CN107412060A - A kind of sunscreen composition, its preparation method, Sun care spray and preparation method thereof - Google Patents
A kind of sunscreen composition, its preparation method, Sun care spray and preparation method thereof Download PDFInfo
- Publication number
- CN107412060A CN107412060A CN201710673312.2A CN201710673312A CN107412060A CN 107412060 A CN107412060 A CN 107412060A CN 201710673312 A CN201710673312 A CN 201710673312A CN 107412060 A CN107412060 A CN 107412060A
- Authority
- CN
- China
- Prior art keywords
- preparation
- sunscreen composition
- extract solution
- sun care
- care spray
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dispersion Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The present invention provides a kind of sunscreen composition, its preparation method, Sun care spray and preparation method thereof, is related to cosmetic field.The preparation method of sunscreen composition, including：Radix scutellariae is extracted to obtain the first extract solution, the mixture of moutan root bark, rhodiola root and sweet wormwood is extracted to obtain the second extract solution, the first extract solution and the second extract solution are mixed.Sun care spray, including：3~5wt% butanediol, 4~6wt% glycerine, 0.2~1.2wt glycine betaine, 0.3~1.3wt% dipotassium glycyrrhizinate, 0.05~0.2wt% Sodium Hyaluronate, 30~55wt% above-mentioned sunscreen composition, 3~5wt% aloe extract, 1~2.5wt% panthenol and the water of surplus.Sun care spray, it is made up using above-mentioned sunscreen composition of raw material, has the advantages that not block pore and do not cause allergy, is a kind of safe sunscreen product.
Description
Technical field
The present invention relates to cosmetic field, and more particularly to a kind of sunscreen composition, its preparation method, Sun care spray and
Its preparation method.
Background technology
Existing chemical sun, it is poor ultraviolet radiation absorption effect to be present, needs to repeat to apply at regular intervals during use
Smear.Meanwhile light reaction can occur after chemical sun illumination, easily cause dermatitis or allergy equivalent risk.
In addition, comprising physical sunscreen compositions such as titanium dioxide and/or zinc oxide in existing physical sunscreen agent, these are tiny
Particle can skin surface formed barrier layer and by reflection, scatters ultraviolet skin is played a protective role while, tool
There is poor transparent feel, easily occur in the phenomenon that skin surface is deposited into white layer and come off, using can excessively cause pore
Blocking.
In view of this, the present invention is proposed.
The content of the invention
The first object of the present invention is to provide a kind of sunscreen composition, is a kind of natural sun-prevention combination of good properties
Thing, there is the characteristics of good and anti-light action of sun-proof result is good.
The second object of the present invention is to provide a kind of Sun care spray, be made using above-mentioned sunscreen composition as raw material and
Physics sun-prevention component is not added, has the advantages that not block pore and does not cause allergy, is a kind of safe sunscreen product.
The present invention is solved its technical problem and realized using following technical scheme.
The present invention proposes a kind of preparation method of sunscreen composition, including：
Radix scutellariae is extracted to obtain the first extract solution, the mixture of moutan root bark, rhodiola root and sweet wormwood is extracted
The second extract solution is obtained, the first extract solution and the second extract solution are mixed.
Further, in present pre-ferred embodiments, above-mentioned radix scutellariae, moutan root bark, the mass ratio of rhodiola root and sweet wormwood
For 1.5~3.5：1.5~2.5：1~2.3：2~4.
Further, in present pre-ferred embodiments, it is above-mentioned by be crushed to 45~60 mesh radix scutellariae and 0.9~
2.9vt% acetic acid solution is 1 according to mass ratio：15~25 mixing after, at a temperature of 38~49 DEG C and 40~60W power
25~35min of lower extraction, the extraction product to radix scutellariae carry out being filtrated to get the first filtrate, and the first filtrate is decolourized using activated carbon
After obtain the first extract solution.
Further, in present pre-ferred embodiments, it is above-mentioned by be crushed to 45~60 mesh mixture and 60~
95vt% ethanol is 1 according to mass ratio：After 15~25 mixing, extract at a temperature of 38~49 DEG C and under 60~80W power
25~35min is taken, the extraction product to mixture carries out being filtrated to get the second filtrate, after being decolourized using activated carbon to the second filtrate
Obtain the second extract solution.
