CN101491205A - Recovery method of waste dregs generated in Chinese patent medicine production - Google Patents

Recovery method of waste dregs generated in Chinese patent medicine production Download PDF

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CN101491205A
CN101491205A CNA2009101024430A CN200910102443A CN101491205A CN 101491205 A CN101491205 A CN 101491205A CN A2009101024430 A CNA2009101024430 A CN A2009101024430A CN 200910102443 A CN200910102443 A CN 200910102443A CN 101491205 A CN101491205 A CN 101491205A
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梁洋
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Abstract

The invention discloses a method for recycling Chinese patent medicine production waste decoction dregs. The method comprises the following steps: chopping the decoction dregs after the extraction of the Chinese medicinal plant into blocks with the length of between 4 and 6cm, packaging the blocks into a plastic bag, sealing the bag, fully decomposing the decoction dregs for 40 to 60 days, and taking the decomposed decoction dregs as a substrate for the soilless culture of Chinese medicinal plants, vegetables or fruit seedlings. Compared with the prior art, the decoction dregs can be used as the substrate for the soilless culture of the Chinese medicinal plants, vegetables or fruit seedlings after the decomposition, thereby making full use of the nutrient contents in the decoction dregs, avoiding the pollution of the Chinese medicinal plants, vegetables and fruits caused by the heavy metals and pesticides in the soil, opening up an economical cycle way for producing green Chinese medicinal plants, vegetables and fruits, and saving the land resources needed by the burying of the decoction dregs.

