CN101449717A - Manufacturing method of Lactuca taiwaniana Maxim. plant beverage - Google Patents

Manufacturing method of Lactuca taiwaniana Maxim. plant beverage Download PDF

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Publication number
CN101449717A
CN101449717A CNA2007101938777A CN200710193877A CN101449717A CN 101449717 A CN101449717 A CN 101449717A CN A2007101938777 A CNA2007101938777 A CN A2007101938777A CN 200710193877 A CN200710193877 A CN 200710193877A CN 101449717 A CN101449717 A CN 101449717A
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China
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extract
vitamin
sucralose
water
add
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CNA2007101938777A
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Chinese (zh)
Inventor
张大卫
张仲铭
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Individual
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Priority to CNA2007101938777A priority Critical patent/CN101449717A/en
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Abstract

The invention discloss a method of manufacturing bitter leaf vegetable drink, comprising: kudingcha extract, vitamin c, xanthan gum, golden syrup, sucralose, pure water, with weight percent: kudingcha extract 0.3-0.8g, vitamin c 0.05-0.1g, xanthan gum 0.01-0.03, sucralose 0.01-0.02g, golden syrup 8-12g, pure water 250 g. Impurities of kudingcha extract are removed through high separating purification, biological activity is kept, and special faint scent is present, the extract has active components of actarit glycosides and actarit different glycosides, providing assistant auxiliary protection for chemical liver injury. Natural extract of kudingcha is the material, free of side effect, special taste, and has health care functions of protecting liver, neutralizing the effect of alcoholic drinks, relieving inflammation, clearing away the heat-evil and expelling superficial evils, quenching thirst and improving acuity of vision and the like.