The present invention proposes a kind of sunscreen composition, is made according to the preparation method of above-mentioned sunscreen composition.
The present invention proposes a kind of Sun care spray, including：
3~5wt% butanediol, 4~6wt% glycerine, 0.2~1.2wt glycine betaine, 0.3~1.3wt% radix glycyrrhizae
Sour dipotassium, 0.05~0.2wt% Sodium Hyaluronate, 30~55wt% above-mentioned sunscreen composition, 3~5wt% aloe
The water of extract, 1~2.5wt% panthenol and surplus.
The present invention proposes a kind of preparation method of Sun care spray, including：
Above-mentioned sunscreen composition, aloe extract, panthenol and base-material are mixed at a temperature of 40~50 DEG C.
Further, in present pre-ferred embodiments, cosmetic base and temperature are mixed simultaneously for 60~80 DEG C of water
Base-material is obtained after 30~40min of holding at a temperature of 95~100 DEG C.
Further, in present pre-ferred embodiments, by butanediol, glycerine, glycine betaine, dipotassium glycyrrhizinate and hyalomitome
Sour sodium is mixed to get cosmetic base.
Further, in present pre-ferred embodiments, also Sun care spray is packed including the use of two-component packaging.
The beneficial effect of the embodiment of the present invention is：
The preparation method of the sunscreen composition of the embodiment of the present invention, by being extracted to obtain the first extract solution to radix scutellariae,
The mixture of moutan root bark, rhodiola root and sweet wormwood is extracted to obtain the second extract solution, the first extract solution and second are extracted
Liquid mixing can quickly prepare sunscreen composition.
The sunscreen composition of the embodiment of the present invention, is a kind of natural sun-prevention composition of good properties, sun-proof result it is good and
Anti- light action is good, and ultraviolet radiation absorption intensity is big and all has strong absorption in 270~400nm wave-length coverage.Meanwhile with elimination
Ultraviolet radioactive skin and the effect of caused free radical.
The Sun care spray of the embodiment of the present invention, using the extract solution of radix scutellariae, moutan root bark, rhodiola root and sweet wormwood as sun-proof
Active component, have the advantages that not block pore and do not cause allergy, be a kind of safe sunscreen product.With excitant
Low, few side effects and it is safe and reliable the features such as, the stimulation to human body skin and the generation of allergic phenomena can be avoided.It is moreover, anti-
The problems such as dermatitis, allergy or phototoxic reaction can effectively be solved by shining spray.
The preparation method of the Sun care spray of the embodiment of the present invention, it is made using above-mentioned sunscreen composition as active component.
Brief description of the drawings
In order to illustrate the technical solution of the embodiments of the present invention more clearly, below by embodiment it is required use it is attached
Figure is briefly described, it will be appreciated that the following drawings illustrate only certain embodiments of the present invention, therefore be not construed as pair
The restriction of scope, for those of ordinary skill in the art, on the premise of not paying creative work, can also be according to this
A little accompanying drawings obtain other related accompanying drawings.
Fig. 1 is two-component packaging structural representation provided by the invention；
Fig. 2 is tank structure schematic diagram provided by the invention；
Fig. 3 is the structural representation of aerosol component provided by the invention.
Icon：100- two-component packagings；110- tank bodies；111- tank mouths；120- air bags；130- aerosol components；131- lids；
132- injection spray pipes；133- valve modules；140- shower nozzles.
Embodiment
, below will be in the embodiment of the present invention to make the purpose, technical scheme and advantage of the embodiment of the present invention clearer
Technical scheme be clearly and completely described.Unreceipted actual conditions person, builds according to normal condition or manufacturer in embodiment
The condition of view is carried out.Agents useful for same or the unreceipted production firm person of instrument, it is the conventional production that can be obtained by commercially available purchase
Product.
Sunscreen composition, its preparation method, Sun care spray of the embodiment of the present invention and preparation method thereof are carried out below
Illustrate.
A kind of preparation method of sunscreen composition, including：
Mass ratio according to radix scutellariae, moutan root bark, rhodiola root and sweet wormwood is 1.5~3.5：1.5~2.5：1~2.3：2~
4, radix scutellariae, moutan root bark, rhodiola root and sweet wormwood are on the waiting list respectively.