Description

The recoverying and utilizing method of Chinese patent medicine production waste decoction dregs
Technical field:
The present invention relates to a kind of recoverying and utilizing method of Chinese patent medicine production waste decoction dregs, belong to the waste residue of Chinese herbs processing technology field.
Background technology:
In the Chinese patent drug production process, the discharging of the dregs of a decoction and processing are the thorny problems that Chinese patent drug is produced after the medicinal material extract, and each Chinese medicine manufacturing enterprise all will discharge a large amount of dregs of a decoction every day.Because of the dregs of a decoction have in various degree pollution to environment, so often at present adopt the method for landfill to handle.According to Wudang District garbage disposal center, Guiyang statistical result showed, this local only GuiZhou WeiMen Pharmacy Co., Ltd and other once tame enterprise dregs of a decoction generation reach annual 2000 surplus ton, and the Guiyang has family surplus in the of 70 producing by the herbal pharmaceutical enterprise of GMP authentication at present.In prediction on such basis, with regard to the herbal pharmaceutical enterprise of whole Guizhou, surplus annual dregs of a decoction generation reaches 20 approximately ten thousand tons.Take the method for landfill to handle approximately 35 yuans of the costs of one ton of dregs of a decoction, herbal pharmaceutical enterprise in Guizhou Province's spends in the funds of handling on the dregs of a decoction every year and is approximately surplus the RMB 700 ten thousand yuan so.Moreover, when landfill, can take a large amount of land resources and contaminated land and underground water, because contain nutriments such as abundant organic matter, carbohydrate and thick protein etc. and trace element in the dregs of a decoction, so also can cause the waste of resource.How handling and utilize the dregs of a decoction again, be not only the problem that the pharmaceutical factory need solve, also is that people need the major issue that solves in environmental protection.
Along with the development of society, the improving constantly of living standards of the people, people are more urgent to the requirement of prevention and treatment disease, and under the trend of back to nature, the demand of traditional Chinese medicine increases greatly.The resources of natural crude drugs can't satisfy people's medication needs.And the traditional Chinese medicine cultivation, then be to plant, set up and enlarge the production measures such as enforcement of medicinal plant cultivation production base, high quality and yield cultivation techniques, under the prerequisite of not destroying natural resources by wild change is man, constantly enlarge the source of medicinal material, change the situation that supply falls short of demand.The many problems of China's traditional Chinese medicine production long-term existence, the residue of pesticide that cause as soil pollution, heavy metal severe overweight etc.This has become a big bottleneck of Chinese medicine industry development.
" traditional Chinese medicine quality of production management regulation " is the basic norm of specially traditional Chinese medicine being produced the implementation specification management (GAP).The purpose of GAP is that collateral security traditional Chinese medicine quality is set out, and control influences the various factors of quality of medicinal material, and each link and even overall process that the standard medicinal material is produced are to reach the purpose of medicinal material " safely, effectively, stable yield, steady quality, controlled ".Particularly in recent years, the measure of regulating to import Chinese medicine commodity is constantly strengthened in most countries and area---and mainly be aspect noxious materials such as heavy metal, residue of pesticide limit the quantity of.International, a domestic part of production of healthful Chinese crud drug having been regarded as in the sustainable development agricultural.
Substrate culture is a kind of mode of popularizing area maximum in the soilless culture.It is that root system with crop is fixed in the matrix of organic or inorganic, by the method for drip irrigation or trickle irrigation, supplies with crop alimentary liquid.The substrate culture buffer capacity is strong, does not have moisture, nutrient and supplies O 2Between contradiction, do not need power, so small investment, cost are low, generally adopt in the production.From China's present situation, substrate culture is a kind of soilless culture mode that realistic meaning is arranged most.
Summary of the invention:
The objective of the invention is to: the recoverying and utilizing method that a kind of Chinese patent medicine production waste decoction dregs is provided.The present invention handles the dregs of a decoction through becoming thoroughly decomposed after, be used for the soilless culture of traditional Chinese medicine, vegetables or fruit seedling as matrix, made full use of the nutrient component that the dregs of a decoction contain, avoided of the pollution of noxious materials such as heavy metal, agricultural chemicals, saved the required land resources of the landfill dregs of a decoction medicinal material, vegetables or fruit.