Description

A kind of manufacture method of bitter leaves plant beverage
Technical field
The invention belongs to technical field of beverage, specifically, relate to the manufacture method of a kind of bitter leaves plant beverage with health care function.
Background technology
Bitter leaves tea is China tradition medicinal plant, and is with a long history in use among the people, has the merit of clearing heat and cooling blood, nourishing the liver and kidney, can loose wind-heat, refresh oneself, relieving thirst and restlessness, deoils greasyly, controls headache, dentalgia, hot eyes, pyreticosis polydipsia, dysentery etc.And existing Ilex kadincha beverage processing is to adopt Ilex latifolia tea-leaf to quench through lixiviate, separation, clarification or process to get, and methods such as filtration are made.The Ilex kadincha beverage bitter of producing, impurity is many.
From the Ilex kadincha beverage bitter that above-mentioned open Ilex kadincha beverage processing is come out, impurity is many, function singleness, and bitter leaves tea effective ingredient is extracted not exclusively.
Summary of the invention
The object of the present invention is to provide a kind of novel taste beverage that the bitter leaves tea smell has the local flavor of mellow sweetness and chemical damage had assistant protection function that both had.
In order to realize purpose of the present invention, the present invention realizes like this.A kind of manufacture method of bitter leaves plant beverage, it is formed and comprises: Folum Ilicis extract, vitamin C, xanthans, HFCS, Sucralose, glycyrrhizin, pure water, its weight ratio is: Folum Ilicis extract 0.2~0.8g; Vitamin C 0.05~0.1g; Xanthans 0.008~0.03g; Sucralose 0.008~0.03g; HFCS 8~12g; Glycyrrhizin 0.01~0.05g; Pure water 190~250g; Described Folum Ilicis extract, its procedure of processing is:
The first step: Ilex latifolia tea-leaf is pulverized and lixiviate
(1) Ilex latifolia tea-leaf is pulverized, and cross 20 mesh sieves: (2) are abandoned residue, obtained extract with 95% edible ethanol lixiviate; (3) with the concentrated concentrated extract that obtains of extract decompression;
Second step: purify
(1) resin preliminary treatment: get resin, add isopyknic 10% NaOH aqueous solution and stir, soaked 2 hours, emit cleaning solution, wash with water once, resin changes in the chromatographic column;
(2) medicinal extract is handled: medicinal extract is water-soluble, carry out centrifugal; Repeated centrifugation merges centrifugate 2-5 time, abandons sediment after the processing;
(3) upper prop absorption: with centrifugate with per hour 600L flow velocity absorption, till sample has adsorbed;
(4) desorb: first water flushing, use 85% alcohol desorption then, begin to collect from there being color to get off, till outflow liquid is colourless;
The 3rd step: concentrate and spray drying treatment
(1) the eluent temperature is reduced pressure under 70 ℃ of-90 ℃ of conditions concentrates, pump into the spraying head tank then;
(2) spray-drying;
(3) pulverize, sieve, pack, get finished product-dry powder.
2, the manufacture method of a kind of bitter leaves plant beverage according to claim 1 is characterized in that: the manufacture method step is:
(1) changes glue: at first xanthans 0.01~0.03g is separated with 70~80 ℃ of temperature water-soluble and by colloid mill glue.
(2) allotment: add 0.01~0.02g Sucralose, 8~12g HFCS, glycyrrhizin 0.01~0.02g again, add 0.05~0.1g vitamin C then, add 0.3~0.8g Folum Ilicis extract and moisturizing at last and be settled to 250g, the supplementary material dissolving is mixed 70 ℃-90 ℃ abundant down stirrings of temperature.
(3) can, seal: deaeration, it is qualified to seal.
(4) sterilization: 121 ℃~126 ℃, the time kept 10~15 minutes.
(5) cooling: rush in the row cooling with running water.
3, the manufacture method of a kind of bitter leaves plant beverage according to claim 1 is characterized in that: the manufacture method step is:
(1) change glue: with xanthans 0.008~0.03g by colloid mill glue;
(2) molten powder: with 0.008~0.02g Sucralose, 6~10g HFCS, 0.01~0.02g glycyrrhizin, 0.03~0.08g vitamin C, 0.2~0.7g Folum Ilicis extract adds, and pays special attention to, and must add vitamin C before adding Folum Ilicis extract;
(3) allotment:, water is settled to 190g, and is warmed up to 45~60 ℃ of abundant stirrings 15~25 minutes, make raw material fully dissolve mixing;
(4) homogeneous: through the homogenizer homogeneous, this step also can be according to the actual conditions adjustment;
(5) sterilization: adopt the TRANSIENT HIGH TEMPERATURE sterilization, 135~145 ℃, kept 2~8 seconds;
(6) can: adopt the Tetrapack cold-aseptic filling.
The invention has the beneficial effects as follows: the extract of bitter leaves that adds among (1) the present invention has passed through the separation of height and has purified; removed impurity; kept its biologically active; and special fragrant arranged; active ingredient is Verbascoside and acteoside isomer in this extract; chemical damage there is auxiliary protection function, has tangible anti-alcohol function.
(2) after the present invention adds vitamin C, both can also can play antioxidation by enriched nutritive, need not add other antioxidant again, make drink natural health more.
(3) the present invention adds xanthans, and the certain bitter taste of energy embedding makes Ilex kadincha beverage not bitter, widely popular acceptance.
(5) add Sucralose, HFCS, glycyrrhizin among the present invention, make this product mellow fresh and sweet.
(6) drink and be not subjected to time, site limitation, instant is easy to carry.
(7) adopt the natural extract of leaflet Kuding tea to be raw material, without any side effects, special taste has liver-protecting and alcoholism-relieving, and anti-inflammatory is convenient, and is clearing heat and detoxicating, and quenching the thirst makes eye bright, the health-care effect of pharynx-clearing throat-benefiting.
The specific embodiment
Below in conjunction with embodiment the present invention is described.
A kind of manufacture method of bitter leaves plant beverage, it is formed and comprises: Folum Ilicis extract, vitamin C, xanthans, HFCS, Sucralose, glycyrrhizin, pure water, its weight ratio is: Folum Ilicis extract 0.2~0.8g; Vitamin C 0.05~0.1g; Xanthans 0.008~0.03g; Sucralose 0.008~0.03g; HFCS 8~12g; Glycyrrhizin 0.01~0.05g; Pure water 190~250g; Described Folum Ilicis extract, its procedure of processing is:
The first step: Ilex latifolia tea-leaf is pulverized and lixiviate
1), Ilex latifolia tea-leaf pulverizes, and crosses 20 mesh sieves: 2), abandon residue, obtain extract with 95% edible ethanol lixiviate; 3), with the concentrated concentrated extract that obtains of extract decompression;
Second step: purify
