CN101361702A - Nano sunscreen foundation cream and preparation method thereof - Google Patents
Nano sunscreen foundation cream and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a nano sun-screen foundation cream and a preparation method thereof, which belong to the field of cosmetics and the processing technology thereof. The foundation cream is prepared by using water, 15-100 nano titanium dioxide, isopropyl myristate, polyoxyethylene-21 stearic alcohol ether, melissyl PVP, octodecyl alcohol, 5-100 nano iron trioxide, white oil, propanetriol, propanediol, polyoxypropylene-15 Stearic ether, milkvetch root extract, white beeswax, polydimethyl siloxane fluid, stearic acid monoglyceryl ester, vitamin E nicotinic acid ester, alose, acrylic acid polymer, diazolidinyl urea, acetaldehyde di-uride and essence. The nano sun-screen foundation cream has safety and good sun-screen effects, and has the functions of sun screen, after-sun repair and covering facial flaw.
Description
Technical field
The present invention relates to a kind of nano sunscreen foundation cream and preparation method thereof, belong to cosmetics and processing technique field thereof.
Background technology
Along with running down of earth environment, ozone hole is more and more serious, causes ultraviolet more and more to threaten human skin.In recent years, the dermatology scientific research finds that the UVA ultraviolet accounts for 98% in the ultraviolet gross energy that arrives human body, and it is strong more than the UVB ultraviolet to glass, medicated clothing, water and people's skin penetration, though the skin effect to the people is slower, accumulating over a long period to cause grievous injury.UVA can bring out photosensitization, phototoxic reaction or the like.Also can bring out skin carcinoma under the serious situation.UVA has been identified as the one of the main reasons of skin aging.Recent research is pointed out, when people's skin is exposed under the ultraviolet, form the main cause of sunburn, be the immunologic function that ultraviolet can reduce and damage skin, skin has been reduced external microorganism is caused disease with viral opposing, severe patient can cause the formation of tumor.Along with the progressively enhancing of people's aesthetic health care consciousness, also more and more higher to the requirement of sunscreen product, quality and safety become the basic demand of people to sun care preparations.But present sunscreen product is common sunscreen foundation cream, and sun-proof result is undesirable, and safety is relatively poor, function singleness.
Summary of the invention
The present invention is exactly the safety that provides in order to solve the problems of the technologies described above, the nano sunscreen foundation cream that sun-proof result is good, and it has effect sun-proof, that repair and cover facial defect after shining.
Another technical problem to be solved by this invention provides that technology is simple, cost is low, the preparation method of safe, the nano sunscreen foundation cream that is easy to suitability for industrialized production.
In order to solve the problems of the technologies described above, the present invention realizes like this, nano sunscreen foundation cream, it is to be prepared from by following mass fraction by following raw material: water 30-60 part, 15-100 nano titanium oxide 6-12 part, isopropyl myristate 8-12 part, the stearic alcohol ether 3-8 of polyoxyethylene-21 part, melissyl PVP 3-8 part, octadecanol 1-5 part, 5-100 nanometer iron sesquioxide 1-4 part, white oil 1-3 part, glycerol 1-3 part, propylene glycol 1-3 part, polyoxypropylene-15 stearyl ether 1-3 part, Radix Astragali extractive solution 1-3 part, cera alba 0.5-1.5 part, polydimethyl siloxane fluid 0.5-1.5 part, glycerol monostearate 0.5-1.5 part, vitamin E Nicotinate 0.5-1.5 part, Aloe powder 0.5-1.5 part, acrylate copolymer 0.2-1 part, two imidazolidinyl urea 0.1-0.3 parts, the two uride 0.1-0.3 parts of acetaldehyde, essence 0.1-0.3 part.
Described nano sunscreen foundation cream, it is to be prepared from by following mass fraction by following raw material: 40 parts in water, 8 parts of 15-100 nano titanium oxides, 10 parts of isopropyl myristates, 5 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP5 part, 3 parts of octadecanol, 2.9 parts of 5-100 nanometer iron sesquioxide, 2 parts of white oils, 2 parts of glycerol, 2 parts of propylene glycol, 2 parts of polyoxypropylene-15 stearyl ethers, 2 parts of Radix Astragali extractive solutions [Astragalusmembranaceus (Fisch.) Bge.], 1 part of cera alba, 1 part of polydimethyl siloxane fluid, 1 part of glycerol monostearate, 1 part of vitamin E Nicotinate, 1 part of Aloe powder, 0.5 part of acrylate copolymer, 0.2 part of two imidazolidinyl urea, 0.2 part of the two uride of acetaldehyde, 0.2 part in essence.