The present invention is achieved in that a kind of recoverying and utilizing method of Chinese patent medicine production waste decoction dregs: the dregs of a decoction chopping after traditional Chinese medicine is extracted, and in the plastic sack of packing into, sealing, the back of fully becoming thoroughly decomposed is used for the soilless culture of traditional Chinese medicine, vegetables or fruit seedling as matrix.
The aforesaid dregs of a decoction are the dregs of a decoction after a kind of, two or more traditional Chinese medicines extract.
Described dregs of a decoction chopping is to the section of 4~6cm, and the time of becoming thoroughly decomposed is 40~60 days.
Preferable methods is: the dregs of a decoction after traditional Chinese medicine is extracted shred the section to 5cm, and in the plastic sack of packing into, sealing was fully become thoroughly decomposed 50 days, and is standby as matrix; After traditional Chinese medicine, vegetables or fruit seeds are sowed, grown seedlings, transplant to the good dregs of a decoction matrix of becoming thoroughly decomposed, carry out soilless culture.
Specifically, can carry out the soilless culture of medicinal material of polygonum capilalum with the dregs of a decoction chopping of 'Relinqing ', the back of becoming thoroughly decomposed as matrix.
Also the dregs of a decoction of Liuwei Dihuang preparation and 'Relinqing ' can be shredded, become thoroughly decomposed, mix the back, carry out the soilless culture of medicinal material of polygonum capilalum as matrix.
Described 'Relinqing ' is that raw medicinal material is made with the headdress flower knotweed.
Described Liuwei Dihuang preparation is that raw medicinal material is made with prepared rhizome of rehmannia, moutan bark, Chinese yam, dogwood, rhizoma alismatis and Poria cocos.
Soilless culture to the requirement of matrix is:
(1) has a certain size solid content matter;
(2) have good physical property, matrix must be loosened, and preserve moisture and fertility is ventilative again;
(3) have stable chemical property, itself does not contain harmful ingredients, and nutrient solution is changed.
(4) require matrix to draw materials conveniently, wide material sources, cheap.
Matrix commonly used has bark, sawdust, the peat composed of rotten mosses, vermiculite, rock wool etc.The dregs of a decoction not only satisfy the requirement as matrix, the constituent analysis result shows that the dregs of a decoction also contain rich nutrient contents, pH is moderate, in pharmacy procedure, handle thereby also have water content height, aseptic characteristics through the high temperature poach, the dregs of a decoction can also carry out certain shear treatment, can reach size more uniformly, not only anchor effect is good, and gas permeability is also fine.
The inventor compares through the experimental result of carrying out soilless culture and soil cultivation with the dregs of a decoction, find that its appearance character and active constituent content are more or less the same, and soilless culture does not have residue of pesticide and heavy metal pollution.And the medicinal material planting base is very high to the requirement of soil, so often be selected in away from meagrely-populated place, city, will produce a large number of freight when transporting medicinal material, and is not easy to management.If substitute soil with the dregs of a decoction, carry out the medicinal material standardized planting the most nearby in the distance pharmaceutical factory, can not only open up new page for the medicinal material standardized planting, can also economize on the use of funds for the pharmaceutical factory.Moreover land resources is very limited, if certain plant species of plantation will make the soil nutritional deficiency on a slice soil for a long time, after by the fertilising improvement, can change the physicochemical property of soil again, thereby lose soil fertility, just can address this problem and substitute soil, and economize the land resource with the dregs of a decoction.
Compared with prior art, after the dregs of a decoction after the present invention extracts traditional Chinese medicine are handled through becoming thoroughly decomposed, be used for the soilless culture of traditional Chinese medicine, vegetables or fruit seedling as matrix, made full use of the nutrient component that the dregs of a decoction contain, avoided of the pollution of noxious materials such as heavy metal in soil, agricultural chemicals to medicinal material, vegetables or fruit, open up a road that produces the economy circulation of healthful Chinese crud drug, vegetables, fruit, and saved the required land resources of the landfill dregs of a decoction.
Description of drawings:
Fig. 1 is the HPLC collection of illustrative plates of Quercetin reference substance;
Fig. 2 is that " heat is drenched clear particle " dregs of a decoction are made the headdress flower knotweed HPLC collection of illustrative plates of substrate culture;
Fig. 3 is that " heat is drenched clear particle " dregs of a decoction mix the headdress flower knotweed HPLC collection of illustrative plates of doing substrate culture with " LIUWEIDIHUANG JIAONANG " dregs of a decoction;
