CN101647521B - Egg promoting feed additive for poultry and preparation method thereof - Google Patents
Egg promoting feed additive for poultry and preparation method thereof Download PDFInfo
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Abstract
The invention discloses an egg promoting feed additive for poultry and a preparation method thereof, belonging to the field of animal nutrition. The egg promoting feed additive is mainly prepared from codonopsis pilosula leaves, astragalus root, epimedium, glossy privet fruit, folium artemisiae argyi, notherwort herb, acanthopanax root, hawthorn, humifuse euphorbaia herb, scurfpea fruit, pine leaves and radix polygoni multiflori preparata. The preparation method comprises the following steps: adding water in the 12 Chinese herbal medicines and decocting the Chinese herbal medicines 1 to 3 times, filtering, mixing decoction, concentrating filtrate into thick paste which has the relative density of 1.10 to 1.30 at 60 DEG C to 80 DEG C, adding ethanol, after the ethanol content reaches 47.5 percent to 80 percent in the ratio by volume, performing ethanol precipitation, filtering, recovering ethanol from filtrate until no ethanol odor is smelt and drying to obtain the active ingredients of the egg promoting feed additive. The egg promoting feed additive for poultry has the advantages of small side effect, convenient use and quick absorption. After the egg promoting feed additive for poultry is used, the egg laying rate is obviously improved, the feed-egg ratio is reduced, and the feed returns are improved. The preparation method adopts water extraction, ethanol precipitation and spray drying so that the active ingredients are sufficiently extracted, the impurities are less and the dissolution effect is favorable.
Description
Technical field
The invention belongs to the animal nutrition field, be specifically related to a stud bird and used egg promoting feed additive and preparation method thereof.
Background technology
Along with the fast development of modern feed industry, a large amount of artificial synthetic feed addictives such as antibiotic, somatotropin, pest repellant, hormone, flavor enhancement, modifying agent, anticorrisive agent generally add in feed.These Application of Additives have played huge impetus undoubtedly to animal husbandry, but along with research deepen continuously and produce in the problem that occurs, people have recognized the negative effect that these additives bring gradually.Particularly antibiotic a large amount of uses, even abuse, the drug resistance and the harm residual and that bring for humans and animals health that cause producing have caused vast researcher and consumer's concern and worry.And Chinese herbal medicine is just with the mode of action of its uniqueness, good result, noresidue, the no resistance to the action of a drug and pollution-free and be subjected to vast research and production personnel's favor.China is vast in territory, and Chinese herbal medicine resource is very abundant, therefore aspect the development Chinese herb feed additive great potential is being arranged.The present Chinese herbal feed additive of producing directly makes an addition in the feed with the pulverizing of bulk drug, after stirring, or with rough digestion agent feed interpolation.Adapt to the requirement of modernized feed production technology, just must change this rough method and formulation at present, take diverse ways to separate purification, extraction or refining at compound or folk prescription, obtain its active ingredient or bioactivator, to realize using trace mineral supplement can obtain satisfied effect, adapt to the modern production of feed industry better.
Summary of the invention
The object of the present invention is to provide a stud bird to use egg promoting feed additive and preparation method thereof.
For achieving the above object, the present invention has taked following technical scheme:
One stud bird is used egg promoting feed additive, and this additive is mainly made by each raw material of following weight proportion: Radix Codonopsis leaf 6～48g, the Radix Astragali 6～36g, barrenwort 6～21g, the fruit of glossy privet 6～21g, tarragon 6～48g, motherwort 9～48g, wilsonii 6～36g, hawthorn 9～36g, wolf's milk 6～36g, Psoralea corylifolia 6～21g, pine needle 6～240g, RADIX POLYGONI MULTIFLORI PREPARATA 6～21g.
Further, adding has VA 1,000 ten thousand～5,000 ten thousand IU, VB in the described additive
11～3g, VD
33,000,000～7,500,000 IU, VB
21～6g, calcium pantothenate 5～20g, VE 1.5 ten thousand～30,000 IU, VB
61～6g, VB
120.01～0.06g, VK
32～10g, VC 5～50g.
Preferably, additive is granule or powder.
