CN101461564B - Tar-reducing flavour intensifier of fire-cured tobacco as well as preparation method and use method thereof - Google Patents
Tar-reducing flavour intensifier of fire-cured tobacco as well as preparation method and use method thereof Download PDFInfo
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- CN101461564B CN101461564B CN2008100491741A CN200810049174A CN101461564B CN 101461564 B CN101461564 B CN 101461564B CN 2008100491741 A CN2008100491741 A CN 2008100491741A CN 200810049174 A CN200810049174 A CN 200810049174A CN 101461564 B CN101461564 B CN 101461564B
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Abstract
The invention discloses a tar lowering aroma adding agent for cured tobacco leaf, preparation and use method thereof. The cured tobacco leaf tar lowering aroma adding agent includes 1-2 by weight parts of cured tobacco leaf tar lowering agent, 1-3 by weight parts of cured tobacco leaf aroma adding agent, 5-10 by weight parts of moist keeping agent. The cured tobacco leaf tar lowering aroma adding agent is capable of reducing tar content in the cigarette fume, reducing harmful gas CO, which is added into the tobacco leaf to make the fragrance more special. The tar lowering aroma adding agent is simple in preparation, low in production cost, easy for production.
Description
Technical field
The present invention relates to a kind of cured tobacco leaf additive, be specifically related to a kind of cigarette additive and preparation method thereof and using method that tar content has the flavouring effect that reduce.
Background technology
Tar is the product of incomplete combustion in the cigarette smoking process, the extremely complicated mixture such as oxide, sulfide and nitride that comprises hydro carbons, hydrocarbon, wherein multiple carcinogen and short cancer materials such as phenol, fumaric acid such as BaP, cadmium, arsenic, beta-naphthylamine, nitrosamine and radio isotope, though its amount is atomic, often have, repeatedly, long-term summation.American Cancer Society points out: it is 5 times of non-smoker that smoking every day is less than chance that 10 smoker suffers from lung cancer, if smoking every day then is 20 times more than 2 bags.Every year is died from lung cancer person up to 1,000,000 people in the whole world, and wherein 90% is directly caused by smoking.
Smoking and health are one of main challenges of facing of tobacco business, and the 50-60 age in last century has caused that countries in the world generally pay attention to.China after the eighties especially reducing tar and reducing harm as main research topic.Reducing the method that tar in the cigarette smoke and harmful components thereof adopt usually has: (1) directly adds absorption and falls burnt additive in filter tip or pipe tobacco, remove bad smell, reduces harmful substance.Chinese patent 93102104.9 discloses in the middle of tow that a kind of adsorbent that crude drug is made with medical stone processing is added on filter tip, the silk ribbon, is combined into the method for dual filter cigarette with the acetate fiber filter tip.Chinese patent 200610032237.3 has been reported a kind of cigarette additives with reducing poison function, is the sol system that is become with polyvinyl alcohol or organic carboxyl acid complexing by inorganic salts.(2) part of burnt Chinese herbal medicine as pipe tobacco can fall in interpolation in pipe tobacco, or adds the plant extracts that can reduce tar content.Disclose the cigarette method for making of adding ginkgo leaf in tobacco leaf such as Chinese patent 98119469.9, Chinese patent 01101963.8 cigarette falls toxic agent and then relates to Wen Guanli, honeysuckle, perilla leaf, bluish dogbane etc.
According to China's national standard, tar content can come into the market less than 15mg in every cigarette.Along with the raising of people's living standard, reducing tar and reducing harm has become international main trend.But present fall burnt measure and then have reduction with releasing content of coke tar, physiological strength and fragrance weaken.
Summary of the invention
The objective of the invention is to utilize to have the Chinese herbal medicine active ingredient that reduces tar content, join can increase the tsaoko class plant component of smoke perfume, provide a kind of and can reduce the cured tobacco leaf tar content, can protect fragrant tar lowering aroma adding agent again.
Another object of the present invention provides that a kind of extraction efficiency height, speed are fast, pollution-free, the preparation method of the simple tar lowering aroma adding agent of technology.
The present invention also aims to provide a kind of using method of tar lowering aroma adding agent of the present invention.
To achieve these goals, the technical solution used in the present invention is:
Tar lowering aroma adding agent comprises cured tobacco leaf tar-reducing agent 1～2 weight portion, cured tobacco leaf fumet 1～3 weight portion, humectant 5～10 weight portions.