The preparation method of described nano sunscreen foundation cream is as follows: the purified water that will meet described parts by weight is earlier put into jar, add weighing and meet 5-100 nanometer iron sesquioxide, glycerol, propylene glycol, the acroleic acid polymerization raw material of described parts by weight well, begin to stir, be heated to 85-95 ℃ simultaneously and make first group of solution; Weighing is met isopropyl myristate, 15-100 nano titanium oxide, the stearic alcohol ether of polyoxyethylene-21, melissyl PVP, octadecanol, white oil, polyoxypropylene-15 stearyl ether, cera alba, polydimethyl siloxane fluid, the glycerol monostearate raw material of described parts by weight well, put into jar and heat and be raised to 85-95 ℃ to the complete molten second group of solution of making; First group of solution and second group of solution are mixed, 70-80 ℃ of emulsifying homogenizing 7-15 minute, reemulsification stirred 50-80 minute; Add when temperature drops to 45-55 ℃ and meet described parts by weight Radix Astragali extractive solution, vitamin E Nicotinate, Aloe powder, the reemulsification homogenizing was made the 3rd group of solution in 1-3 minute; Add when treating that temperature drops to 35-45 ℃ and meet the two imidazolidinyl urea of described parts by weight, the two urides of acetaldehyde, essence, stop after stirring evenly, evacuation, packing was both when temperature to be expected was reduced to room temperature.
Nano sunscreen foundation cream, it is to be prepared from by following mass fraction by following raw material: water 30-60 part, 15-100 nano titanium oxide 15-25 part, isopropyl myristate 8-12 part, the stearic alcohol ether 3-8 of polyoxyethylene-21 part, melissyl PVP 3-8 part, octadecanol 1-5 part, 5-100 nanometer iron sesquioxide 1-4 part, white oil 1-3 part, glycerol 1-3 part, propylene glycol 1-3 part, polyoxypropylene-15 stearyl ether 1-3 part, Radix Astragali extractive solution 1-3 part, cera alba 0.5-1.5 part, polydimethyl siloxane fluid 0.5-1.5 part, glycerol monostearate 0.5-1.5 part, vitamin E Nicotinate 0.5-1.5 part, Aloe powder 0.5-1.5 part, acrylate copolymer 0.2-1 part, two imidazolidinyl urea 0.1-0.3 parts, the two uride 0.1-0.3 parts of acetaldehyde, essence 0.1-0.3 part.
Described nano sunscreen foundation cream, it is to be prepared from by following mass fraction by following raw material: 50 parts in water, 18 parts of 15-100 nano titanium oxides, 10 parts of isopropyl myristates, 5 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP5 part, 3 parts of octadecanol, 2.9 parts of 5-100 nanometer iron sesquioxide, 2 parts of white oils, 2 parts of glycerol, 2 parts of propylene glycol, 2 parts of polyoxypropylene-15 stearyl ethers, 2 parts of Radix Astragali extractive solutions, 1 part of cera alba, 1 part of polydimethyl siloxane fluid, 1 part of glycerol monostearate, 1 part of vitamin E Nicotinate, 1 part of Aloe powder, 0.5 part of acrylate copolymer, 0.2 part of two imidazolidinyl urea, 0.2 part of the two uride of acetaldehyde, 0.2 part in essence.
The preparation method of described nano sunscreen foundation cream is as follows: will meet described parts by weight purified water earlier and put into jar, add load weighted 5-100 nanometer iron sesquioxide, glycerol, propylene glycol, the acroleic acid polymerization raw material that meets described parts by weight, begin to stir, be heated to 85-95 ℃ simultaneously and make first group of solution; With load weighted isopropyl myristate, 15-100 nano titanium oxide, the stearic alcohol ether of polyoxyethylene-21, melissyl PVP, octadecanol, white oil, polyoxypropylene-15 stearyl ether, cera alba, polydimethyl siloxane fluid, the glycerol monostearate raw material that meets described parts by weight, put into jar and heat and be raised to 85-95 ℃ to the complete molten second group of solution of making; First group of solution and second group of solution are mixed, 70-80 ℃ of emulsifying homogenizing 7-15 minute, reemulsification stirred 50-70 minute; Add Radix Astragali extractive solution, vitamin E Nicotinate, the Aloe powder that meets described parts by weight when temperature drops to 45-55 ℃, the reemulsification homogenizing was made the 3rd group of solution in 1-3 minute; Treat to add when temperature drops to 35-45 ℃ two imidazolidinyl urea, the two urides of acetaldehyde, essence, stop evacuation after stirring evenly; Packing both got when temperature to be expected was reduced to room temperature.
Described Radix Astragali extractive solution is that the Radix Astragali is formed with three merging of 50% alcohol reflux, and three times time was respectively 4 hours, 2 hours and 2 hours.