One stud bird is used the preparation method of egg promoting feed additive, this method follows these steps to preparation: take by weighing Radix Codonopsis leaf 6～48g by weight ratio, the Radix Astragali 6～36g, barrenwort 6～21g, the fruit of glossy privet 6～21g, tarragon 6～48g, motherwort 9～48g, wilsonii 6～36g, hawthorn 9～36g, wolf's milk 6～36g, Psoralea corylifolia 6～21g, pine needle 6～240g, RADIX POLYGONI MULTIFLORI PREPARATA 6～21g, with above 12 flavor Chinese medicine boilings 1～3 time, filter, collecting decoction, it is 1.10～1.30 thick paste at 60～80 ℃ that filtrate is concentrated into relative density, add ethanol, in volume ratio, make the alcohol amount of containing reach 47.5～80% and carry out alcohol precipitation, leave standstill, filter, filtrate recycling ethanol is not to there being the alcohol flavor, and drying promptly gets the active constituent of additive of the present invention.
Further, after the drying, add VA 1,000 ten thousand～5,000 ten thousand IU, VB by weight ratio
11～3g, VD
33,000,000～7,500,000 IU, VB
21～6g, calcium pantothenate 5～20g, VE 1.5 ten thousand～30,000 IU, VB
61～6g, VB
120.010～0.060g, VK
32～10g, VC 5～50g.
Preferably, described drying is a spray-drying, and EAT is 80～90 ℃, and leaving air temp is 30～45 ℃, and the pan feeding flow is 50～70L/h, and atmospheric pressure is 0.4～0.8Mpa, and aerosol pressure is 0.1～0.3Mpa.Atmospheric pressure refers to the pressure that the external world gives, and the aerosol adjustable in pressure saves the shower nozzle size and regulates aerosol pressure.
Preferably, during boiling, add the water of 6～12 times of 12 flavor Chinese medicine gross weight at every turn, decoct 1～2h.
Preferably, used ethanol is that bulk purity is 95% ethanol.
Preferably, the active constituent of additive of the present invention routinely processing technology make granule or powder.
When preparation granule or powder, can also add in active constituent of the present invention has auxiliary material, and described auxiliary material is sucrose 0～850g, add beneficial powder 0～850g.Sucrose both can be used as filler and also can be used as binder, added beneficial powder as filler, and filler plays diluting effect in powder and granule.
Among the present invention, Radix Codonopsis leaf, the Radix Astragali, air making-up and spleen enlivening; Hawthorn, food digesting stomach fortifying; Wolf's milk, clearing heat and detoxicating; Barrenwort, Psoralea corylifolia, warming and invigorating kidney Yang; Wilsonii, the fruit of glossy privet, RADIX POLYGONI MULTIFLORI PREPARATA nourish kidney yin; Motherwort, tarragon specially go into uterus, by promoting blood circulation, help the output of egg; Pine needle (another name pine needle), bitter, warm in nature, have that extra-nutrition, invigorating the spleen are regulated the flow of vital energy, dispelled pathogenic wind and remove dampness, desinsection and effect such as antipruritic, a lot of in recent years tests confirm: pine needle contains necessary bioactivator of growth of animal and nutritional labeling, contain abundant carrotene, chlorophyll and multivitamin, and contain 17 seed amino acids and tens kinds of trace elements and various plants bacteriocidin, it can strengthen metabolism, disease preventing and treating, the promotion growth of animal body and improve production performance.
Using method of the present invention: mixed feeding, every 100g additive mix fodder of the present invention 200kg, fowl free choice feeding; Mix drink, every 100g additive of the present invention is converted water 400kg, and fowl is from drinking.
Fowl of the present invention is little with the egg promoting feed additive side effect, easy to use, absorb fast, do not influence the charge ratio of feed, after the use, to bird egg-decreasing syndrome, egg duck, laying hen unknown cause egg drop reduction, do not have the peak or lay eggs of laying eggs and pace up and down and symptom such as do not rise and laying rate after the sick fowl rehabilitation is all had significant rise effect; Preparation method of the present invention adopts water extract-alcohol precipitation, spray-drying, and active constituent extracts fully, and impurity is few, and result of extraction is good.
The specific embodiment
Below the present invention is described in further detail with specific embodiment, but protection scope of the present invention is not limited thereto:
Formulation Example 1～7 sees Table 1.