Cured tobacco leaf tar-reducing agent in the tar lowering aroma adding agent is mainly by cordate houttuynia 0.5～2.0 weight portion, wild sole of the foot grass 0.5～2.0 weight portion, and Chinese lobelia 1～4 weight portion, honeysuckle 1～4 weight portion is made.The cured tobacco leaf fumet is mainly by Radix Acanthopanacis Senticosi root 1.0～1.5 weight portions, siberian rose 1.0～1.5 weight portions, and vanilla beanpod 2.0～2.5 weight portions, ladanum branches and leaves 2.0～2.5 weight portions are made.Humectant is made up of the propane diols of 0.5～2.0 weight portion and the compound corn syrup of 1～4 weight portion.
The preparation method of the cured tobacco leaf tar-reducing agent in tar lowering aroma adding agent step as follows carries out:
(1) respectively with cordate houttuynia, wild sole of the foot grass, Chinese lobelia is dried and is cut into broken section, honeysuckle is made fragment, will be through 0.5～2.0 weight portion of the cordate houttuynia after the above-mentioned processing, wild sole of the foot grass 0.5～2.0 weight portion, Chinese lobelia 1～4 weight portion, honeysuckle 1～4 weight portion is put into ceramic vessel, the water that adds 40 ℃, amount of water is 2.5～3.0 times of raw material gross weight, presses raw material 0.3～0.5% addition and adds cellulase, put into 40 ℃ of insulations of incubator 1 hour, taking-up is placed on heats 1～3 minute in the micro-wave oven, filter, and collects filtrate and leaves standstill 24 hours, discard precipitation, obtain supernatant.
(2) with 1.0～1.5 weight portion Monosodium Edetate salt, 1.5～2.0 weight portion potassium malates, 1.5 it is abundant mixing in the supernatant that obtains of 1.5～2.0 times step (1) of above-mentioned three kinds of material gross weights that～2.0 weight portion dipotassium glycyrrhizinates are dissolved in weight, obtains the cured tobacco leaf tar-reducing agent.
The preparation method of the cured tobacco leaf fumet in tar lowering aroma adding agent step as follows carries out:
(1) Radix Acanthopanacis Senticosi root is run through section and dry, siberian rose dries section, and the vanilla beanpod was pulverized 20 mesh sieves and made meal, and the ladanum branches and leaves are made fragment; Will be through 1.0～1.5 weight portions of the Radix Acanthopanacis Senticosi root after the above-mentioned processing, siberian rose 1.0～1.5 weight portions, vanilla beanpod 2.0～2.5 weight portions, ladanum branches and leaves 2.0～2.5 weight portions are put into supercritical CO
2In the fluid extraction device, add ethanol for guiding and supporting agent, the addition of ethanol is 7～9% of a raw material weight, at extracting pressure 20～50Mpa, 30～60 ℃ of following cycling extractions of extraction temperature 1～3 hour, the plant extraction liquid that obtains left standstill 24 hours, discard precipitation, obtain supernatant.
(2) with 2.0～2.5 weight portion isovaleric acid, 1.5～2.0 weight portion Beta-methyl valeric acids, 1.0～1.5 weight portion alpha-angelica lactones are dissolved in weight and are in the supernatant that the step (1) of 1.5～2.0 times of above-mentioned three kinds of material gross weights obtains fully mixing, obtain the cured tobacco leaf fumet.
Humectant in the tar lowering aroma adding agent is by mixed the getting of compound corn syrup of the propane diols and 1～4 weight portion of 0.5～2.0 weight portion.
The preparation method of tar lowering aroma adding agent: cured tobacco leaf tar-reducing agent 1～2 weight portion, cured tobacco leaf fumet 1～3 weight portion, humectant 5～10 weight portions are mixed and obtain tar lowering aroma adding agent.
The using method of tar lowering aroma adding agent: the tar lowering aroma adding agent of per 1 weight portion is dissolved the water dilution of back with 3～5 weight portions with the ethanol of 2～3 weight portions; The delicate fragrance type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and the tar lowering aroma adding agent dilution is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 15～30 days; The tar lowering aroma adding agent addition is that the sheet cigarette of per 1000 weight portions adds tar lowering aroma adding agent 7～15 weight portions.
Tar lowering aroma adding agent of the present invention has following advantage: evenly be sprayed at after (1) dilutes tar lowering aroma adding agent of the present invention and carry out redrying on the cured tobacco leaf, the tar content in the cigarette smoke can be reduced, and the pernicious gas CO (seeing the following form) in the flue gas can be reduced.(2) tar lowering aroma adding agent of the present invention is added on and can makes its delicate fragrance style more outstanding in the tobacco leaf.(3) preparation method's technology of tar lowering aroma adding agent of the present invention is simple, and production cost is low, is easy to realize producing.
| Interventions Requested | Assay |
| Average resistance to suction (Pa/ props up) TPM (mg/ props up) moisture content (mg/ props up) nicotine content in smoke (mg/ props up) tar content (mg/ props up) puff number of average weight (g/ props up) (mouthful /) CO content (mg/ props up) | 0.833 1072 4.62 0.25 0.32 4.1 5.9 6.2 |
Description of drawings
Accompanying drawing is a tar lowering aroma adding agent preparation method's of the present invention process chart.
