 1:0.0005-0.005:0.001-0.01 through the steps of essential oil extraction, seed oil extraction, content preparation, soft capsule preparation, and the like. The invention not only provides an extraction method of paeonia rockii essential oil, but also develops a product being suitable to be developed by using the peony essential oil, thereby solving the problems of inconvenient taking of fresh flower essential oil and difficult quantification and filling the blank of the development of a paeonia rockii essential oil product. The peony essential oil soft capsule product has abundant nutrition, and the peony essential oil contains abundant natural scent substances such as citronellol, geraniol, linalool, and the like and also contains abundant terpenes and hydrocarbons which can relax human bodies, calm down emotions and diminish inflammation and has good effect on adjusting female incretion. Meanwhile, the peony seed oil and the vitamin E in the raw materials have the effects of enhancing intelligence, enhancing immunity, reducing blood fat, preventing inflammation, delaying senescence, and the like.
Description
Technical field
The present invention relates to ethereal oil of flower production and applied technical field, especially the production technology of Flos Moutan quintessence oil is a kind of peony essential oil soft capsule specifically, and the present invention also comprises the preparation method of this peony essential oil soft capsule.
Background technology
Paeonia suffruticosa is as traditional famous flower of China, and with its elegant and poised appearance, rich and honour lucky symbolic meaning is loved by the people.Flos Moutan not only has ornamental value, also has very high medical value.Carry according to the doctor's brief note that is unearthed in the Gansu Wuwei tomb of Han dynasty in 1972, as far back as the Han dynasty, people are with Paeonia suffruticosa treatment blood stasis disease; The record Flos Moutan is traditional medical material of heat-clearing and toxic substances removing in the Compendium of Material Medica, and its bitter in the mouth, property are flat, nontoxic, have the effect with blood, hemopoietic, removing heat from blood, regulating menstruation and activating blood; On Linxia, Gansu and other places, the white disease of local women red peony petal treatment stream red, white petal treatment stream commonly used; In China dietetic therapy side among the people, Flos Moutan commonly used is treated dysmenorrhea.Find according to modern scientific research, contain a large amount of vitamin, protein, saccharide, trace element etc. in the Flos Moutan, it is not only nutritious to take Flos Moutan, also has certain function of health care.Flos Moutan is carried and contains abundant natural flavor material in the quintessence oil, as citronellol, geraniol, linalool etc., contains abundant terpenes and hydrocarbon compound simultaneously, can releive, calm, antiinflammatory, to regulating female incretion good effect is arranged.The Gansu Paeonia papaveracea is the second largest product population of Chinese Paeonia suffruticosa, with cold-resistant drought-enduring, plant is tall and big, large flower and brilliant color, give off a strong fragrance, characteristics such as resistant to diseases and insects is strong, significantly being different from Luoyang, Henan and Heze, Shandong is the Central Plains Paeonia suffruticosa of representative.Paeonia papaveracea is extensively planted in the various places, Gansu, and concentrated cultivation mainly is distributed in ground such as Lanzhou, Linxia, Lintao.Along with Chinese economic development, the Paeonia papaveracea demand is increasing in recent years, and the cultivated area of Paeonia suffruticosa is also increasing rapidly.Paeonia papaveracea gives off a strong fragrance, and the quintessence oil extraction rate reached is to more than three times of Central Plains Paeonia suffruticosa, for exploitation Paeonia papaveracea essential oil product provides good basis.And the Paeonia suffruticosa Products Development also is in the starting stage now, and the utilization of peony essential oil also only is confined to the cosmetics aspect.Because Central Plains peony petal essential oil content is very low, the peony essential oil Products Development has been subjected to very big restriction, and Paeonia papaveracea is at present to sell Miao Weizhu, the flowers are in blossom for annual large quantities of Paeonia suffruticosa in the ground, mashed in the ground, fail to bring into play its due effect.The exploitation of ethereal oil of flower at present is mainly used in champignon, cosmetics exploitation.The peony essential oil cost is too high, and it is lower to be used for the conventional use earning rate, is difficult to embody its advantage.Oral ethereal oil of flower instant effect, effective, but because most quintessence oils require own allotment when edible uses inconveniently, and the amount of quintessence oil is difficult to assurance, has limited the popularization of oral quintessence oil.
