CN101496513B - 一种苯醚甲环唑悬浮种衣剂及其制备方法 - Google Patents
一种苯醚甲环唑悬浮种衣剂及其制备方法 Download PDFInfo
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- CN101496513B CN101496513B CN2008100569252A CN200810056925A CN101496513B CN 101496513 B CN101496513 B CN 101496513B CN 2008100569252 A CN2008100569252 A CN 2008100569252A CN 200810056925 A CN200810056925 A CN 200810056925A CN 101496513 B CN101496513 B CN 101496513B
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- difenoconazole
- agent
- seed
- coating agent
- suspension seed
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- 239000005760 Difenoconazole Substances 0.000 title claims abstract description 39
- BQYJATMQXGBDHF-UHFFFAOYSA-N difenoconazole Chemical compound O1C(C)COC1(C=1C(=CC(OC=2C=CC(Cl)=CC=2)=CC=1)Cl)CN1N=CN=C1 BQYJATMQXGBDHF-UHFFFAOYSA-N 0.000 title claims abstract description 39
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 239000003795 chemical substances by application Substances 0.000 title claims description 32
- 239000000725 suspension Substances 0.000 claims abstract description 19
- -1 alkane sulfonate Chemical class 0.000 claims abstract description 16
- 239000011248 coating agent Substances 0.000 claims abstract description 15
- DMAXMXPDVWTIRV-UHFFFAOYSA-N 2-(2-phenylethyl)phenol Chemical compound OC1=CC=CC=C1CCC1=CC=CC=C1 DMAXMXPDVWTIRV-UHFFFAOYSA-N 0.000 claims abstract description 10
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000004576 sand Substances 0.000 claims abstract description 9
- 239000004094 surface-active agent Substances 0.000 claims abstract description 7
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims abstract description 6
- 239000000600 sorbitol Substances 0.000 claims abstract description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229920000570 polyether Polymers 0.000 claims abstract description 4
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims abstract description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 3
- 239000010452 phosphate Substances 0.000 claims abstract description 3
- 238000003756 stirring Methods 0.000 claims abstract description 3
- 229910021653 sulphate ion Inorganic materials 0.000 claims abstract description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 30
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000002518 antifoaming agent Substances 0.000 claims description 10
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims description 7
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims description 7
- 150000004996 alkyl benzenes Chemical class 0.000 claims description 7
- 239000011575 calcium Substances 0.000 claims description 7
- 229910052791 calcium Inorganic materials 0.000 claims description 7
- 239000007859 condensation product Substances 0.000 claims description 7
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 7
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 7
- 239000003755 preservative agent Substances 0.000 claims description 6
- 230000002335 preservative effect Effects 0.000 claims description 6
- 239000002562 thickening agent Substances 0.000 claims description 6
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 5
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- 239000004698 Polyethylene Substances 0.000 claims description 4
- ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 claims description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 4
- 229920001038 ethylene copolymer Polymers 0.000 claims description 4
- 229920000573 polyethylene Polymers 0.000 claims description 4
- 229920001296 polysiloxane Polymers 0.000 claims description 4
- 239000004302 potassium sorbate Substances 0.000 claims description 4
- 235000010241 potassium sorbate Nutrition 0.000 claims description 4
- 229940069338 potassium sorbate Drugs 0.000 claims description 4
- 239000011347 resin Substances 0.000 claims description 4
- 229920005989 resin Polymers 0.000 claims description 4
- 229960004025 sodium salicylate Drugs 0.000 claims description 4
- 229920002554 vinyl polymer Polymers 0.000 claims description 4
- 229920001285 xanthan gum Polymers 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 3
- 230000004048 modification Effects 0.000 claims description 3