The specific embodiment
Below by embodiment the present invention is elaborated.
Embodiment 1
One, the preparation of tar lowering aroma adding agent
1. the preparation method of cured tobacco leaf tar-reducing agent
(1) respectively with cordate houttuynia, wild sole of the foot grass, Chinese lobelia is dried and is cut into broken section, and honeysuckle is made fragment, gets material by following weight proportion then:
Cordate houttuynia 0.5 weight portion
Wild sole of the foot grass 0.5 weight portion
Chinese lobelia 1 weight portion
Honeysuckle 1 weight portion
The raw material of above-mentioned weight portion is put into ceramic vessel, 40 ℃ of water that add 2.5 times of amounts of raw material weight (7.5 weight portion), press raw material 0.3% (0.009 weight portion) addition and add cellulase, put into temperature and be 40 ℃ haybox cooking 1 hour, taking-up is placed in the micro-wave oven heated 1 minute, filtered, and collected filtrate and left standstill 24 hours, discard precipitation, obtain supernatant.
(2) with 1.0 weight portion Monosodium Edetate salt, 1.5 weight portion potassium malates, 1.5 weight portion dipotassium glycyrrhizinates are dissolved in the supernatant that above-mentioned 1.5 times of amount (6 weight portion) steps of three kinds of material gross weights (1) obtain fully mixing, obtain the cured tobacco leaf tar-reducing agent.
2. the preparation method of cured tobacco leaf fumet
(1) Radix Acanthopanacis Senticosi root is run through section and dry, siberian rose dries section, and the vanilla beanpod was pulverized 20 mesh sieves and made meal, and the ladanum branches and leaves are made fragment; Get material by following weight proportion then:
Radix Acanthopanacis Senticosi root 1.0 weight portions
Siberian rose 1.0 weight portions
Vanilla beanpod 2.0 weight portions,
Ladanum branches and leaves 2.0 weight portions
The raw material of above-mentioned weight portion is put into supercritical CO
2In the fluid extraction device, the ethanol that adds raw material weight 7% (0.42 weight portion) is for guiding and supporting agent, at extracting pressure 20Mpa, and 30 ℃ of following cycling extractions of extraction temperature 1 hour, the plant extraction liquid that obtains left standstill 24 hours, discarded precipitation, the acquisition supernatant.
(2) with 2.0 weight portion isovaleric acid, 1.5 weight portion Beta-methyl valeric acids, 1.0 weight portion alpha-angelica lactones are dissolved in the supernatant that the step (1) of above-mentioned three kinds of material gross weights 1.5 times (6.75 weight portions) obtains fully mixing, obtain the cured tobacco leaf fumet.
3. the preparation method of humectant
With the propane diols of 0.5 weight portion and the mixed humectant that gets of compound corn syrup of 3 weight portions.
4. the preparation method of tar lowering aroma adding agent
Cured tobacco leaf tar-reducing agent 1 weight portion, cured tobacco leaf fumet 1 weight portion, humectant 7 weight portions that said method is made mix and obtain tar lowering aroma adding agent.
Two, the using method of tar lowering aroma adding agent
The tar lowering aroma adding agent of per 1 weight portion is dissolved the water dilution of back with 4 weight portions with the ethanol of 2 weight portions; The delicate fragrance type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and the tar lowering aroma adding agent dilution is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 15 days; The tar lowering aroma adding agent addition is that the sheet cigarette of per 1000 weight portions adds tar lowering aroma adding agent 15 weight portions.
Embodiment 2
One, the preparation of tar lowering aroma adding agent
1. the preparation method of cured tobacco leaf tar-reducing agent
(1) respectively with cordate houttuynia, wild sole of the foot grass, Chinese lobelia is dried and is cut into broken section, and honeysuckle is made fragment, gets material by following weight proportion then:
Cordate houttuynia 0.7 weight portion
Wild sole of the foot grass 1.0 weight portions
Chinese lobelia 3.5 weight portions
Honeysuckle 2 weight portions
The raw material of above-mentioned weight portion is put into ceramic vessel, 40 ℃ of water that add 2.6 times of amounts of raw material weight (18.72 weight portion), press raw material 0.35% (0.025 weight portion) addition and add cellulase, put into temperature and be 40 ℃ haybox cooking 1 hour, taking-up is placed in the micro-wave oven heated 2 minutes, filtered, and collected filtrate and left standstill 24 hours, discard precipitation, obtain supernatant.