Prepare the first extract solution.
According to mass ratio it is 1 by the radix scutellariae being on the waiting list and acetic acid solution：Extracted after 15~25 mixing.Specifically, 38
25~35min is extracted at a temperature of~49 DEG C and under 40~60W power, obtains the extraction product of radix scutellariae.Extraction to radix scutellariae
Product is carried out being filtrated to get the first filtrate, and the first extract solution is obtained after being decolourized using activated carbon to the first filtrate.
Wherein, acetic acid solution selects 0.9~2.9vt% acetic acid solution.
In order to ensure the effect of extracting of radix scutellariae, radix scutellariae is crushed to 45~60 mesh before being mixed with acetic acid solution, by radix scutellariae, obtains
Extracting operation is carried out after to Baical Skullcap Root again.By such operation, the availability of material is effectively increased.
Prepare the second extract solution.
The moutan root bark being on the waiting list, rhodiola root and sweet wormwood are mixed, obtain mixture, as moutan root bark, rhodiola root and green grass or young crops
The mixture of wormwood artemisia mixing.
According to mass ratio it is 1 by mixture and ethanol：Extracted after 15~25 mixing.Specifically, at 38~49 DEG C
At a temperature of and 60~80W power under extract 25~35min, obtain the extraction product of mixture.Extraction product to mixture
Carry out being filtrated to get the second filtrate, the second extract solution is obtained after being decolourized using activated carbon to the second filtrate.
Wherein, ethanol selects 60~95vt% ethanol.
In order to ensure the effect of extracting of the mixture of moutan root bark, rhodiola root and sweet wormwood, mixture mixes with acetic acid solution
Before conjunction, mixture is crushed to 45~60 mesh, obtains that mixture is last to carry out extracting operation again.By such operation, effectively
Improve the availability of material.
First extract solution and the second extract solution are mixed, obtain sunscreen composition.Complete the preparation of sunscreen composition.
Radix scutellariae, moutan root bark, the extract solution of rhodiola root and sweet wormwood include the materials such as glycoside, polysaccharide, flavonoids, pass through this
The synergy of individual material forms above-mentioned sunscreen composition.
Hold above-mentioned, be a kind of good properties by sunscreen composition made from the preparation method of above-mentioned sunscreen composition
Natural sun-prevention composition, the good and anti-light action of sun-proof result is good, and ultraviolet radiation absorption intensity is big and in 270~400nm wavelength
In the range of all have strong absorption.Meanwhile the effect of with ultraviolet radioactive skin and caused free radical is eliminated.
Therefore, the sunscreen composition is respectively provided with extensive purposes in skin repair, sun-proof and treatment.Meanwhile this is sun-proof
Composition is natural sun-prevention component, has the characteristics that low excitant, few side effects and safe and reliable, can avoid to human body skin
Stimulation and allergic phenomena generation.
A kind of Sun care spray, component include：Butanediol, glycerine, glycine betaine, dipotassium glycyrrhizinate, Sodium Hyaluronate, on
State sunscreen composition, aloe extract, general alcohol and water.
Also, said components mix according to following proportioning：3~5wt% butanediol, 4~6wt% glycerine, 0.2~
1.2wt glycine betaine, 0.3~1.3wt% dipotassium glycyrrhizinate, 0.05~0.2wt% Sodium Hyaluronate, 30~55wt%
Above-mentioned sunscreen composition, 3~5wt% aloe extract, the water of 1~2.5wt% panthenol and surplus.
A kind of preparation method of Sun care spray, including：
Matched according to the above-mentioned raw materials of Sun care spray component, be on the waiting list butanediol, glycerine, glycine betaine, glycyrrhizic acid two respectively
Potassium, Sodium Hyaluronate, above-mentioned sunscreen composition, aloe extract, general alcohol and water.
Butanediol, glycerine, glycine betaine, dipotassium glycyrrhizinate and Sodium Hyaluronate are mixed to get cosmetic base.
It is that after 60~80 DEG C of water mix, 30~40min is kept at a temperature of 95~100 DEG C by cosmetic base and temperature
After obtain base-material.
Preferably, the temperature of water is 75 DEG C.