Summary of the invention
The present invention will solve ethereal oil of flower exactly and take inconvenience, is difficult to quantized problem, and a kind of peony essential oil soft capsule and preparation method thereof is provided, and fills up the blank of Paeonia papaveracea essential oil product exploitation.
The present invention solves its technical problem by following technical proposals:
A kind of peony essential oil soft capsule is a raw material by peony seed oil, peony essential oil and vitamin E, is prepared from by following weight proportion:
Peony seed oil: peony essential oil: vitamin E=1: 0.0005～0.005: 0.001～0.01.
Prepare by following step and method:
A. quintessence oil extracts: the morning, 6:00-11:00 adopted half-open Paeonia papaveracea, adopted vapor distillation or solvent extraction legal system Flos Moutan quintessence oil;
B. seed oil extracts: adopt sophisticated seed of Flos Moutan, machine barking makes peony seed oil with physical squeezing or solvent extraction, through deacidification, comes unstuck, dry decolouring, and technologies such as vacuum deodorization make refining Paeonia suffruticosa oil;
C. content preparation: peony essential oil with 10 times of refining peony seed oil dilutions, will be diluted quintessence oil and peony seed oil again with 1: 19～199 mixed, and the vitamin E and the mix homogeneously that add 0.1-1% are done content, stir;
D. soft capsule is made: conventional method is made soft capsule.
The steam distillation that described quintessence oil extracts by: added immediately in the extraction pot adopting peony petal, add the water of 4 times of volumes, be heated to boiling, backflow 3h tells the upper strata quintessence oil.
When the described peony petal of adopting can not in time be put into extraction pot, be placed at the shady and cool ventilation place, flower thickness is preserved less than 10cm, and the holding time surpasses at 1 o'clock, adopts saline preservation or ethanol to preserve.
The solvent extraction that described quintessence oil extracts is: in new fresh peong flower, add the long-pending ethanol of triploid, and lixiviate twice, each 5 hours, decompression recycling ethanol got Flos Moutan extractum; Add 60～90 petroleum ether of two volumes in extractum, fully stir, filter, get filtrate, the reclaim under reduced pressure petroleum ether gets peony essential oil.
The present invention not only provides Paeonia papaveracea extracts essential oil method, and has developed the product of suitable peony essential oil development, has solved ethereal oil of flower and has taken inconvenience, is difficult to quantized problem; Contain abundant natural flavor material in the peony essential oil,, contain abundant terpenes and hydrocarbon compound simultaneously, can releive, calm, antiinflammatory, good effect is arranged regulating female incretion as citronellol, geraniol, linalool etc.Peony seed oil and vitamin E in the raw material has effects such as nootropics, enhancing immunity, blood fat reducing, prevention of inflammation, slow down aging again simultaneously.
The specific embodiment
Below in conjunction with embodiment the present invention is further elaborated.
Embodiment 1
1. quintessence oil extracts: the morning, 6:00-11:00 adopted half-open Paeonia papaveracea, adopted steam distillation to extract quintessence oil: adopting peony petal 400kg is added in the extraction pot immediately, add 1200L water, be heated to boiling, backflow 3h tells upper strata quintessence oil 40ml.
2. seed oil extracts: adopt sophisticated paeonia rockii seed, machine barking makes Paeonia suffruticosa var. papaveracea (Andr.) Kerner seed oil with milling process, through deacidification, comes unstuck, dry decolouring, and technologies such as vacuum deodorization make refining Paeonia suffruticosa oil.