The formulation Example of table 1 poultry fodder additive of the present invention
Preparation embodiment
Embodiment 8
Proportioning by embodiment 1 takes by weighing each raw material, with the Radix Codonopsis leaf, the Radix Astragali, barrenwort, the fruit of glossy privet, tarragon, motherwort, wilsonii, hawthorn, wolf's milk, Psoralea corylifolia, pine needle, RADIX POLYGONI MULTIFLORI PREPARATA 12 flavor Chinese medicine boilings 1 time, in water/12 flavor Chinese medicine gross weights, the water that adds 6 times, decoct 2h, filter, it is 1.10 thick paste at 60 ℃ that filtrate is concentrated into relative density, adds 95% (volume) ethanol, makes to contain the alcohol amount and reach 47.5% (V/V) and carry out alcohol precipitation, leave standstill, filter, filtrate recycling ethanol is not to there being the alcohol flavor, and (EAT is 80 ℃ to spray-drying, leaving air temp is 30 ℃, the pan feeding flow is 50L/h, and atmospheric pressure is 0.4Mpa, and aerosol pressure is 0.1Mpa) the active constituent of additive of the present invention, add auxiliary material sucrose then, pulverize, mixing promptly gets the powder of additive of the present invention.
Embodiment 9
Proportioning by embodiment 2 takes by weighing each raw material, with the Radix Codonopsis leaf, the Radix Astragali, barrenwort, the fruit of glossy privet, tarragon, motherwort, wilsonii, hawthorn, wolf's milk, Psoralea corylifolia, pine needle, RADIX POLYGONI MULTIFLORI PREPARATA 12 flavor Chinese medicine boilings 3 times, in water/12 flavor Chinese medicine gross weights, add for the first time 12 times water, decoct 2h, add 8 times water for the second time, decoct 1.5h, add 6 times water for the third time, decoct 1h, filter, merge three times decocting liquid, it is 1.30 thick paste at 80 ℃ that filtrate is concentrated into relative density, add 95% (volume) ethanol, make to contain the alcohol amount and reach 80% (V/V) and carry out alcohol precipitation, leave standstill, filter, filtrate recycling ethanol is not to there being the alcohol flavor, and (EAT is 90 ℃ to spray-drying, and leaving air temp is 45 ℃, the pan feeding flow is 70L/h, atmospheric pressure is 0.8Mpa, and aerosol pressure is 0.3Mpa) the active constituent of additive of the present invention, add auxiliary material then and add beneficial powder, crushing screening (100 order), mixed softwood, the oven dry of granulating promptly gets the granule of additive of the present invention.
Embodiment 10
Proportioning by embodiment 3 takes by weighing each raw material, with the Radix Codonopsis leaf, the Radix Astragali, barrenwort, the fruit of glossy privet, tarragon, motherwort, wilsonii, hawthorn, wolf's milk, Psoralea corylifolia, pine needle, RADIX POLYGONI MULTIFLORI PREPARATA 12 flavor Chinese medicine boilings 2 times, in water/12 flavor Chinese medicine gross weights, add for the first time 10 times water, decoct 1.5h, add for the second time 8 times water, decoct 1h, filter, merge the decocting liquid of secondary, it is 1.20 thick paste at 70 ℃ that filtrate is concentrated into relative density, add 95% (volume) ethanol, make to contain the alcohol amount and reach 76% (V/V) and carry out alcohol precipitation, leave standstill, filter, filtrate recycling ethanol is not to there being the alcohol flavor, and (EAT is 85 ℃ to spray-drying, and leaving air temp is 40 ℃, the pan feeding flow is 60L/h, atmospheric pressure is 0.6Mpa, and aerosol pressure is 0.2Mpa) the active constituent of additive of the present invention, add auxiliary material sucrose then and add beneficial powder, crushing screening (100 order), mixed softwood, the oven dry of granulating promptly gets the granule of additive of the present invention.
Embodiment 11
Proportioning by embodiment 4 takes by weighing each raw material, Radix Codonopsis leaf, the Radix Astragali, barrenwort, the fruit of glossy privet, tarragon, motherwort, wilsonii, hawthorn, wolf's milk, Psoralea corylifolia, pine needle, RADIX POLYGONI MULTIFLORI PREPARATA 12 flavor Chinese medicines by the active constituent that the water of embodiment 8 is carried, alcohol precipitation, drying process with atomizing get additive of the present invention, are added VA, VB then
1, VD
3, VB
2, calcium pantothenate, VE, VB
6, VK
3, VB
12, VC, auxiliary material sucrose and add beneficial powder, crushing screening (100 order), mixed softwood, the oven dry of granulating promptly get the granule of additive of the present invention.