Fig. 4 is the headdress flower knotweed HPLC collection of illustrative plates of soil plantation.
Embodiment:
Embodiments of the invention 1: the dregs of a decoction that heat is drenched clear particle (medicinal material of polygonum capilalum goods) shred the section to 5cm, and in the plastic sack of packing into, sealing was fully become thoroughly decomposed 50 days, and is standby.
Embodiments of the invention 2: with the section of the dregs of a decoction of LIUWEIDIHUANG JIAONANG (prepared rhizome of rehmannia, moutan bark, Chinese yam, dogwood, rhizoma alismatis and Poria cocos Six-element medicinal material are made) chopping to 4~6cm, in the plastic sack of packing into, sealing was fully become thoroughly decomposed about 50 days, and is standby.
Experimental example: the soilless culture experiment of headdress flower knotweed:
1. dregs of a decoction constituent analysis
The soil condition of suitable headdress flower knotweed growth is: loam or sand loam about fertile, loose, preserve moisture and fertility, farming bed thickness 30cm, and the pH value is 5~7, organic matter is good more than 2.5%.Therefore the inventor has carried out constituent analysis to " heat is drenched clear particle " dregs of a decoction (medicinal material of polygonum capilalum goods), " LIUWEIDIHUANG JIAONANG " dregs of a decoction (prepared rhizome of rehmannia, moutan bark, Chinese yam, dogwood, rhizoma alismatis, Poria cocos) of experiment usefulness, the results are shown in Table 1:
The constituent analysis of table 1 dregs of a decoction
Dregs of a decoction kind N(mg/kg) P(mg/kg) K(mg/kg) Organic (%) pH
Heat is drenched clear particle 1.0 594 3663 50.7 6.28
LIUWEIDIHUANG JIAONANG 2.3 1555 1830 52.0 4.95
2. the dregs of a decoction are handled
(1) " heat is drenched clear particle " dregs of a decoction are handled: see embodiment 1.
(2) " LIUWEIDIHUANG JIAONANG " dregs of a decoction are handled: see embodiment 2.
3. cultivation experiments process
(1) grows seedlings
After the headdress flower knotweed seed of choosing mixed thoroughly with fine earth, be spread on the soil, water, cover plastic film.Observed once every 3~5 days during this time, and water suitable quantity of water, keep the humidity of soil in the flowerpot, be beneficial to the sprouting of seed, the back seed germinates successively about 15 days, according to germination density, removes the part seedling, cultivates strong sprout.Treat headdress flower knotweed seedling length to 7~when 8cm is high, can transplant.
(2) transplant
Put into different substrates (grouping sees Table 2) in flowerpot, headdress flower knotweed seedling is transplanted respectively to flowerpot, an amount of running water is watered in every basin 2~4 strains.
Table 2 flowerpot mesostroma kind
Numbering 1 2 3
Matrix species " heat is drenched clear particle " dregs of a decoction (becoming thoroughly decomposed) " heat the is drenched clear particle " dregs of a decoction and " LIUWEIDIHUANG JIAONANG " dregs of a decoction (becoming thoroughly decomposed) (1: 1) Soil
(3) management
Observe once each weekend during this time, and water suitable quantity of water, keep the humidity of flowerpot mesostroma, and record headdress flower knotweed upgrowth situation.
(4) gather and preliminary working
Medicinal material of polygonum capilalum to cultivation is gathered, and 50 ℃ of oven dry in baking oven, headdress flower knotweed sample is delivered to GuiZhou WeiMen Pharmacy Co., Ltd test, and whether the medicinal material of investigating cultivation meets standard.
4. cultivation experiments result
Assay shows that its appearance character and active constituent content meet the demands, and the results are shown in Figure 1, Fig. 2, Fig. 3 and table 3, table 4.
Table 3 headdress flower knotweed quality testing result
Numbering Proterties Water content (%) Quercetin (%)
1 Stem is thick, leaf plumpness, aubergine, pollen redness, section hollow.The inflorescence head.Gas is little, mildly bitter flavor, puckery. 9.98 0.51
2 Stem is thick, leaf plumpness, aubergine, pollen redness, section hollow.The inflorescence head.Gas is little, mildly bitter flavor, puckery. 11.55 0.52
3 Stem is thick, leaf plumpness, aubergine or light green color, pollen redness, section hollow.The inflorescence head.Gas is little, mildly bitter flavor, puckery. 11.55 0.60
Table 4 residue of pesticide, determining heavy metals result
Figure A20091010244300071
By above-mentioned cultivation experiments, draw following result:
1. make matrix with " heat drench clear particle " dregs of a decoction or mix the headdress flower knotweed growing way of doing substrate culture and, grow fine with being more or less the same of soil cultivation with " LIUWEIDIHUANG JIAONANG " dregs of a decoction and " heat is drenched clear particle " dregs of a decoction.
2. Zai Pei medicinal material detects through GuiZhou WeiMen Pharmacy Co., Ltd, and its appearance character and content all meet " Guizhou Province's traditional Chinese medicine, national quality of medicinal material standard " (version in 2003) requirement.
Conclusion: it is feasible carrying out the soilless culture traditional Chinese medicine with the dregs of a decoction as matrix.