Advantage of the present invention and effect are as follows:
Safety of the present invention, sun-proof result are good, and it has effect sun-proof, that repair and cover facial defect after shining.Further specify beneficial effect of the present invention below in conjunction with examination embodiment and test data.Shining black state-of-the-art in the world nanometer physical sunscreen microgranule technology, the multiple natural plants essence of fusion and the high-grade skin protection feed purification of adopting forms.When being applied in the exposed position of human body, can form the bionical barrier of multilamellar immediately, effectively UVA (tanned), UVB (sunburn) ultraviolet and the computer in the blocking reflected sunlight, TV, the medium ray of daylight lamp are to the injury of skin, increase the activity of Skin Cell, suppress several sunburns of melanin and form, avoid skin aging in advance, it is ventilative that skin please be felt well, elastic reinforcement, pale gloss, wrinkle reduces.
The specific embodiment
Embodiment 1
That nano sunscreen foundation cream of the present invention is to be prepared from by following mass fraction by following raw material: 40 parts in water, 8 parts of 15-100 nano titanium oxides, 10 parts of isopropyl myristates, 5 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP5 part, 3 parts of octadecanol, 2.9 parts of 5-100 nanometer iron sesquioxide, 2 parts of white oils, 2 parts of glycerol, 2 parts of propylene glycol, 2 parts of polyoxypropylene-15 stearyl ethers, 2 parts of Radix Astragali extractive solutions, 1 part of cera alba, 1 part of polydimethyl siloxane fluid, 1 part of glycerol monostearate, 1 part of vitamin E Nicotinate, 1 part of Aloe powder, 0.5 part of acrylate copolymer, 0.2 part of two imidazolidinyl urea, 0.2 part of the two uride of acetaldehyde, 0.2 part in essence.
The following purified water that will meet described parts by weight earlier of its preparation method is put into jar, add weighing and meet 5-100 nanometer iron sesquioxide, glycerol, propylene glycol, the acroleic acid polymerization raw material of described parts by weight well, begin to stir, be heated to 90 ℃ simultaneously and make first group of solution; Weighing is met isopropyl myristate, 15-100 nano titanium oxide, the stearic alcohol ether of polyoxyethylene-21, melissyl PVP, octadecanol, white oil, polyoxypropylene-15 stearyl ether, cera alba, polydimethyl siloxane fluid, the glycerol monostearate raw material of described parts by weight well, put into jar and heat and be raised to 90 ℃ to the complete molten second group of solution of making; First group of solution and second group of solution are mixed, 75 ℃ of emulsifying homogenizing 10 minutes, reemulsification stirred 60 minutes; Add when temperature drops to 50 ℃ and meet described parts by weight Radix Astragali extractive solution, vitamin E Nicotinate, Aloe powder, the reemulsification homogenizing was made the 3rd group of solution in 2 minutes; Add when treating that temperature drops to 40 ℃ and meet the two imidazolidinyl urea of described parts by weight, the two urides of acetaldehyde, essence, stop after stirring evenly, evacuation, packing was both when temperature to be expected was reduced to room temperature.
The examining report of present embodiment product is as follows:
Material and method:
1. detection thing: the cosmetics original.
2. reference standards: 8% homosalate (salicylic acid front three cyclohexyl ester Homosalate), spf value 4.47 ± 1.297, compound method is seen " sun care preparations sun protection coefficient (spf value) body measurements method " appendix A.
3. experimenter: totally 10 people, male 0 people, women 10 people in age 20-50 year, meet the experimenter and volunteer inclusion criteria.
4. light source: the solar simulator xenon arc lamp, every performance indications meet the mensuration code requirement.
5. the method for inspection: test according to " sun care preparations sun protection coefficient (spf value) body measurements method " specific requirement.The experimenter gets the position of leaning forward, and gets its back and shines.Check preceding 24 hours and predict the minimal erythema dose (med value) of experimenter's skin,, be used for sample survey according to the adjustment ultraviolet irradiating dose that predicts the outcome to ultraviolet radiation.The same day was at first selected one 5cm * 6cm normal skin zone in check at the experimenter back, press 2mg/cm
2The consumption of sample evenly spreads upon sample to be checked or standard reference material in the above-mentioned zone; Select suitable ultraviolet irradiating dose then, divide three kinds of situations to shine: 1. experimenter's skin is not coated with sample; 2. be coated with the standard control sample; 3. be coated with sample to be checked.Observation experiment result after 24 hours writes down three kinds of med values under the situation respectively.
6.SPF value calculating method: sample or standard substance protect single experimenter's spf value and represent with following formula:
Calculation sample protects the arithmetic mean of whole experimenter's spf values, gets the spf value that its integer part is this working sample.Estimate that the sampling error of mean can calculate the standard deviation and the standard error of these group data.According to the requirement of " sun care preparations sun protection coefficient (spf value) body measurements method ", standard error should be less than 10% of mean, otherwise should increase experimenter's number until meeting above-mentioned requirements.