Embodiment 12
Proportioning by embodiment 5 takes by weighing each raw material, Radix Codonopsis leaf, the Radix Astragali, barrenwort, the fruit of glossy privet, tarragon, motherwort, wilsonii, hawthorn, wolf's milk, Psoralea corylifolia, pine needle, RADIX POLYGONI MULTIFLORI PREPARATA 12 flavor Chinese medicines by the active constituent that the water of embodiment 9 is carried, alcohol precipitation, drying process with atomizing get additive of the present invention, are added VA, VB then
1, VD
3, VB
2, calcium pantothenate, VE, VB
6, VK
3, VB
12, VC, auxiliary material sucrose and add beneficial powder, pulverize, mixing promptly gets the powder of additive of the present invention.
Embodiment 13
Proportioning by embodiment 6 takes by weighing each raw material, with the Radix Codonopsis leaf, the Radix Astragali, barrenwort, the fruit of glossy privet, tarragon, motherwort, wilsonii, hawthorn, wolf's milk, Psoralea corylifolia, pine needle, RADIX POLYGONI MULTIFLORI PREPARATA 12 flavor Chinese medicine boilings 2 times, in water/12 flavor Chinese medicine gross weights, add for the first time 8 times water, decoct 1.5h, add 6 times water for the second time, decoct 1h, filter, it is 1.15 thick paste at 65 ℃ that the decocting liquid that merges secondary, filtrate are concentrated into relative density, adds 95% (volume) ethanol, make the alcohol amount of containing reach 66% (V/V) and carry out alcohol precipitation, leave standstill, filter, filtrate recycling ethanol is to there not being the alcohol flavor, (EAT is 85 ℃ to spray-drying, leaving air temp is 35 ℃, and the pan feeding flow is 55L/h, and atmospheric pressure is 0.5Mpa, aerosol pressure is 0.15Mpa) the active constituent of additive of the present invention, add VA then, VB
1, VD
3, VB
2, calcium pantothenate, VE, VB
6, VK
3, VB
12, VC, auxiliary material sucrose and add beneficial powder, the powder that pulverize, mixing promptly gets additive of the present invention.
Embodiment 14
Proportioning by embodiment 7 takes by weighing each raw material, with the Radix Codonopsis leaf, the Radix Astragali, barrenwort, the fruit of glossy privet, tarragon, motherwort, wilsonii, hawthorn, wolf's milk, Psoralea corylifolia, pine needle, RADIX POLYGONI MULTIFLORI PREPARATA 12 flavor Chinese medicine boilings 2 times, in water/12 flavor Chinese medicine gross weights, add for the first time 10 times water, decoct 2h, add 8 times water for the second time, decoct 1.5h, filter, it is 1.23 thick paste at 73 ℃ that the decocting liquid that merges secondary, filtrate are concentrated into relative density, adds 95% (volume) ethanol, make the alcohol amount of containing reach 73% (V/V) and carry out alcohol precipitation, leave standstill, filter, filtrate recycling ethanol is to there not being the alcohol flavor, (EAT is 88 ℃ to spray-drying, leaving air temp is 43 ℃, and the pan feeding flow is 65L/h, and atmospheric pressure is 0.7Mpa, aerosol pressure is 0.25Mpa) the active constituent of additive of the present invention, add VA then, VB
1, VD
3, VB
2, calcium pantothenate, VE, VB
6, VK
3, VB
12, VC, auxiliary material sucrose and add beneficial powder, crushing screening (100 order), mixed softwood, the oven dry of granulating promptly get the granule of additive of the present invention.
For further specifying technique effect of the present invention, carried out the clinical experimental study that following laying hen increases the egg effect especially:
1. the selection of test chicken and grouping
For matching the commodity Dai Yafa chicken of commodity in the sea in Northwest Agricultural University irrigation station chicken farm for laying hen and chicken farm, an agricultural station.Test is carried out in two batches, and first selects for use sea match in 62 ages in week commodity for 640 of laying hens, is divided into 8 groups at random, and 80 every group, test 42d.Second batch is selected 54 ages in week inferior commodity of sending out for 320 of laying hens, is divided into 8 groups at random, and 40 every group, test 42d.First all establishes 7 test group, 1 control group with second batch.