- 238000012986 modification Methods 0.000 claims description 3
- HZBAVWLZSLOCFR-UHFFFAOYSA-N oxosilane Chemical compound [SiH2]=O HZBAVWLZSLOCFR-UHFFFAOYSA-N 0.000 claims description 3
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 3
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 2
- 229920000084 Gum arabic Polymers 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 2
- 241000978776 Senegalia senegal Species 0.000 claims description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 2
- 239000000205 acacia gum Substances 0.000 claims description 2
- 235000010489 acacia gum Nutrition 0.000 claims description 2
- 150000008052 alkyl sulfonates Chemical class 0.000 claims description 2
- 239000004202 carbamide Substances 0.000 claims description 2
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 2
- 229920006184 cellulose methylcellulose Polymers 0.000 claims description 2
- 239000000839 emulsion Substances 0.000 claims description 2
- 235000011187 glycerol Nutrition 0.000 claims description 2
- 229920000609 methyl cellulose Polymers 0.000 claims description 2
- 239000001923 methylcellulose Substances 0.000 claims description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 2
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 2
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 2
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 2
- 238000012372 quality testing Methods 0.000 claims description 2
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 2
- 239000004299 sodium benzoate Substances 0.000 claims description 2
- 235000010234 sodium benzoate Nutrition 0.000 claims description 2
- 229940124530 sulfonamide Drugs 0.000 claims description 2
- 150000003456 sulfonamides Chemical class 0.000 claims description 2
- 239000010408 film Substances 0.000 claims 3
- 125000001931 aliphatic group Chemical group 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 4
- 230000002070 germicidal effect Effects 0.000 abstract description 3
- 239000000575 pesticide Substances 0.000 abstract description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 abstract 4
- 229940051841 polyoxyethylene ether Drugs 0.000 abstract 4
- VJOCYCQXNTWNGC-UHFFFAOYSA-L calcium;benzenesulfonate Chemical compound [Ca+2].[O-]S(=O)(=O)C1=CC=CC=C1.[O-]S(=O)(=O)C1=CC=CC=C1 VJOCYCQXNTWNGC-UHFFFAOYSA-L 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 238000009833 condensation Methods 0.000 abstract 2
- 230000005494 condensation Effects 0.000 abstract 2
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 abstract 1
- 239000004721 Polyphenylene oxide Substances 0.000 abstract 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 abstract 1
- 238000001514 detection method Methods 0.000 abstract 1
- 238000000227 grinding Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 238000010008 shearing Methods 0.000 abstract 1
- 229910000077 silane Inorganic materials 0.000 abstract 1
- 230000008901 benefit Effects 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000003960 organic solvent Substances 0.000 description 5
- 239000004557 technical material Substances 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 229930182558 Sterol Natural products 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 230000000855 fungicidal effect Effects 0.000 description 2
- 239000000417 fungicide Substances 0.000 description 2
- 230000007226 seed germination Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 150000003432 sterols Chemical class 0.000 description 2
- 235000003702 sterols Nutrition 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 241000233866 Fungi Species 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 230000017858 demethylation Effects 0.000 description 1
- 238000010520 demethylation reaction Methods 0.000 description 1
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000009969 flowable effect Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000000361 pesticidal effect Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000009885 systemic effect Effects 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 150000003852 triazoles Chemical group 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2008100569252A CN101496513B (zh) | 2008-01-28 | 2008-01-28 | 一种苯醚甲环唑悬浮种衣剂及其制备方法 |