Check conclusion: human test result shows that the spf value of institute's sample product is 22.38.
Test basis " cosmetics health standard " is defended the method prison and is sent out [1999] No. 577
Main checkout equipment and numbering: AAS (5720) ZYG (two types) UV (781009
Testing result:
One, material and method
1. tried thing: sample is a colour of skin semisolid, uses the original during test.
2. animal: 4 of the large ear rabbits (distant real kinoplaszm word 2000-024) that provides by Shenyang City's Yuhong District zoopery feed factory, regular grade, male, body weight 2～3kg.
3. experimental animal feeding environment: laboratory animal room's quality certification number: No. the 08th, distant real rotating ring word 2001, single cage, 25 ± 2 ℃ of room temperatures, humidity 50% ± 10%, animal feed provides (distant real rotating ring word 1999-024) by Shenyang City's Yuhong District zoopery feed factory.
4. method: 24h removes the hair of rabbit back spinal column both sides skin before the test, and the unhairing scope is 6cm
2, the left side is contrast, the right is the test block, is coated with to be tried thing 0.2g, smears every day once, continuous 14 days.Since second day, smear preceding unhairing at every turn, water cleans, and observes the skin irritation reaction after one hour, and the record result.
Two, experimental result: 4 rabbit test block skin is not seen any unusually in smearing overall process in test, and average every day, every animal integral mean value was 0 (seeing Table 1), this product to the rabbit skin repeatedly the skin irritation test show as nonirritant.
Table 1 shines black nano sunscreen foundation cream to rabbit skin irritation result of the test repeatedly
Judge suggestion: this product to the rabbit skin repeatedly the skin irritation test be nonirritant.
Embodiment 2
Nano sunscreen foundation cream is to be prepared from by following mass fraction by following raw material: 50 parts in water, 18 parts of 15-100 nano titanium oxides, 10 parts of isopropyl myristates, 5 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP5 part, 3 parts of octadecanol, 2.9 parts of 5-100 nanometer iron sesquioxide, 2 parts of white oils, 2 parts of glycerol, 2 parts of propylene glycol, 2 parts of polyoxypropylene-15 stearyl ethers, 2 parts of Radix Astragali extractive solutions, 1 part of cera alba, 1 part of polydimethyl siloxane fluid, 1 part of glycerol monostearate, 1 part of vitamin E Nicotinate, 1 part of Aloe powder, 0.5 part of acrylate copolymer, 0.2 part of two imidazolidinyl urea, 0.2 part of the two uride of acetaldehyde, 0.2 part in essence.
Its preparation method is as follows: will meet described parts by weight purified water earlier and put into jar, add load weighted 5-100 nanometer iron sesquioxide, glycerol, propylene glycol, the acroleic acid polymerization raw material that meets described parts by weight, begin to stir, be heated to 90 ℃ simultaneously and make first group of solution; With load weighted isopropyl myristate, 15-100 nano titanium oxide, the stearic alcohol ether of polyoxyethylene-21, melissyl PVP, octadecanol, white oil, polyoxypropylene-15 stearyl ether, cera alba, polydimethyl siloxane fluid, the glycerol monostearate raw material that meets described parts by weight, put into jar and heat and be raised to 90 ℃ to the complete molten second group of solution of making; First group of solution and second group of solution are mixed, 75 ℃ of emulsifying homogenizing 7-15 minute, reemulsification stirred 60 minutes; Add Radix Astragali extractive solution, vitamin E Nicotinate, the Aloe powder that meets described parts by weight when temperature drops to 50 ℃, the reemulsification homogenizing was made the 3rd group of solution in 2 minutes; Treat to add when temperature drops to 40 ℃ two imidazolidinyl urea, the two urides of acetaldehyde, essence, stop evacuation after stirring evenly; Packing both got when temperature to be expected was reduced to room temperature.
The examining report of present embodiment product is as follows:
Material and method:
7. detection thing: the cosmetics original.
8. reference standards: 8% homosalate (salicylic acid front three cyclohexyl ester Homosalate), spf value 4.47 ± 1.297, compound method is seen " sun care preparations sun protection coefficient (spf value) body measurements method " appendix A.
9. experimenter: totally 10 people, male 3 people, women 7 people in age 20-38 year, meet the experimenter and volunteer inclusion criteria.
10. light source: the solar simulator xenon arc lamp, every performance indications meet the mensuration code requirement.