3. content preparation: in the 40ml peony essential oil, add the refining peony seed oil of 360ml, stir the dilution quintessence oil.To dilute quintessence oil and pour in the refining peony seed oil of 7.6L, add the 80g vitamin E, and this mixture be stirred do content.
4. soft capsule is made: conventional method is pressed into soft capsule.
Embodiment 2
1. quintessence oil extracts: the morning, 6:00-11:00 adopted half-open Paeonia papaveracea, adopted solvent extraction to extract quintessence oil: adding 30L ethanol in new fresh peong flower 10kg, and lixiviate twice, each 5 hours, decompression recycling ethanol must about 80g Flos Moutan extractum; Add 160ml boiling range 60～90 petroleum ether in extractum, fully stir, filter, get filtrate, the reclaim under reduced pressure petroleum ether gets the 1.54ml peony essential oil.
2. seed oil extracts: adopt sophisticated paeonia rockii seed, machine barking makes Paeonia suffruticosa var. papaveracea (Andr.) Kerner seed oil with solvent extraction, through deacidification, comes unstuck, dry decolouring, and technologies such as vacuum deodorization make refining Paeonia suffruticosa oil.
3. content preparation: get the 1ml peony essential oil, add the refining peony seed oil of 9ml stir the dilution quintessence oil.In the dilution quintessence oil, add refining peony seed oil of 190ml and 0.2g vitamin E and mix, stir as content.
4. soft capsule is made: conventional method is pressed into soft capsule.
Embodiment 3
1. quintessence oil extracts: the morning, 6:00-11:00 adopted half-open Paeonia papaveracea, adopt steam distillation to extract quintessence oil: adopting peony petal is placed on the shady and cool ventilation place, flower thickness is less than 10cm, preserve, the holding time is no more than one day, gets the 45kg peony petal during extraction, add 120L water, be heated to boiling, backflow 3h tells upper strata quintessence oil 3.8ml.
2. seed oil extracts: adopt sophisticated paeonia rockii seed, machine barking makes Paeonia suffruticosa var. papaveracea (Andr.) Kerner seed oil with milling process, through deacidification, comes unstuck, dry decolouring, and technologies such as vacuum deodorization make refining Paeonia suffruticosa oil.
3. content preparation: in the 3.8ml peony essential oil, add the refining peony seed oil of 34.2ml, stir the dilution quintessence oil.To dilute quintessence oil and pour in the refining peony seed oil of 7.56L, add the 8g vitamin E, and this mixture be stirred do content.
4. soft capsule is made: conventional method is pressed into soft capsule.
Embodiment 4
1. quintessence oil extracts: the morning, 6:00-11:00 adopted half-open Paeonia papaveracea, adopt steam distillation to extract quintessence oil: adopting peony petal is pickled with the Sal of petal 14% amount, get the peony petal that 450kg pickles during extraction, add 1200L water, be heated to boiling, backflow 3h tells upper strata quintessence oil 40ml.
2. seed oil extracts: adopt sophisticated paeonia rockii seed, machine barking makes Paeonia suffruticosa var. papaveracea (Andr.) Kerner seed oil with milling process, through deacidification, comes unstuck, dry decolouring, and technologies such as vacuum deodorization make refining Paeonia suffruticosa oil.
3. content preparation: in the 40ml peony essential oil, add the refining peony seed oil of 360ml, stir the dilution quintessence oil.To dilute quintessence oil and pour in the refining peony seed oil of 77.6L, add the 80g vitamin E, and this mixture be stirred do content.
4. soft capsule is made: conventional method is pressed into soft capsule.
Claims (5)
1, a kind of peony essential oil soft capsule is characterized in that by peony seed oil, peony essential oil and vitamin E be raw material, is prepared from by following weight proportion:
Peony seed oil: peony essential oil: vitamin E=1: 0.0005～0.005: 0.001～0.01.