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CN2008100569252A CN101496513B (zh) | 2008-01-28 | 2008-01-28 | 一种苯醚甲环唑悬浮种衣剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN101496513A CN101496513A (zh) | 2009-08-05 |
CN101496513B true CN101496513B (zh) | 2012-01-04 |
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CN2008100569252A Active CN101496513B (zh) | 2008-01-28 | 2008-01-28 | 一种苯醚甲环唑悬浮种衣剂及其制备方法 |
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Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102090398A (zh) * | 2009-12-10 | 2011-06-15 | 上海市农业科学院 | 一种种子处理剂及其制备方法 |
CN102388911A (zh) * | 2011-09-28 | 2012-03-28 | 联保作物科技有限公司 | 一种悬浮种衣剂 |
CN102308838B (zh) * | 2011-09-28 | 2014-06-11 | 联保作物科技有限公司 | 一种杀虫防病悬浮种衣剂 |
CN102342284B (zh) * | 2011-11-11 | 2014-08-13 | 联保作物科技有限公司 | 一种杀菌抗病组合物及其悬浮种衣剂 |
CN102669133A (zh) * | 2012-05-21 | 2012-09-19 | 四川农业大学 | 一种预防姜瘟病的种衣剂 |
CN103181386A (zh) * | 2012-12-18 | 2013-07-03 | 江苏凯元科技有限公司 | 一种高效广谱种衣剂助剂的制备方法 |
CN106797729B (zh) * | 2017-01-24 | 2020-04-21 | 吉林省农业科学院 | 花生种皮保护剂及花生种衣剂 |
CN108477177A (zh) * | 2018-05-16 | 2018-09-04 | 安徽省四达农药化工有限公司 | 一种苯醚甲环唑悬浮种衣剂及其制备方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1726781A (zh) * | 2005-07-26 | 2006-02-01 | 河北农业大学 | 高效、低毒小麦种衣剂 |
WO2007017231A1 (en) * | 2005-08-05 | 2007-02-15 | Basf Aktiengesellschaft | Use of arylanilides for seed treatment |
-
2008
- 2008-01-28 CN CN2008100569252A patent/CN101496513B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1726781A (zh) * | 2005-07-26 | 2006-02-01 | 河北农业大学 | 高效、低毒小麦种衣剂 |
WO2007017231A1 (en) * | 2005-08-05 | 2007-02-15 | Basf Aktiengesellschaft | Use of arylanilides for seed treatment |
Non-Patent Citations (1)
Title |
---|
侯生英等.3%苯醚甲环唑悬浮种衣剂防治小麦全蚀病试验.《植物保护》.2005,(第05期),全文. * |
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Owner name: BEIJING DASHIFENG BIOTECHNOLOGY CO., LTD. JIXI AGR Effective date: 20120419 |
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Effective date of registration: 20120419 Address after: 100080 Zhongguancun street, Haidian District, Zhongguancun building, No., layer 27, 14 Co-patentee after: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Patentee after: BEIJING GREEN AGROSINO Corp. Co-patentee after: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Co-patentee after: Beijing Agrosino Import and Export Co.,Ltd. Address before: 100080 Zhongguancun street, Haidian District, Zhongguancun building, No., layer 27, 14 Patentee before: BEIJING GREEN AGROSINO Corp. |
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Address after: 100080, Zhongguancun building, No. 27 Zhongguancun street, Beijing, Haidian District, China, 14 floor Co-patentee after: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Patentee after: BEIJING GREEN AGROSINO CROP TECHNOLOGY CO.,LTD. Co-patentee after: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Co-patentee after: Beijing Agrosino Import and Export Co.,Ltd. Address before: 100080, Zhongguancun building, No. 27 Zhongguancun street, Beijing, Haidian District, China, 14 floor Co-patentee before: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Patentee before: BEIJING GREEN AGROSINO Corp. Co-patentee before: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Co-patentee before: Beijing Agrosino Import and Export Co.,Ltd. |
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Effective date of registration: 20180824 Address after: 100080, Zhongguancun building, No. 27 Zhongguancun street, Beijing, Haidian District, China, 14 floor Co-patentee after: HEBEI GREEN NONGHUA CROP TECHNOLOGY CO.,LTD. Patentee after: BEIJING GREEN AGROSINO CROP TECHNOLOGY CO.,LTD. Co-patentee after: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Address before: 100080, Zhongguancun building, No. 27 Zhongguancun street, Beijing, Haidian District, China, 14 floor Co-patentee before: BEIJING DASHIFENG BIOTECHNOLOGY Co.,Ltd. Patentee before: BEIJING GREEN AGROSINO CROP TECHNOLOGY CO.,LTD. Co-patentee before: JIXI AGROSINO BIOTECHNOLOGY CO.,LTD. Co-patentee before: Beijing Agrosino Import and Export Co.,Ltd. |
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