11. the method for inspection: test according to " sun care preparations sun protection coefficient (spf value) body measurements method " specific requirement.The experimenter gets the position of leaning forward, and gets its back and shines.Check preceding 24 hours and predict the minimal erythema dose (med value) of experimenter's skin,, be used for sample survey according to the adjustment ultraviolet irradiating dose that predicts the outcome to ultraviolet radiation.The same day was at first selected one 5cm * 6cm normal skin zone in check at the experimenter back, press 2mg/cm
2The consumption of sample evenly spreads upon sample to be checked or standard reference material in the above-mentioned zone; Select suitable ultraviolet irradiating dose then, divide three kinds of situations to shine: 1. experimenter's skin is not coated with sample; 2. be coated with the standard control sample; 3. be coated with sample to be checked.Observation experiment result after 24 hours writes down three kinds of med values under the situation respectively.
12.SPF value calculating method: sample or standard substance protect single experimenter's spf value and represent with following formula:
Calculation sample protects the arithmetic mean of whole experimenter's spf values, gets the spf value that its integer part is this working sample.Estimate that the sampling error of mean can calculate the standard deviation and the standard error of these group data.According to the requirement of " sun care preparations sun protection coefficient (spf value) body measurements method ", standard error should be less than 10% of mean, otherwise should increase experimenter's number until meeting above-mentioned requirements.
Check conclusion: human test result shows that the spf value of institute's sample product is 36.9.
The present embodiment product has carried out experimental test for 50 people through this area method in common, and the result proves that it has effect sun-proof, that repair and cover facial defect after shining, and safety is good, does not see any untoward reaction.
Embodiment 3
Nano sunscreen foundation cream is to be prepared from by following mass fraction by following raw material: 30 parts in water, 6 parts of 15-100 nano titanium oxides, 8 parts of isopropyl myristates, 3 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP3 part, 1 part of octadecanol, 1 part of 5-100 nanometer iron sesquioxide, 1 part of white oil, 1 part of glycerol, 1 part of propylene glycol, 1 part of polyoxypropylene-15 stearyl ether, 1 part of Radix Astragali extractive solution, 0.5 part of cera alba, 0.5 part of polydimethyl siloxane fluid, 0.5 part of glycerol monostearate, 0.5 part of vitamin E Nicotinate, 0.5 part of Aloe powder, 0.2 part of acrylate copolymer, 0.1 part of two imidazolidinyl urea, 0.1 part of the two uride of acetaldehyde, 0.1 part in essence.
Its preparation method is with embodiment 1.
Embodiment 4
Nano sunscreen foundation cream is to be prepared from by following mass fraction by following raw material: 60 parts in water, 12 parts of 15-100 nano titanium oxides, 12 parts of isopropyl myristates, 8 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP8 part, 5 parts of octadecanol, 4 parts of 5-100 nanometer iron sesquioxide, 3 parts of white oils, 3 parts of glycerol, 3 parts of propylene glycol, 3 parts of polyoxypropylene-15 stearyl ethers, 3 parts of Radix Astragali extractive solutions, 1.5 parts of cera alba, 1.5 parts of polydimethyl siloxane fluids, 1.5 parts of glycerol monostearate, 1.5 parts of vitamin E Nicotinate, 1.5 parts of Aloe powder, 1 part of acrylate copolymer, 0.3 part of two imidazolidinyl urea, 0.3 part of the two uride of acetaldehyde, 0.3 part in essence.
Its preparation method is with embodiment 1.
Embodiment 5
Nano sunscreen foundation cream is to be prepared from by following mass fraction by following raw material: 45 parts in water, 8 parts of 15-100 nano titanium oxides, 10 parts of isopropyl myristates, 4 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP5 part, 2 parts of octadecanol, 22 parts of 5-100 nanometer three oxidations, 2 parts of white oils, 2 parts of glycerol, 2 parts of propylene glycol, 1.5 parts of polyoxypropylene-15 stearyl ethers, 1.5 parts of Radix Astragali extractive solutions, 1.2 parts of cera alba, 0.8 part of polydimethyl siloxane fluid, 0.8 part of glycerol monostearate, 0.8 part of vitamin E Nicotinate, 0.9 part of Aloe powder, 0.8 part of acrylate copolymer, 0.15 part of two imidazolidinyl urea, 0.2 part of the two uride of acetaldehyde, 0.2 part in essence.