(2) with 1.1 weight portion Monosodium Edetate salt, 1.9 weight portion potassium malate, 1.6 the weight portion dipotassium glycyrrhizinate is dissolved in the supernatant that above-mentioned 1.6 times of amount (7.36 weight portion) steps of three kinds of material gross weights (1) obtain fully mixing, obtains the cured tobacco leaf tar-reducing agent.
2. the preparation method of cured tobacco leaf fumet
(1) Radix Acanthopanacis Senticosi root is run through section and dry, siberian rose dries section, and the vanilla beanpod was pulverized 20 mesh sieves and made meal, and the ladanum branches and leaves are made fragment; Get material by following weight proportion then:
Radix Acanthopanacis Senticosi root 1.1 weight portions
Siberian rose 1.5 weight portions
Vanilla beanpod 2.1 weight portions,
Ladanum branches and leaves 2.4 weight portions
The raw material of above-mentioned weight portion is put into supercritical CO
2In the fluid extraction device, the ethanol that adds raw material weight 8% (0.57 weight portion) is for guiding and supporting agent, at extracting pressure 25Mpa, and 35 ℃ of following cycling extractions of extraction temperature 2.5 hours, the plant extraction liquid that obtains left standstill 24 hours, discarded precipitation, the acquisition supernatant.
(2) with 2.1 weight portion isovaleric acid, 2.0 weight portion Beta-methyl valeric acids, 1.3 weight portion alpha-angelica lactones are dissolved in the supernatant that the step (1) of above-mentioned three kinds of material gross weights 1.6 times (8.64 weight portions) obtains fully mixing, obtain the cured tobacco leaf fumet.
3. the preparation method of humectant
With the propane diols of 0.6 weight portion and the mixed humectant that gets of compound corn syrup of 2.5 weight portions.
4. the preparation method of tar lowering aroma adding agent
Cured tobacco leaf tar-reducing agent 1.2 weight portions that said method is made, cured tobacco leaf fumet 1.5 weight portions, the mixed tar lowering aroma adding agent that evenly obtains of humectant 8 weight portions.
Two, the using method of tar lowering aroma adding agent
The tar lowering aroma adding agent of per 1 weight portion is dissolved the water dilution of back with 4.2 weight portions with the ethanol of 2.2 weight portions; The delicate fragrance type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and the tar lowering aroma adding agent dilution is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 18 days; The tar lowering aroma adding agent addition is that the sheet cigarette of per 1000 weight portions adds tar lowering aroma adding agent 14 weight portions.
Embodiment 3
One, the preparation of tar lowering aroma adding agent
1. the preparation method of cured tobacco leaf tar-reducing agent
(1) respectively with cordate houttuynia, wild sole of the foot grass, Chinese lobelia is dried and is cut into broken section, and honeysuckle is made fragment, gets material by following weight proportion then:
Cordate houttuynia 1.0 weight portions
Wild sole of the foot grass 1.5 weight portions
Chinese lobelia 2.5 weight portions
Honeysuckle 1.5 weight portions
The raw material of above-mentioned weight portion is put into ceramic vessel, 40 ℃ of water that add 2.7 times of amounts of raw material weight (17.55 weight portion), press raw material 0.4% (0.026 weight portion) addition and add cellulase, put into 40 ℃ of insulations of incubator 1 hour, taking-up is placed in the micro-wave oven heated 3 minutes, filtered, and collected filtrate and left standstill 24 hours, discard precipitation, obtain supernatant.
(2) with 1.3 weight portion Monosodium Edetate salt, 1.7 weight portion potassium malate, 1.8 the weight portion dipotassium glycyrrhizinate is dissolved in the supernatant that above-mentioned 1.8 times of amount (8.64 weight portion) steps of three kinds of material gross weights (1) obtain fully mixing, obtains the cured tobacco leaf tar-reducing agent.
2. the preparation method of cured tobacco leaf fumet
(1) Radix Acanthopanacis Senticosi root is run through section and dry, siberian rose dries section, and the vanilla beanpod was pulverized 20 mesh sieves and made meal, and the ladanum branches and leaves are made fragment; Get material by following weight proportion then:
Radix Acanthopanacis Senticosi root 1.3 weight portions
Siberian rose 1.3 weight portions
Vanilla beanpod 2.3 weight portions,
Ladanum branches and leaves 2.3 weight portions
The raw material of above-mentioned weight portion is put into supercritical CO
2In the fluid extraction device, the ethanol that adds raw material weight 9% (0.65 weight portion) is for guiding and supporting agent, at extracting pressure 30Mpa, and 40 ℃ of following cycling extractions of extraction temperature 2 hours, the plant extraction liquid that obtains left standstill 24 hours, discarded precipitation, the acquisition supernatant.