(1) resin preliminary treatment: get resin, add isopyknic 10% NaOH aqueous solution and stir, soaked 2 hours, emit cleaning solution, wash with water once, resin changes in the chromatographic column;
(2) medicinal extract is handled: medicinal extract is water-soluble, carry out centrifugal; Repeated centrifugation merges centrifugate 2-5 time, abandons sediment after the processing;
(3) upper prop absorption: with centrifugate with per hour 600L flow velocity absorption, till sample has adsorbed;
(4) desorb: first water flushing, use 85% alcohol desorption then, begin to collect from there being color to get off, till outflow liquid is colourless;
The 3rd step: concentrate and spray drying treatment
(1) the eluent temperature is reduced pressure under 70 ℃ of-90 ℃ of conditions concentrates, pump into the spraying head tank then;
(2) spray-drying;
(3) pulverize, sieve, pack, get finished product-dry powder.
The manufacture method of described a kind of bitter leaves plant beverage, the manufacture method step is:
(1) changes glue: at first xanthans 0.01~0.03g is separated with 70~80 ℃ of temperature water-soluble and by colloid mill glue.
(2) allotment: add 0.01~0.02g Sucralose, 8~12g HFCS, glycyrrhizin 0.01~0.02g again, add 0.05~0.1g vitamin C then, add 0.3~0.8g Folum Ilicis extract and moisturizing at last and be settled to 250g, the supplementary material dissolving is mixed 70 ℃-90 ℃ abundant down stirrings of temperature.
(3) can, seal: deaeration, it is qualified to seal.
(4) sterilization: 121 ℃~126 ℃, the time kept 10~15 minutes.
(5) cooling: rush in the row cooling with running water.
The manufacture method of described a kind of bitter leaves plant beverage, the manufacture method step is:
(1) change glue: with xanthans 0.008~0.03g by colloid mill glue;
(2) molten powder: with 0.008~0.02g Sucralose, 6~10g HFCS, 0.01~0.02g glycyrrhizin, 0.03~0.08g vitamin C, 0.2~0.7g Folum Ilicis extract adds, and pays special attention to, and must add vitamin C before adding Folum Ilicis extract;
(3) allotment:, water is settled to 190g, and is warmed up to 45~60 ℃ of abundant stirrings 15~25 minutes, make raw material fully dissolve mixing;
(4) homogeneous: through the homogenizer homogeneous, this step also can be according to the actual conditions adjustment;
(5) sterilization: adopt the TRANSIENT HIGH TEMPERATURE sterilization, 135~145 ℃, kept 2~8 seconds;
(6) can: adopt the Tetrapack cold-aseptic filling.
Embodiment 1:
The manufacture method step of described a kind of bitter leaves plant beverage is:
(1), changes glue: at first xanthans 0.01~0.03g is separated with 70~80 ℃ of temperature water-soluble and by colloid mill glue.
(2), allotment: add 0.01~0.02g Sucralose, 8~12g HFCS, glycyrrhizin 0.01~0.02g again, add 0.05~0.1g vitamin C last adding 0.3~0.8g Folum Ilicis extract and moisturizing then and be settled to 250g, the supplementary material dissolving is mixed 70 ℃-90 ℃ abundant down stirrings of temperature.
(3), can, seal: deaeration, it is qualified to seal.
(4), sterilization: 121 ℃~126 ℃, the time kept 10~15 minutes.
(5), cooling: rush in the row cooling with running water.
Embodiment 2:
A kind of preparation method of above-mentioned Ilex kadincha beverage.
The manufacture method step of described a kind of bitter leaves plant beverage is:
(1) change glue: with xanthans 0.008~0.03g by colloid mill glue.
(2) molten powder: with 0.008~0.02g Sucralose, 6~10g HFCS, 0.01~0.02g glycyrrhizin, 0.03~0.08g vitamin C, 0.2~0.7g Folum Ilicis extract adds, and pays special attention to, and must add vitamin C before adding Folum Ilicis extract.
(3) allotment:, water is settled to 190g, and is warmed up to 45~60 ℃ of abundant stirrings 15~25 minutes, make raw material fully dissolve mixing.
(4) homogeneous: through the homogenizer homogeneous, this step also can be according to the actual conditions adjustment.
(5) sterilization: adopt the TRANSIENT HIGH TEMPERATURE sterilization, 135~145 ℃, kept 2~8 seconds.
(6) can: adopt the Tetrapack cold-aseptic filling.
Embodiment 3:
The manufacture method step of described a kind of bitter leaves plant beverage is:
(1), changes glue: at first xanthans 0.01g is separated with 70~80 ℃ of temperature water-soluble and by colloid mill glue.
(2), allotment: add 0.02g Sucralose, 12g HFCS, glycyrrhizin 0.01g again, add then that the 0.05g vitamin C adds the 0.3g Folum Ilicis extract at last and moisturizing is settled to 250g, fully stir down for 70 ℃-90 ℃ in temperature the supplementary material dissolving is mixed.
(3), can, seal: deaeration, it is qualified to seal.
(4), sterilization: 121 ℃~126 ℃, the time kept 10~15 minutes.
(5), cooling: rush in the row cooling with running water.
Embodiment 4:
The manufacture method step of described a kind of bitter leaves plant beverage is:
(1), changes glue: at first xanthans 0.03g is separated with 70~80 ℃ of temperature water-soluble and by colloid mill glue.
(2), allotment: add the 0.01g Sucralose again, the 8g HFCS, glycyrrhizin 0.02g adds then that the 0.1g vitamin C adds the 0.8g Folum Ilicis extract at last and moisturizing is settled to 250g, fully stirs down for 70 ℃-90 ℃ in temperature the supplementary material dissolving is mixed.
(3), can, seal: deaeration, it is qualified to seal.
(4), sterilization: 121 ℃~126 ℃, the time kept 10~15 minutes.
(5), cooling: rush in the row cooling with running water.
Embodiment 5:
The manufacture method step of described a kind of bitter leaves plant beverage is:
(1) change glue: with xanthans 0.008g by colloid mill glue.
(2) molten powder: with the 0.02g Sucralose, the 10g HFCS, the 0.01g glycyrrhizin, the 0.08g vitamin C, the 0.2g Folum Ilicis extract adds, and pays special attention to, and must add vitamin C before adding Folum Ilicis extract.
(3) allotment:, water is settled to 190g, and is warmed up to 45~60 ℃ of abundant stirrings 15~25 minutes, make raw material fully dissolve mixing.
(4) homogeneous: through the homogenizer homogeneous, this step also can be according to the actual conditions adjustment.
(5) sterilization: adopt the TRANSIENT HIGH TEMPERATURE sterilization, 135~145 ℃, kept 2~8 seconds.
(6) can: adopt the Tetrapack cold-aseptic filling.
Embodiment 5:
The manufacture method step of described a kind of bitter leaves plant beverage is:
(1) change glue: with xanthans 0.03g by colloid mill glue.
(2) molten powder: with the 0.008g Sucralose, the 6g HFCS, the 0.02g glycyrrhizin, the 0.03g vitamin C, the 0.7g Folum Ilicis extract adds, and pays special attention to, and must add vitamin C before adding Folum Ilicis extract.
(3) allotment:, water is settled to 190g, and is warmed up to 45~60 ℃ of abundant stirrings 15~25 minutes, make raw material fully dissolve mixing.
(4) homogeneous: through the homogenizer homogeneous, this step also can be according to the actual conditions adjustment.
(5) sterilization: adopt the TRANSIENT HIGH TEMPERATURE sterilization, 135~145 ℃, kept 2~8 seconds.
(6) can: adopt the Tetrapack cold-aseptic filling.