2. feed and management
The honest 114 laying hen complete diet pellets that experimental period all provides with the honest feed corporation,Ltd in Handan, its trophic level is a crude protein 15.79%, coarse ash 11.23%, crude fibre 3.24%, calcium 3.5%, phosphorus 0.5%, metabolizable energy 11.17 million Jiao/kg, above percentage composition all is meant weight percentage.Test chicken all adopts and raises in cages, and free choice feeding is given cleaning drinking-water, by each laying hen Routine Management.
3. the consumption of poultry fodder additive of the present invention and usage
7 test group are fed respectively and are raised the additive that formulation Example 1～7 and corresponding preparation embodiment 8～14 prepare.Test group is all fed by 0.05% (100g poultry fodder additive of the present invention mix fodder 200kg), and control group is only fed the honest 114 laying hen complete diet pellets of basal feed.
4. observe the mensuration project
4.1 chickens' extract god, appetite, morbidity and death condition respectively organized in record.
4.2 egg number and the weight of chicken respectively organized in record.
4.3 feed consumption every day respectively organized in record, measures feedstuff-egg ratio, calculates the price of deed.
5. result of the test
5.1 clinical observation
Duration of test, test group and control group are searched for food, ight soil, the state of mind, general Non Apparent Abnormality, the test initial stage of test group is more dried slightly than control group ight soil.Test group average every batch every group dead 0～1 (less than 1), dead 5 of control group.
5.2 the price of deed and production performance
First, second batch of result of the test see Table 2,3 respectively.
First result of the test of table 2
Second batch of result of the test of table 3
Annotate: laying rate raising=test group test back laying rate-control group test back laying rate; Price of deed raising=(control group feedstuff-egg ratio-test group feedstuff-egg ratio)/test group feedstuff-egg ratio
6. discussion of results
From table 2,3 as can be known: feed addictive of the present invention is significantly increased to the laying rate of laying hen, and the feedstuff-egg ratio of test group significantly reduces than the feedstuff-egg ratio of control group, and the price of deed significantly improves, and economic benefit is considerable, this product also has the disease-prevention health effect simultaneously, can reduce the death of chicken.The pure Chinese medicine class (embodiment 1～3) of feed addictive of the present invention is with adding vitamins (embodiment 4～7) relatively, add laying rate behind the vitamins, the price of deed improve more more than pure Chinese medicine class, similar between each test group laying rate, price of deed there was no significant difference.
7. expansion feeding experiment
On the basis of two batches of tests, respectively in the Yanshi, Qixian County, Zhumadian mechanized chicken farm and the specialist of raising chickens, to 12000 laying hens, the contrast test of feeding is as stated above further verified its effect.Result and above-mentioned result of the test basically identical.
Claims (10)
1. a stud bird is used egg promoting feed additive, it is characterized in that this additive mainly made by each raw material of following weight proportion: Radix Codonopsis leaf 6～48g, the Radix Astragali 6～36g, barrenwort 6～21g, the fruit of glossy privet 6～21g, tarragon 6～48g, motherwort 9～48g, wilsonii 6～36g, hawthorn 9～36g, wolf's milk 6～36g, Psoralea corylifolia 6～21g, pine needle 6～240g, RADIX POLYGONI MULTIFLORI PREPARATA 6～21g; With above 12 flavor Chinese medicine boilings 1～3 time, filter, it is 1.10～1.30 thick paste at 60～80 ℃ that collecting decoction, filtrate are concentrated into relative density, adds ethanol, in volume ratio, make the alcohol amount of containing reach 47.5～80% and carry out alcohol precipitation, filter, filtrate recycling ethanol is to there not being the alcohol flavor, drying promptly gets the active constituent of additive of the present invention; Described drying is a spray-drying, and EAT is 80～90 ℃, and leaving air temp is 30～45 ℃, and the pan feeding flow is 50～70L/h, and atmospheric pressure is 0.4～0.8Mpa, and aerosol pressure is 0.1～0.3Mpa.