(2) with 2.4 weight portion isovaleric acid, 1.7 weight portion Beta-methyl valeric acids, 1.5 weight portion alpha-angelica lactones are dissolved in the supernatant that the step (1) of above-mentioned three kinds of material gross weights 1.8 times (10.08 weight portions) obtains fully mixing, obtain the cured tobacco leaf fumet.
3. the preparation method of humectant
With the propane diols of 1 weight portion and the mixed humectant that gets of compound corn syrup of 1 weight portion.
4. the preparation method of tar lowering aroma adding agent
Cured tobacco leaf tar-reducing agent 1.4 weight portions, cured tobacco leaf fumet 2 weight portions, humectant 10 weight portions that said method is made mix and obtain tar lowering aroma adding agent.
Two, the using method of tar lowering aroma adding agent
The tar lowering aroma adding agent of per 1 weight portion is dissolved the water dilution of back with 3.5 weight portions with the ethanol of 2.5 weight portions; The delicate fragrance type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and the tar lowering aroma adding agent dilution is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 20 days; The tar lowering aroma adding agent addition is that the sheet cigarette of per 1000 weight portions adds tar lowering aroma adding agent 12 weight portions.
Embodiment 4
One, the preparation of tar lowering aroma adding agent
1. the preparation method of cured tobacco leaf tar-reducing agent
(1) respectively with cordate houttuynia, wild sole of the foot grass, Chinese lobelia is dried and is cut into broken section, and honeysuckle is made fragment, gets material by following weight proportion then:
Cordate houttuynia 1.2 weight portions
Wild sole of the foot grass 1.8 weight portions
Chinese lobelia 2.0 weight portions
Honeysuckle 2.5 weight portions
The raw material of above-mentioned weight portion is put into ceramic vessel, 40 ℃ of water that add 2.8 times of amounts of raw material weight (21 weight portion), press raw material 0.45% (0.034 weight portion) addition and add cellulase, put into temperature and be 40 ℃ haybox cooking 1 hour, taking-up is placed in the micro-wave oven heated 1.5 minutes, filtered, and collected filtrate and left standstill 24 hours, discard precipitation, obtain supernatant.
(2) with 1.4 weight portion Monosodium Edetate salt, 1.6 weight portion potassium malate, 1.9 the weight portion dipotassium glycyrrhizinate is dissolved in the supernatant that above-mentioned 1.9 times of amount (9.31 weight portion) steps of three kinds of material gross weights (1) obtain fully mixing, obtains the cured tobacco leaf tar-reducing agent.
2. the preparation method of cured tobacco leaf fumet
(1) Radix Acanthopanacis Senticosi root is run through section and dry, siberian rose dries section, and the vanilla beanpod was pulverized 20 mesh sieves and made meal, and the ladanum branches and leaves are made fragment; Get material by following weight proportion then:
Radix Acanthopanacis Senticosi root 1.4 weight portions
Siberian rose 1.2 weight portions
Vanilla beanpod 2.2 weight portions,
Ladanum branches and leaves 2.1 weight portions
The raw material of above-mentioned weight portion is put into supercritical CO
2In the fluid extraction device, the ethanol that adds raw material weight 8.5% (0.59 weight portion) is for guiding and supporting agent, at extracting pressure 35Mpa, and 45 ℃ of following cycling extractions of extraction temperature 2.2 hours, the plant extraction liquid that obtains left standstill 24 hours, discarded precipitation, the acquisition supernatant.
(2) with 2.5 weight portion isovaleric acid, 1.6 weight portion Beta-methyl valeric acids, 1.4 weight portion alpha-angelica lactones are dissolved in the supernatant that the step (1) of above-mentioned three kinds of material gross weights 1.9 times (10.45 weight portions) obtains fully mixing, obtain the cured tobacco leaf fumet.
3. the preparation method of humectant
With the propane diols of 1.5 weight portions and the mixed humectant that gets of compound corn syrup of 2.0 weight portions.
4. the preparation method of tar lowering aroma adding agent
Cured tobacco leaf tar-reducing agent 1.6 weight portions, cured tobacco leaf fumet 2 weight portions, humectant 6 weight portions that said method is made mix and obtain tar lowering aroma adding agent.
Two, the using method of tar lowering aroma adding agent
The tar lowering aroma adding agent of per 1 weight portion is dissolved the water dilution of back with 5 weight portions with the ethanol of 2.6 weight portions; The delicate fragrance type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and the tar lowering aroma adding agent dilution is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 25 days; The tar lowering aroma adding agent addition is that the sheet cigarette of per 1000 weight portions adds tar lowering aroma adding agent 10 weight portions.