Claims (3)

1, a kind of manufacture method of bitter leaves plant beverage is characterized in that: it is formed and comprises: Folum Ilicis extract, vitamin C, xanthans, HFCS, Sucralose, glycyrrhizin, pure water, and its weight ratio is: Folum Ilicis extract 0.2~0.8g; Vitamin C 0.05~0.1g; Xanthans 0.008~0.03g; Sucralose 0.008~0.03g; HFCS 8~12g; Glycyrrhizin 0.01~0.05g; Pure water 190~250g; Described Folum Ilicis extract, its procedure of processing is:
The first step: Ilex latifolia tea-leaf is pulverized and lixiviate
(1) Ilex latifolia tea-leaf is pulverized, and cross 20 mesh sieves: (2) are abandoned residue, obtained extract with 95% edible ethanol lixiviate; (3) with the concentrated concentrated extract that obtains of extract decompression;
Second step: purify
(1) resin preliminary treatment: get resin, add isopyknic 10%NaOH aqueous solution and stir, soaked 2 hours, emit cleaning solution, wash with water once, resin changes in the chromatographic column;
(2) medicinal extract is handled: medicinal extract is water-soluble, carry out centrifugal; Repeated centrifugation merges centrifugate 2-5 time, abandons sediment after the processing;
(3) upper prop absorption: with centrifugate with per hour 600L flow velocity absorption, till sample has adsorbed;
(4) desorb: first water flushing, use 85% alcohol desorption then, begin to collect from there being color to get off, till outflow liquid is colourless;
The 3rd step: concentrate and spray drying treatment
(1) the eluent temperature is reduced pressure under 70 ℃ of-90 ℃ of conditions concentrates, pump into the spraying head tank then;
(2) spray-drying;
(3) pulverize, sieve, pack, get finished product-dry powder.
2, the manufacture method of a kind of bitter leaves plant beverage according to claim 1 is characterized in that: the manufacture method step is:
(1) changes glue: at first xanthans 0.01~0.03g is separated with 70~80 ℃ of temperature water-soluble and by colloid mill glue.
(2) allotment: add 0.01~0.02g Sucralose, 8~12g HFCS, glycyrrhizin 0.01~0.02g again, add 0.05~0.1g vitamin C then, add 0.3~0.8g Folum Ilicis extract and moisturizing at last and be settled to 250g, the supplementary material dissolving is mixed 70 ℃-90 ℃ abundant down stirrings of temperature.
(3) can, seal: deaeration, it is qualified to seal.
(4) sterilization: 121 ℃~126 ℃, the time kept 10~15 minutes.
(5) cooling: rush in the row cooling with running water.
3, the manufacture method of a kind of bitter leaves plant beverage according to claim 1 is characterized in that: the manufacture method step is:
(1) change glue: with xanthans 0.008~0.03g by colloid mill glue;
(2) molten powder: with 0.008~0.02g Sucralose, 6~10g HFCS, 0.01~0.02g glycyrrhizin, 0.03~0.08g vitamin C, 0.2~0.7g Folum Ilicis extract adds, and pays special attention to, and must add vitamin C before adding Folum Ilicis extract;
(3) allotment:, water is settled to 190g, and is warmed up to 45~60 ℃ of abundant stirrings 15~25 minutes, make raw material fully dissolve mixing;
(4) homogeneous: through the homogenizer homogeneous, this step also can be according to the actual conditions adjustment;
(5) sterilization: adopt the TRANSIENT HIGH TEMPERATURE sterilization, 135~145 ℃, kept 2~8 seconds;
(6) can: adopt the Tetrapack cold-aseptic filling.
CNA2007101938777A 2007-11-30 2007-11-30 Manufacturing method of Lactuca taiwaniana Maxim. plant beverage Pending CN101449717A (en)