The preparation method of described nano sunscreen foundation cream is as follows: the purified water that will meet described parts by weight is earlier put into jar, add weighing and meet 5-100 nanometer iron sesquioxide, glycerol, propylene glycol, the acroleic acid polymerization raw material of described parts by weight well, begin to stir, be heated to 85 or 95 ℃ simultaneously and make first group of solution; Weighing is met isopropyl myristate, 15-100 nano titanium oxide, the stearic alcohol ether of polyoxyethylene-21, melissyl PVP, octadecanol, white oil, polyoxypropylene-15 stearyl ether, cera alba, polydimethyl siloxane fluid, the glycerol monostearate raw material of described parts by weight well, put into jar and heat and be raised to 85 or 95 ℃ to the complete molten second group of solution of making; First group of solution and second group of solution are mixed, 70 or 80 ℃ of emulsifying homogenizing 7 or 15 minutes, reemulsification stirred 50 or 80 minutes; When temperature drops to 45 or 55 ℃, add and meet described parts by weight Radix Astragali extractive solution, vitamin E Nicotinate, Aloe powder, reemulsification homogenizing 1 or made the 3rd group of solution in 3 minutes; Add when treating that temperature drops to 35 or 45 ℃ and meet the two imidazolidinyl urea of described parts by weight, the two urides of acetaldehyde, essence, stop after stirring evenly, evacuation, packing was both when temperature to be expected was reduced to room temperature.
Embodiment 6
Nano sunscreen foundation cream is to be prepared from by following mass fraction by following raw material: 30 parts in water, 15 parts of 15-100 nano titanium oxides, 8 parts of isopropyl myristates, 3 parts of the stearic alcohol ethers of polyoxyethylene-21,3 parts of melissyl PVP, 1 part of octadecanol, 1 part of 5-100 nanometer iron sesquioxide, 1 part of white oil, 1 part of glycerol, 1 part of propylene glycol, 1 part of polyoxypropylene-15 stearyl ether, 1 part of Radix Astragali extractive solution, 0.5 part of cera alba, 0.5 part of polydimethyl siloxane fluid, 0.5 part of glycerol monostearate, 0.5 part of vitamin E Nicotinate, 0.5 part of Aloe powder, 0.2 part of acrylate copolymer, 0.1 part of two imidazolidinyl urea, 0.1 part of the two uride of acetaldehyde, 0.1 part in essence.
Its preparation method is with embodiment 2.
Embodiment 7
Nano sunscreen foundation cream is to be prepared from by following mass fraction by following raw material: 60 parts in water, 25 parts of 15-100 nano titanium oxides, 12 parts of isopropyl myristates, 8 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP8 part, 5 parts of octadecanol, 4 parts of 5-100 nanometer iron sesquioxide, 3 parts of white oils, 3 parts of glycerol, propylene glycol 1-3 part, polyoxypropylene-15 stearyl ether 1-3 part, Radix Astragali extractive solution 1-3 part, 1.5 parts of cera alba, 1.5 parts of polydimethyl siloxane fluids, 1.5 parts of glycerol monostearate, 1.5 parts of vitamin E Nicotinate, 1.5 parts of Aloe powder, 1 part of acrylate copolymer, 0.3 part of two imidazolidinyl urea, 0.3 part of the two uride of acetaldehyde, 0.3 part in essence.
Its preparation method is with embodiment 2.
Embodiment 8
Nano sunscreen foundation cream is to be prepared from by following mass fraction by following raw material: 40 parts in water, 18 parts of 15-100 nano titanium oxides, 9 parts of isopropyl myristates, 7 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP7 part, 4 parts of octadecanol, 2 parts of 5-100 nanometer iron sesquioxide, 2 parts of white oils, 2 parts of glycerol, 1.5 parts of propylene glycol, 1.5 parts of polyoxypropylene-15 stearyl ethers, 1.5 parts of Radix Astragali extractive solutions, 1.2 parts of cera alba, 0.8 part of polydimethyl siloxane fluid, 1.2 parts of glycerol monostearate, 1.2 parts of vitamin E Nicotinate, 1.2 parts of Aloe powder, 0.5 part of acrylate copolymer, 0.15 part of two imidazolidinyl urea, 0.15 part of the two uride of acetaldehyde, 0.15 part in essence.
Its preparation method is as follows: the purified water that will meet described parts by weight is earlier put into jar, add weighing and meet 5-100 nanometer iron sesquioxide, glycerol, propylene glycol, the acroleic acid polymerization raw material of described parts by weight well, begin to stir, be heated to 90 ℃ simultaneously and make first group of solution; Weighing is met isopropyl myristate, 15-100 nano titanium oxide, the stearic alcohol ether of polyoxyethylene-21, melissyl PVP, octadecanol, white oil, polyoxypropylene-15 stearyl ether, cera alba, polydimethyl siloxane fluid, the glycerol monostearate raw material of described parts by weight well, put into jar and heat and be raised to 90 ℃ to the complete molten second group of solution of making; First group of solution and second group of solution are mixed, 75 ℃ of emulsifying homogenizing 10 minutes, reemulsification stirred 60 minutes; Add when temperature drops to 50 ℃ and meet described parts by weight Radix Astragali extractive solution, vitamin E Nicotinate, Aloe powder, the reemulsification homogenizing was made the 3rd group of solution in 2 minutes; Add when treating that temperature drops to 40 ℃ and meet the two imidazolidinyl urea of described parts by weight, the two urides of acetaldehyde, essence, stop after stirring evenly, evacuation, packing was both when temperature to be expected was reduced to room temperature.