Embodiment 5
One, the preparation of tar lowering aroma adding agent
1. the preparation method of cured tobacco leaf tar-reducing agent
(1) respectively with cordate houttuynia, wild sole of the foot grass, Chinese lobelia is dried and is cut into broken section, and honeysuckle is made fragment, gets material by following weight proportion then:
Cordate houttuynia 1.5 weight portions
Wild sole of the foot grass 1.2 weight portions
Chinese lobelia 1.5 weight portions
Honeysuckle 3.5 weight portions
The raw material of above-mentioned weight portion is put into ceramic vessel, 40 ℃ of water that add 2.9 times of amounts of raw material weight (22.33 weight portion), press raw material 0.5% (0.039 weight portion) addition and add cellulase, put into temperature and be 40 ℃ haybox cooking 1 hour, taking-up is placed in the micro-wave oven heated 2.5 minutes, filtered, and collected filtrate and left standstill 24 hours, discard precipitation, obtain supernatant.
(2) with 1.2 weight portion Monosodium Edetate salt, 1.8 weight portion potassium malate, 1.7 the weight portion dipotassium glycyrrhizinate is dissolved in the supernatant that above-mentioned 1.7 times of amount (7.99 weight portion) steps of three kinds of material gross weights (1) obtain fully mixing, obtains the cured tobacco leaf tar-reducing agent.
2. the preparation method of cured tobacco leaf fumet
(1) Radix Acanthopanacis Senticosi root is run through section and dry, siberian rose dries section, and the vanilla beanpod was pulverized 20 mesh sieves and made meal, and the ladanum branches and leaves are made fragment; Get material by following weight proportion then:
Radix Acanthopanacis Senticosi root 1.2 weight portions
Siberian rose 1.4 weight portions
Vanilla beanpod 2.4 weight portions,
Ladanum branches and leaves 2.2 weight portions
The raw material of above-mentioned weight portion is put into supercritical CO
2In the fluid extraction device, the ethanol that adds raw material weight 7.5% (0.54 weight portion) is for guiding and supporting agent, at extracting pressure 50Mpa, and 50 ℃ of following cycling extractions of extraction temperature 1.5 hours, the plant extraction liquid that obtains left standstill 24 hours, discarded precipitation, the acquisition supernatant.
(2) with 2.2 weight portion isovaleric acid, 1.8 weight portion Beta-methyl valeric acids, 1.1 weight portion alpha-angelica lactones are dissolved in the supernatant that the step (1) of above-mentioned three kinds of material gross weights 1.7 times (8.67 weight portions) obtains fully mixing, obtain the cured tobacco leaf fumet.
3. the preparation method of humectant
With the propane diols of 1.8 weight portions and the mixed humectant that gets of compound corn syrup of 3.5 weight portions.
4. the preparation method of tar lowering aroma adding agent
Cured tobacco leaf tar-reducing agent 1.8 weight portions, cured tobacco leaf fumet 3 weight portions, humectant 5 weight portions that said method is made mix and obtain tar lowering aroma adding agent.
Two, the using method of tar lowering aroma adding agent
The tar lowering aroma adding agent of per 1 weight portion is dissolved the water dilution of back with 3.8 weight portions with the ethanol of 2.8 weight portions; The delicate fragrance type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and the tar lowering aroma adding agent dilution is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 28 days; The tar lowering aroma adding agent addition is that the sheet cigarette of per 1000 weight portions adds tar lowering aroma adding agent 8 weight portions.
Embodiment 6
One, the preparation of tar lowering aroma adding agent
1. the preparation method of cured tobacco leaf tar-reducing agent
(1) respectively with cordate houttuynia, wild sole of the foot grass, Chinese lobelia is dried and is cut into broken section, and honeysuckle is made fragment, gets material by following weight proportion then:
Cordate houttuynia 2 weight portions
Wild sole of the foot grass 2 weight portions
Chinese lobelia 4 weight portions
Honeysuckle 4 weight portions
The raw material of above-mentioned weight portion is put into ceramic vessel, 40 ℃ of water that add 3 times of amounts of raw material weight (36 weight portion), press raw material 0.38% (0.046 weight portion) addition and add cellulase, put into temperature and be 40 ℃ haybox cooking 1 hour, taking-up is placed in the micro-wave oven heated 2.8 minutes, filtered, and collected filtrate and left standstill 24 hours, discard precipitation, obtain supernatant.
(2) with 1.5 weight portion Monosodium Edetate salt, 2 weight portion potassium malates, 2 weight portion dipotassium glycyrrhizinates are dissolved in the supernatant that above-mentioned 2 times of amount (11 weight portion) steps of three kinds of material gross weights (1) obtain fully mixing, obtain the cured tobacco leaf tar-reducing agent.