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Application Number Priority Date Filing Date Title
CNA2007101938777A CN101449717A (en) 2007-11-30 2007-11-30 Manufacturing method of Lactuca taiwaniana Maxim. plant beverage

Publications (1)

Publication Number Publication Date
CN101449717A true CN101449717A (en) 2009-06-10

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101911993A (en) * 2010-08-09 2010-12-15 深圳市华熙生物科技有限公司 Folium llicis latifoliae drink and preparation method thereof
CN104921221A (en) * 2015-06-05 2015-09-23 贵州苗姑娘食品有限责任公司 Liver tonifying herbaceous plant beverage
CN105580932A (en) * 2014-10-22 2016-05-18 可口可乐公司 Method for preparing tea-leaf extracts of different flavors
CN107467439A (en) * 2017-10-14 2017-12-15 保定市冰花食品股份有限公司 A kind of beverage and preparation method thereof
CN107897486A (en) * 2017-11-20 2018-04-13 深圳大学 A kind of chewing gum
CN109043270A (en) * 2018-08-06 2018-12-21 林健 Natural fruit and vegetables component extracting method, solid beverage mix and beverage
CN114766672A (en) * 2022-05-25 2022-07-22 贵州泰和现代生态农业科技有限公司 Old lobular broadleaf holly leaf extract and application thereof in preparing food for relieving alcohol-induced liver injury

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101911993A (en) * 2010-08-09 2010-12-15 深圳市华熙生物科技有限公司 Folium llicis latifoliae drink and preparation method thereof
CN105580932A (en) * 2014-10-22 2016-05-18 可口可乐公司 Method for preparing tea-leaf extracts of different flavors
CN105580932B (en) * 2014-10-22 2021-11-30 可口可乐公司 Method for preparing tea leaf extract with different tastes
CN104921221A (en) * 2015-06-05 2015-09-23 贵州苗姑娘食品有限责任公司 Liver tonifying herbaceous plant beverage
CN107467439A (en) * 2017-10-14 2017-12-15 保定市冰花食品股份有限公司 A kind of beverage and preparation method thereof
CN107467439B (en) * 2017-10-14 2021-02-12 保定市冰花食品股份有限公司 Beverage and preparation method thereof
CN107897486A (en) * 2017-11-20 2018-04-13 深圳大学 A kind of chewing gum
CN109043270A (en) * 2018-08-06 2018-12-21 林健 Natural fruit and vegetables component extracting method, solid beverage mix and beverage
CN114766672A (en) * 2022-05-25 2022-07-22 贵州泰和现代生态农业科技有限公司 Old lobular broadleaf holly leaf extract and application thereof in preparing food for relieving alcohol-induced liver injury

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