Claims (8)
1. nano sunscreen foundation cream is characterized in that it is to be prepared from by following mass fraction by following raw material: water 30-60 part, 15-100 nano titanium oxide 6-12 part, isopropyl myristate 8-12 part, the stearic alcohol ether 3-8 of polyoxyethylene-21 part, melissyl PVP3-8 part, octadecanol 1-5 part, 5-100 nanometer iron sesquioxide 1-4 part, white oil 1-3 part, glycerol 1-3 part, propylene glycol 1-3 part, polyoxypropylene-15 stearyl ether 1-3 part, Radix Astragali extractive solution 1-3 part, cera alba 0.5-1.5 part, polydimethyl siloxane fluid 0.5-1.5 part, glycerol monostearate 0.5-1.5 part, vitamin E Nicotinate 0.5-1.5 part, Aloe powder 0.5-1.5 part, acrylate copolymer 0.2-1 part, two imidazolidinyl urea 0.1-0.3 parts, the two uride 0.1-0.3 parts of acetaldehyde, essence 0.1-0.3 part.
2. nano sunscreen foundation cream according to claim 1, it is characterized in that described nano sunscreen foundation cream, it is to be prepared from by following mass fraction by following raw material: 40 parts in water, 8 parts of 15-100 nano titanium oxides, 10 parts of isopropyl myristates, 5 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP5 part, 3 parts of octadecanol, 2.9 parts of 5-100 nanometer iron sesquioxide, 2 parts of white oils, 2 parts of glycerol, 2 parts of propylene glycol, 2 parts of polyoxypropylene-15 stearyl ethers, 2 parts of Radix Astragali extractive solutions, 1 part of cera alba, 1 part of polydimethyl siloxane fluid, 1 part of glycerol monostearate, 1 part of vitamin E Nicotinate, 1 part of Aloe powder, 0.5 part of acrylate copolymer, 0.2 part of two imidazolidinyl urea, 0.2 part of the two uride of acetaldehyde, 0.2 part in essence.
3. the preparation method of the described nano sunscreen foundation cream of claim 1, it is characterized in that method is as follows: the purified water that will meet described parts by weight is earlier put into jar, add weighing and meet 5-100 nanometer iron sesquioxide, glycerol, propylene glycol, the acroleic acid polymerization raw material of described parts by weight well, begin to stir, be heated to 85-95 ℃ simultaneously and make first group of solution; Weighing is met isopropyl myristate, 15-100 nano titanium oxide, the stearic alcohol ether of polyoxyethylene-21, melissyl PVP, octadecanol, white oil, polyoxypropylene-15 stearyl ether, cera alba, polydimethyl siloxane fluid, the glycerol monostearate raw material of described parts by weight well, put into jar and heat and be raised to 85-95 ℃ to the complete molten second group of solution of making; First group of solution and second group of solution are mixed, 70-80 ℃ of emulsifying homogenizing 7-15 minute, reemulsification stirred 50-80 minute; Add when temperature drops to 45-55 ℃ and meet described parts by weight Radix Astragali extractive solution, vitamin E Nicotinate, Aloe powder, the reemulsification homogenizing was made the 3rd group of solution in 1-3 minute; Add when treating that temperature drops to 35-45 ℃ and meet the two imidazolidinyl urea of described parts by weight, the two urides of acetaldehyde, essence, stop after stirring evenly, evacuation, packing was both when temperature to be expected was reduced to room temperature.
4. the preparation method of nano sunscreen foundation cream according to claim 3 is characterized in that described Radix Astragali extractive solution is that the Radix Astragali is prepared from for three times with 50% alcohol reflux.
5. nano sunscreen foundation cream is characterized in that it is to be prepared from by following mass fraction by following raw material: water 30-60 part, 15-100 nano titanium oxide 15-25 part, isopropyl myristate 8-12 part, the stearic alcohol ether 3-8 of polyoxyethylene-21 part, melissyl PVP3-8 part, octadecanol 1-5 part, 5-100 nanometer iron sesquioxide 1-4 part, white oil 1-3 part, glycerol 1-3 part, propylene glycol 1-3 part, polyoxypropylene-15 stearyl ether 1-3 part, Radix Astragali extractive solution 1-3 part, cera alba 0.5-1.5 part, polydimethyl siloxane fluid 0.5-1.5 part, glycerol monostearate 0.5-1.5 part, vitamin E Nicotinate 0.5-1.5 part, Aloe powder 0.5-1.5 part, acrylate copolymer 0.2-1 part, two imidazolidinyl urea 0.1-0.3 parts, the two uride 0.1-0.3 parts of acetaldehyde, essence 0.1-0.3 part.