2. the preparation method of cured tobacco leaf fumet
(1) Radix Acanthopanacis Senticosi root is run through section and dry, siberian rose dries section, and the vanilla beanpod was pulverized 20 mesh sieves and made meal, and the ladanum branches and leaves are made fragment; Get material by following weight proportion then
Radix Acanthopanacis Senticosi root 1.5 weight portions
Siberian rose 1.5 weight portions
Vanilla beanpod 2.5 weight portions,
Ladanum branches and leaves 2.5 weight portions
The raw material of above-mentioned weight portion is put into supercritical CO
2In the fluid extraction device, the ethanol that adds raw material weight 7.9% (0.63 weight portion) is for guiding and supporting agent, at extracting pressure 40Mpa, and 60 ℃ of following cycling extractions of extraction temperature 3 hours, the plant extraction liquid that obtains left standstill 24 hours, discarded precipitation, the acquisition supernatant.
(2) with 2.3 weight portion isovaleric acid, 2.0 weight portion Beta-methyl valeric acids, 1.5 weight portion alpha-angelica lactones are dissolved in the supernatant that the step (1) of above-mentioned three kinds of material gross weights 2 times (11.6 weight portions) obtains fully mixing, obtain the cured tobacco leaf fumet.
3. the preparation method of humectant
With the propane diols of 2 weight portions and the mixed humectant that gets of compound corn syrup of 4 weight portions.
4. the preparation method of tar lowering aroma adding agent
Cured tobacco leaf tar-reducing agent 2 weight portions, cured tobacco leaf fumet 1.8 weight portions, humectant 9 weight portions that said method is made mix and obtain tar lowering aroma adding agent.
Two, the using method of tar lowering aroma adding agent
The tar lowering aroma adding agent of per 1 weight portion is dissolved the water dilution of back with 4.5 weight portions with the ethanol of 3 weight portions; The delicate fragrance type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and the tar lowering aroma adding agent dilution is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 30 days; The tar lowering aroma adding agent addition is that the sheet cigarette of per 1000 weight portions adds tar lowering aroma adding agent 7 weight portions.
Embodiment 7
One, the preparation of tar lowering aroma adding agent
1. the preparation of cured tobacco leaf tar-reducing agent: the preparation method who repeats embodiment 1 obtains the cured tobacco leaf tar-reducing agent.
2. the preparation of cured tobacco leaf fumet: the preparation method who repeats embodiment 1 obtains the cured tobacco leaf fumet.
3. the preparation of humectant: the preparation method who repeats embodiment 1 obtains humectant.
4. the preparation of tar lowering aroma adding agent: the preparation method who repeats embodiment 1 obtains falling burnt fumet.
Two, the using method of tar lowering aroma adding agent
Per 1 weight portion tar lowering aroma adding agent is diluted with the water of 3 weight portions after with the dissolving of the ethanol of 2.5 weight portions again.The delicate fragrance type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and the above-mentioned dilution that obtains is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 27 days; The tar lowering aroma adding agent addition is that the sheet cigarette of per 1000 weight portions adds cured tobacco leaf tar-reducing agent 2 weight portions, cured tobacco leaf fumet 1 weight portion, humectant 10 weight portions.
Weight portion in the embodiment of the invention can be gram, kilogram or other unit of weight.
Claims (2)
1. tar lowering aroma adding agent, it is characterized in that: it comprises cured tobacco leaf tar-reducing agent 1～2 weight portion, cured tobacco leaf fumet 1～3 weight portion, humectant 5～10 weight portions;
Described cured tobacco leaf tar-reducing agent is mainly by cordate houttuynia 0.5～2.0 weight portion, wild sole of the foot grass 0.5～2.0 weight portion, and Chinese lobelia 1～4 weight portion, honeysuckle 1～4 weight portion is made; The preparation method of described cured tobacco leaf tar-reducing agent step as follows carries out: (1) is respectively with cordate houttuynia, wild sole of the foot grass, Chinese lobelia is dried and is cut into broken section, honeysuckle is made fragment, will be through 0.5～2.0 weight portion of the cordate houttuynia after the above-mentioned processing, wild sole of the foot grass 0.5～2.0 weight portion, Chinese lobelia 1～4 weight portion, honeysuckle 1～4 weight portion is put into ceramic vessel, the water that adds 40 ℃, amount of water is 2.5～3.0 times of raw material gross weight, presses raw material 0.3～0.5% addition and adds cellulase, put into temperature and be 40 ℃ haybox cooking 1 hour, taking-up is placed on heats 1～3 minute in the micro-wave oven, filter, and collects filtrate and leaves standstill 24 hours, discard precipitation, obtain supernatant; (2) with 1.0～1.5 weight portion Monosodium Edetate salt, 1.5～2.0 weight portion potassium malates, 1.5 it is abundant mixing in the supernatant that obtains of 1.5～2.0 times step (1) of above-mentioned three kinds of material gross weights that～2.0 weight portion dipotassium glycyrrhizinates are dissolved in weight, obtains the cured tobacco leaf tar-reducing agent;