2. fowl according to claim 1 is used egg promoting feed additive, it is characterized in that: described additive is after drying, and adding has VA 1,000 ten thousand～5,000 ten thousand IU, VB
11～3g, VD
33,000,000～7,500,000 IU, VB
21～6g, calcium pantothenate 5～20g, VE 1.5 ten thousand～30,000 IU, VB
61～6g, VB
120.01～0.06g, VK
32～10g, VC 5～50g.
3. fowl according to claim 1 and 2 is used egg promoting feed additive, it is characterized in that: additive is granule or powder.
4. a stud bird is used the preparation method of egg promoting feed additive, it is characterized in that this method follows these steps to preparation: take by weighing Radix Codonopsis leaf 6～48g by weight ratio, the Radix Astragali 6～36g, barrenwort 6～21g, the fruit of glossy privet 6～21g, tarragon 6～48g, motherwort 9～48g, wilsonii 6～36g, hawthorn 9～36g, wolf's milk 6～36g, Psoralea corylifolia 6～21g, pine needle 6～240g, RADIX POLYGONI MULTIFLORI PREPARATA 6～21g, with above 12 flavor Chinese medicine boilings 1～3 time, filter, collecting decoction, it is 1.10～1.30 thick paste at 60～80 ℃ that filtrate is concentrated into relative density, add ethanol, in volume ratio, make the alcohol amount of containing reach 47.5～80% and carry out alcohol precipitation, filter, filtrate recycling ethanol is to there not being the alcohol flavor, drying promptly gets the active constituent of additive of the present invention.
5. fowl according to claim 4 is characterized in that: after the drying, add VA 1,000 ten thousand～5,000 ten thousand IU, VB by weight ratio with the preparation method of egg promoting feed additive
11～3g, VD
33,000,000～7,500,000 IU, VB
21～6g, calcium pantothenate 5～20g, VE 1.5 ten thousand～30,000 IU, VB
61～6g, VB
120.010～0.060g, VK
32～10g, VC 5～50g.
6. according to claim 4 or 5 described fowl preparation method with egg promoting feed additives, it is characterized in that: described drying is a spray-drying, EAT is 80～90 ℃, leaving air temp is 30～45 ℃, the pan feeding flow is 50～70L/h, atmospheric pressure is 0.4～0.8Mpa, and aerosol pressure is 0.1～0.3Mpa.
7. fowl according to claim 6 is characterized in that: during boiling, add the water of 6～12 times of 12 flavor Chinese medicine gross weight at every turn, decoct 1～2h with the preparation method of egg promoting feed additive.
8. fowl according to claim 7 is used the preparation method of egg promoting feed additive, and it is characterized in that: the bulk purity of used ethanol is 95%.
9. fowl according to claim 8 is used the preparation method of egg promoting feed additive, and it is characterized in that: the active constituent of additive of the present invention processing technology is routinely made granule or pulvis.
10. fowl according to claim 9 is used the preparation method of egg promoting feed additive, it is characterized in that: when preparation granule or pulvis, adding has auxiliary material sucrose 0～850g, adds beneficial powder 0～850g.
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| CN104938805A (en) * | 2015-05-22 | 2015-09-30 | 黄海英 | Additive for increasing laying rate of ducks |
| CN105232678A (en) * | 2015-11-11 | 2016-01-13 | 郑州后羿制药有限公司 | Traditional Chinese medicine granules capable of increasing egg yield of laying hens and preparing method thereof |
| CN106578383A (en) * | 2016-12-13 | 2017-04-26 | 敦化市长白山绿色禽产品科技开发有限公司 | Herba epimedii-mugwort compound poultry feed additive |
| CN110122702A (en) * | 2019-06-18 | 2019-08-16 | 河南省帝一方生物制药有限公司 | It is a kind of for improving the compound preparation and preparation method thereof of fowl laying rate |
| CN114617196A (en) * | 2022-04-06 | 2022-06-14 | 西藏自治区农牧科学院畜牧兽医研究所 | Supplementary feed concentrate capable of increasing milk yield of yaks and preparation method thereof |
-
2009
- 2009-06-26 CN CN2009100652860A patent/CN101647521B/en not_active Expired - Fee Related
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| CN101647521A (en) | 2010-02-17 |
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