6. nano sunscreen foundation cream according to claim 5 is characterized in that it is to be prepared from by following mass fraction by following raw material: 50 parts in water, 18 parts of 15-100 nano titanium oxides, 10 parts of isopropyl myristates, 5 parts of the stearic alcohol ethers of polyoxyethylene-21, melissyl PVP5 part, 3 parts of octadecanol, 2.9 parts of 5-100 nanometer iron sesquioxide, 2 parts of white oils, 2 parts of glycerol, 2 parts of propylene glycol, 2 parts of polyoxypropylene-15 stearyl ethers, 2 parts of Radix Astragali extractive solutions, 1 part of cera alba, 1 part of polydimethyl siloxane fluid, 1 part of glycerol monostearate, 1 part of vitamin E Nicotinate, 1 part of Aloe powder, 0.5 part of acrylate copolymer, 0.2 part of two imidazolidinyl urea, 0.2 part of the two uride of acetaldehyde, 0.2 part in essence.
7. the preparation method of the described nano sunscreen foundation cream of claim 5, it is characterized in that method is as follows: will meet described parts by weight purified water earlier and put into jar, add load weighted 5-100 nanometer iron sesquioxide, glycerol, propylene glycol, the acroleic acid polymerization raw material that meets described parts by weight, begin to stir, be heated to 85-95 ℃ simultaneously and make first group of solution; With load weighted isopropyl myristate, 15-100 nano titanium oxide, the stearic alcohol ether of polyoxyethylene-21, melissyl PVP, octadecanol, white oil, polyoxypropylene-15 stearyl ether, cera alba, polydimethyl siloxane fluid, the glycerol monostearate raw material that meets described parts by weight, put into jar and heat and be raised to 85-95 ℃ to the complete molten second group of solution of making; First group of solution and second group of solution are mixed, 70-80 ℃ of emulsifying homogenizing 7-15 minute, reemulsification stirred 50-70 minute; Add Radix Astragali extractive solution, vitamin E Nicotinate, the Aloe powder that meets described parts by weight when temperature drops to 45-55 ℃, the reemulsification homogenizing was made the 3rd group of solution in 1-3 minute; Treat to add when temperature drops to 35-45 ℃ two imidazolidinyl urea, the two urides of acetaldehyde, essence, stop evacuation after stirring evenly; Packing both got when temperature to be expected was reduced to room temperature.
8. the preparation method of nano sunscreen foundation cream according to claim 5 is characterized in that described Radix Astragali extractive solution is that the Radix Astragali is prepared from for three times with 50% alcohol reflux.
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| CN104644489A (en) * | 2014-06-10 | 2015-05-27 | 莫治玲 | Sun protection cream |
| CN104721106A (en) * | 2013-12-23 | 2015-06-24 | 青岛东昌源仪器有限公司 | Nutritional sun-protection compact powder capable of delaying senescence |
| CN105434289A (en) * | 2016-01-12 | 2016-03-30 | 广州智媛生物科技有限公司 | Novel efficient sunscreen liquid foundation |
| CN107242980A (en) * | 2017-06-27 | 2017-10-13 | 江苏天芳健康科技有限公司 | A kind of cream of containing gingko extract |
| CN107412060A (en) * | 2017-08-08 | 2017-12-01 | 广州无添加主义化妆品有限公司 | A kind of sunscreen composition, its preparation method, Sun care spray and preparation method thereof |
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2008
- 2008-09-11 CN CN2008100131642A patent/CN101361702B/en active Active
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104721106A (en) * | 2013-12-23 | 2015-06-24 | 青岛东昌源仪器有限公司 | Nutritional sun-protection compact powder capable of delaying senescence |
| CN104644489A (en) * | 2014-06-10 | 2015-05-27 | 莫治玲 | Sun protection cream |
| CN105434289A (en) * | 2016-01-12 | 2016-03-30 | 广州智媛生物科技有限公司 | Novel efficient sunscreen liquid foundation |
| CN105434289B (en) * | 2016-01-12 | 2018-08-17 | 广州智媛生物科技有限公司 | A kind of sun-proof foundation emulsion |
| CN107242980A (en) * | 2017-06-27 | 2017-10-13 | 江苏天芳健康科技有限公司 | A kind of cream of containing gingko extract |
| CN107412060A (en) * | 2017-08-08 | 2017-12-01 | 广州无添加主义化妆品有限公司 | A kind of sunscreen composition, its preparation method, Sun care spray and preparation method thereof |
| CN107412060B (en) * | 2017-08-08 | 2020-07-24 | 广州无添加主义化妆品有限公司 | Sunscreen spray and preparation method thereof |
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|---|---|
| CN101361702B (en) | 2010-09-08 |
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