2, a kind of method for preparing the described peony essential oil soft capsule of claim 1 is characterized in that by following step and method preparation:
A. quintessence oil extracts: the morning, 6:00-11:00 adopted half-open Paeonia papaveracea, adopted vapor distillation or solvent extraction legal system Flos Moutan quintessence oil;
B. seed oil extracts: adopt sophisticated seed of Flos Moutan, machine barking makes peony seed oil with physical squeezing or solvent extraction, through deacidification, comes unstuck, dry decolouring, and technologies such as vacuum deodorization make refining peony seed oil;
C. content preparation: peony essential oil with 10 times of refining peony seed oil dilutions, will be diluted quintessence oil and peony seed oil again with 1: 19～199 mixed, and the vitamin E and the mix homogeneously that add 0.1-1% are done content, stir;
D. soft capsule is made: make soft capsule according to a conventional method.
3, the preparation method of a kind of peony essential oil soft capsule according to claim 2, it is characterized in that steam distillation that described quintessence oil extracts by: added immediately in the extraction pot adopting peony petal, add the water of 4 times of volumes, be heated to boiling, refluxed 3 hours, and told the upper strata quintessence oil.
4, according to the preparation method of claim 2 or 3 described a kind of peony essential oil soft capsules, it is characterized in that described steam distillation extracts quintessence oil, the peony petal of adopting is placed on the shady and cool ventilation place and preserves, and flower thickness is less than 10cm; Holding time surpasses at 1 o'clock, adds 14% Sal preservation.
5, the preparation method of a kind of peony essential oil soft capsule according to claim 2, it is characterized in that the solvent extraction that described quintessence oil extracts is: in new fresh peong flower, add the long-pending ethanol of triploid, lixiviate twice, each 5 hours, decompression recycling ethanol gets Flos Moutan extractum; Add 60～90 petroleum ether of two volumes in extractum, fully stir, filter, get filtrate, the reclaim under reduced pressure petroleum ether gets peony essential oil.
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| CN102362895A (en) * | 2011-11-19 | 2012-02-29 | 河南科技大学 | Method for extracting medicinal ingredient against methicillin-resistant staphylococcus aureus from peony seeds |
| CN102599495A (en) * | 2012-02-29 | 2012-07-25 | 赵孝庆 | Peony-seed-oil soft capsule and preparation method thereof |
| CN102631669A (en) * | 2012-03-23 | 2012-08-15 | 天津市益倍建生物技术有限公司 | Nutritional breast patch and preparation method thereof |
| CN102071096B (en) * | 2009-11-20 | 2012-08-22 | 菏泽瑞璞牡丹产业科技发展有限公司 | Preparation method of peony seed oil |
| CN102766535A (en) * | 2012-08-01 | 2012-11-07 | 河南华美生物工程有限公司 | Method for extracting peony oil by water |
| CN102907741A (en) * | 2012-10-24 | 2013-02-06 | 刘文锋 | Preparation method of peony seed oil oral liquid |
| CN103432028A (en) * | 2013-08-09 | 2013-12-11 | 安徽农业大学 | Paeonia ostii seed natural activity skin cream and preparation method thereof |
| CN103484256A (en) * | 2013-10-11 | 2014-01-01 | 青岛农业大学 | Method for extracting peony stamen volatile oil by using steam distillation |
| CN103494206A (en) * | 2013-10-24 | 2014-01-08 | 洛阳祥和牡丹科技有限公司 | Preparation process of soft capsule containing peony seed essential oil and peony petal isoflavone |