Claims (8)

1. the recoverying and utilizing method of a Chinese patent medicine production waste decoction dregs is characterized in that: the dregs of a decoction after the traditional Chinese medicine extraction are shredded, in the plastic sack of packing into, seal, as matrix, be used for the soilless culture of traditional Chinese medicine, vegetables or fruit seedling after fully becoming thoroughly decomposed.
2. according to the recoverying and utilizing method of the described Chinese patent medicine production waste decoction dregs of claim 1, it is characterized in that: the described dregs of a decoction are the dregs of a decoction after a kind of, two or more traditional Chinese medicines extract.
3. according to the recoverying and utilizing method of claim 1 or 2 described Chinese patent medicine production waste decoction dregs, it is characterized in that: dregs of a decoction chopping is to the section of 4~6cm, and the time of becoming thoroughly decomposed is 40~60 days.
4. according to the recoverying and utilizing method of the described Chinese patent medicine production waste decoction dregs of claim 3, it is characterized in that: the dregs of a decoction after traditional Chinese medicine is extracted shred the section to 5cm, and in the plastic sack of packing into, sealing was fully become thoroughly decomposed 50 days, and is standby as matrix; After traditional Chinese medicine, vegetables or fruit seeds are sowed, grown seedlings, transplant to the good dregs of a decoction matrix of becoming thoroughly decomposed, carry out soilless culture.
5. according to the recoverying and utilizing method of the described Chinese patent medicine production waste decoction dregs of claim 4, it is characterized in that: the soilless culture of medicinal material of polygonum capilalum as matrix, is carried out in the dregs of a decoction chopping of 'Relinqing ', the back of becoming thoroughly decomposed.
6. according to the recoverying and utilizing method of the described Chinese patent medicine production waste decoction dregs of claim 4, it is characterized in that: the dregs of a decoction of Liuwei Dihuang preparation and 'Relinqing ' are shredded, become thoroughly decomposed, mix the back, carry out the soilless culture of medicinal material of polygonum capilalum as matrix.
7. according to the recoverying and utilizing method of claim 5 or 6 described Chinese patent medicine production waste decoction dregs, it is characterized in that: described 'Relinqing ' is that raw medicinal material is made with the headdress flower knotweed.
8. according to the recoverying and utilizing method of the described Chinese patent medicine production waste decoction dregs of claim 6, it is characterized in that: described Liuwei Dihuang preparation is that raw medicinal material is made with prepared rhizome of rehmannia, moutan bark, Chinese yam, dogwood, rhizoma alismatis and Poria cocos.
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101768453B (en) * 2010-01-25 2013-07-03 哈尔滨工业大学 Innocent treatment method for traditional Chinese medicinal dregs
CN104429557A (en) * 2014-12-22 2015-03-25 中国林业科学研究院亚热带林业研究所 Soapberry cutting seedling method
CN105036932A (en) * 2015-07-27 2015-11-11 太仓市王秀粮食生产专业合作社 Ecological organic fertilizer
CN106316563A (en) * 2015-07-11 2017-01-11 镇江贝思特有机活性肥料有限公司 Rice seedling raising substrate produced from licorice root decoction dregs and preparation method thereof
CN111345219A (en) * 2020-03-25 2020-06-30 贵州弘康药业有限公司 Special base fertilizer for planting polygonum capitatum and fertilizing method
CN111373990A (en) * 2020-03-25 2020-07-07 贵州弘康药业有限公司 Polygonum capitatum planting method
CN111373989A (en) * 2020-03-25 2020-07-07 贵州弘康药业有限公司 Method for planting polygonum capitatum by taking herb residues as base fertilizer

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101768453B (en) * 2010-01-25 2013-07-03 哈尔滨工业大学 Innocent treatment method for traditional Chinese medicinal dregs
CN104429557A (en) * 2014-12-22 2015-03-25 中国林业科学研究院亚热带林业研究所 Soapberry cutting seedling method
CN106316563A (en) * 2015-07-11 2017-01-11 镇江贝思特有机活性肥料有限公司 Rice seedling raising substrate produced from licorice root decoction dregs and preparation method thereof
CN105036932A (en) * 2015-07-27 2015-11-11 太仓市王秀粮食生产专业合作社 Ecological organic fertilizer
CN111345219A (en) * 2020-03-25 2020-06-30 贵州弘康药业有限公司 Special base fertilizer for planting polygonum capitatum and fertilizing method
CN111373990A (en) * 2020-03-25 2020-07-07 贵州弘康药业有限公司 Polygonum capitatum planting method
CN111373989A (en) * 2020-03-25 2020-07-07 贵州弘康药业有限公司 Method for planting polygonum capitatum by taking herb residues as base fertilizer

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