Described cured tobacco leaf fumet is mainly by Radix Acanthopanacis Senticosi root 1.0～1.5 weight portions, siberian rose 1.0～1.5 weight portions, and vanilla beanpod 2.0～2.5 weight portions, ladanum branches and leaves 2.0～2.5 weight portions are made; The preparation method of described cured tobacco leaf fumet step as follows carries out: (1) runs through section with Radix Acanthopanacis Senticosi root and dries, and siberian rose dries section, and the vanilla beanpod was pulverized 20 mesh sieves and made meal, and the ladanum branches and leaves are made fragment; Will be through 1.0～1.5 weight portions of the Radix Acanthopanacis Senticosi root after the above-mentioned processing, siberian rose 1.0～1.5 weight portions, vanilla beanpod 2.0～2.5 weight portions, ladanum branches and leaves 2.0～2.5 weight portions are put into supercritical CO
2In the fluid extraction device, add ethanol for guiding and supporting agent, the addition of ethanol is 7～9% of a raw material weight, at extracting pressure 20～50Mpa, 30～60 ℃ of following cycling extractions of extraction temperature 1～3 hour, the plant extraction liquid that obtains left standstill 24 hours, discard precipitation, obtain supernatant; (2) with 2.0～2.5 weight portion isovaleric acid, 1.5～2.0 weight portion Beta-methyl valeric acids, 1.0～1.5 weight portion alpha-angelica lactones are dissolved in weight and are in the supernatant that the step (1) of 1.5～2.0 times of above-mentioned three kinds of material gross weights obtains fully mixing, obtain the cured tobacco leaf fumet;
Described humectant is made up of the propane diols of 0.5～2.0 weight portion and the compound corn syrup of 1～4 weight portion;
The preparation method of tar lowering aroma adding agent: cured tobacco leaf tar-reducing agent 1～2 weight portion, cured tobacco leaf fumet 1～3 weight portion, humectant 5～10 weight portions are mixed and obtain tar lowering aroma adding agent.
2. the using method of the described tar lowering aroma adding agent of claim 1 is characterized in that: the tar lowering aroma adding agent of per 1 weight portion is diluted with the ethanol dissolving back of 2～3 weight portions water with 3～5 weight portions; The delicate fragrance type cured tobacco leaf is beaten leaf becomes the sheet cigarette, and the tar lowering aroma adding agent dilution is evenly sprayed on above-mentioned sheet cigarette after beating leaf, carries out redrying then, and vanning was deposited 15～30 days; The tar lowering aroma adding agent addition is that the sheet cigarette of per 1000 weight portions adds tar lowering aroma adding agent 7～15 weight portions.
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| CN103099300B (en) * | 2013-02-20 | 2014-10-29 | 河北中烟工业有限责任公司 | Preparation method of ultralow tar flue-cured tobacco type cigarettes |
| CN103230089B (en) * | 2013-03-18 | 2015-07-22 | 河北中烟工业有限责任公司 | Preparation method for ultralow tar oil flue-cured tobacco type cigarettes with quiet and beautiful aroma |
| CN104126865B (en) * | 2014-07-11 | 2016-05-11 | 深圳市汇金禾生物制剂有限公司 | The method of cigarette toxicity reduction liquid, its preparation method and reduction tobacco toxicity |
| CN104856217B (en) * | 2015-05-06 | 2017-04-12 | 湖北省烟草科学研究院 | Method for reducing nitrosamine content special in tobacco during redrying process |
| CN113040420B (en) * | 2019-12-27 | 2022-09-16 | 湖南中烟工业有限责任公司 | Preparation method of tobacco raw material for heating cigarette and heating cigarette product |
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| CN1064792A (en) * | 1991-03-18 | 1992-09-30 | 杨一兵 | The production method of tobacco extract |
| CN1494837A (en) * | 2002-04-30 | 2004-05-12 | 吴上辉 | Xinjian tobacco. health-care cigarette |
| CN1933744A (en) * | 2004-02-19 | 2007-03-21 | 三荣源有限公司 | Nicotine-reducing agent and nicotine reduction method |
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| CN1064792A (en) * | 1991-03-18 | 1992-09-30 | 杨一兵 | The production method of tobacco extract |
| CN1494837A (en) * | 2002-04-30 | 2004-05-12 | 吴上辉 | Xinjian tobacco. health-care cigarette |
| CN1933744A (en) * | 2004-02-19 | 2007-03-21 | 三荣源有限公司 | Nicotine-reducing agent and nicotine reduction method |
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