| CN103519177A (en) * | 2013-10-24 | 2014-01-22 | 洛阳祥和牡丹科技有限公司 | Preparation method for soft capsule containing peony seed essential oil and xylitol |
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| CN102362895A (en) * | 2011-11-19 | 2012-02-29 | 河南科技大学 | Method for extracting medicinal ingredient against methicillin-resistant staphylococcus aureus from peony seeds |
| CN102599495A (en) * | 2012-02-29 | 2012-07-25 | 赵孝庆 | Peony-seed-oil soft capsule and preparation method thereof |
| CN102599495B (en) * | 2012-02-29 | 2013-08-07 | 赵孝庆 | Peony-seed-oil soft capsule and preparation method thereof |
| CN102631669A (en) * | 2012-03-23 | 2012-08-15 | 天津市益倍建生物技术有限公司 | Nutritional breast patch and preparation method thereof |
| CN102631669B (en) * | 2012-03-23 | 2013-11-06 | 天津市益倍建生物技术有限公司 | Nutritional breast patch and preparation method thereof |
| CN102766535A (en) * | 2012-08-01 | 2012-11-07 | 河南华美生物工程有限公司 | Method for extracting peony oil by water |
| CN102907741A (en) * | 2012-10-24 | 2013-02-06 | 刘文锋 | Preparation method of peony seed oil oral liquid |
| CN103844270A (en) * | 2012-12-04 | 2014-06-11 | 洛阳花瓣舞生物技术有限公司 | Hypolipidemic compound peony seed oil soft capsule |
| CN103432028A (en) * | 2013-08-09 | 2013-12-11 | 安徽农业大学 | Paeonia ostii seed natural activity skin cream and preparation method thereof |
| CN103432028B (en) * | 2013-08-09 | 2015-08-12 | 安徽农业大学 | A kind of Paeonia ostii seed natural activity protective skin cream and preparation method thereof |
| CN103484256A (en) * | 2013-10-11 | 2014-01-01 | 青岛农业大学 | Method for extracting peony stamen volatile oil by using steam distillation |
| CN103494206B (en) * | 2013-10-24 | 2014-12-24 | 洛阳祥和牡丹科技有限公司 | Preparation process of soft capsule containing peony seed essential oil and peony petal isoflavone |
| CN103519177A (en) * | 2013-10-24 | 2014-01-22 | 洛阳祥和牡丹科技有限公司 | Preparation method for soft capsule containing peony seed essential oil and xylitol |
| CN103494206A (en) * | 2013-10-24 | 2014-01-08 | 洛阳祥和牡丹科技有限公司 | Preparation process of soft capsule containing peony seed essential oil and peony petal isoflavone |
| CN103519177B (en) * | 2013-10-24 | 2015-04-08 | 洛阳祥和牡丹科技有限公司 | Preparation method for soft capsule containing peony seed essential oil and xylitol |
| CN103820212A (en) * | 2014-03-06 | 2014-05-28 | 洛阳春魁农业开发有限公司 | Blend edible oil of peony seed oil and peanut oil and preparation method of blend edible oil |
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| CN104000196A (en) * | 2014-06-04 | 2014-08-27 | 李�杰 | Compound peony seed oil preparation, and making method and application thereof |
| CN104000196B (en) * | 2014-06-04 | 2016-03-16 | 李�杰 | Compound tree peony seed oil formulation and preparation method and application |
| CN104041831A (en) * | 2014-06-26 | 2014-09-17 | 河南科技大学 | Soft peony peptide capsule and preparation method thereof |
| CN104041831B (en) * | 2014-06-26 | 2015-08-26 | 河南科技大学 | A kind of tree peony polypeptide soft capsule and preparation method thereof |
| CN104116913A (en) * | 2014-07-31 | 2014-10-29 | 河南科技大学第一附属医院 | Speckle removing oral solution and preparation method thereof |
| CN105038946A (en) * | 2015-06-24 | 2015-11-11 | 洛阳国花坊牡丹生物科技有限公司 | Peony essential oil supercritical CO2 extraction method |
| CN106350224A (en) * | 2016-08-31 | 2017-01-25 | 镇雄县益雄药业有限公司 | Compound blood pressure reducing peony oil |
| CN112920905A (en) * | 2021-02-03 | 2021-06-08 | 甘肃盛宏牡业综合开发集团有限公司 | Method for extracting essential oil from paeonia rockii petals |
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Open date: 20100217 |