Afterwards, sunscreen composition, aloe extract, panthenol and base-material mixing at a temperature of 40~50 DEG C, is obtained sun-proof
Spray.
Hold it is above-mentioned, Sun care spray using the extract solution of radix scutellariae, moutan root bark, rhodiola root and sweet wormwood as sunscreen actives into
Point, have the advantages that not block pore and do not cause allergy, be a kind of safe sunscreen product.
Sun care spray is packed using two-component packaging 100.Fig. 1, Fig. 2 and Fig. 3 are refer to, two-component packaging 100 wraps
Include tank body 110, air bag 120, aerosol component 130 and shower nozzle 140.
Wherein, tank body 110 has tank mouth 111, has compressed air in tank body 110.Tank body 110 can be aluminium pot or iron
Tank, it is also not necessarily limited to the unlisted other manner of the present embodiment.
Aerosol component 130 includes lid 131, injection spray pipe 132 and valve module 133.Lid 131 is covered on tank mouth 111 and realized
Aerosol component 130 is installed on tank body 110.Valve module 133 is arranged at lid 131, and injection spray pipe 132 is connected with valve module 133 and court
Extend to the direction away from tank body 110.
Air bag 120 is used to hold Sun care spray.The openend of air bag 120 is arranged at valve module 133 and realizes its openend
Closing.Fig. 3 is refer to, when aerosol component 130 is not installed on tank body 110, air bag 120 is cylindrical；It refer to Fig. 1, aerosol
When component 130 is installed on tank body 110, it will be vacuumized in tank body 110 and sun-proof spray be passed through into air bag 120 by injection spray pipe 132
Mist agent, air bag are in expansion state.
Shower nozzle 140 covers at injection spray pipe 132, can be achieved the Sun care spray in air bag 120 by pressing shower nozzle 140
Spray.
In addition, two-component packaging 100 can also include the lid (figure does not illustrate) for covering at shower nozzle 140, the quilt of shower nozzle 140 is prevented
Outside contamination.
By two-component packaging 100, Sun care spray can be prevented to be secondary polluted, avoid material in outside air and spraying from connecing
Touch to cause to repair sun-prevention component and be oxidized and fail, turned to be yellow and face with using the cognition appearance of air oxidation time lengthening spraying material
Discoloration depth phenomenon.That is, avoid influenceing the aesthetics of Sun care spray.
Meanwhile two-component packaging 100 need not add propellant, you can realization sprays Sun care spray in two-component packaging 100.
The feature and performance of the present invention are described in further detail with reference to embodiments.
Embodiment 1
Prepare sunscreen composition：
It is on the waiting list the medicinal material of drying：The radix scutellariae of 25 parts by weight, the moutan root bark of 20 parts by weight, the rhodiola root of 15 parts by weight and 40
The sweet wormwood of parts by weight.Radix scutellariae, moutan root bark, rhodiola root and sweet wormwood are crushed to 45 mesh respectively, it is standby.
The acetic acid solution of radix scutellariae and the 1.5vt% of 500 parts by weight is mixed and heated to 40 DEG C, extracted using supercritical ultrasonics technology
The active ingredient of radix scutellariae obtains the extraction product of radix scutellariae, and specifically, extraction temperature is 40 DEG C, and extraction power is 55W, extraction time
For 30min.Extraction product to radix scutellariae carries out being filtrated to get the first filtrate, and the first filtrate is decolourized to obtain first using activated carbon
Extract solution.
Moutan root bark, rhodiola root and sweet wormwood are mixed to get mixture, the concentration by mixture and 1500 parts by weight is
90vt% ethanol is mixed and heated to 40 DEG C, and the active ingredient that mixture is extracted using supercritical ultrasonics technology obtains the extraction of mixture
Product, specifically, extraction temperature are 40 DEG C, and extraction power is 70W, extraction time 25min.Extraction product to mixture enters
Row is filtrated to get the second filtrate, and the second filtrate is decolourized using activated carbon to obtain the second extract solution.
First extract solution and the second extract solution are mixed to get sunscreen composition.
Prepare Sun care spray：
Each component is on the waiting list according to following proportioning：4.2wt% butanediol, 5.5wt% glycerine, 0.3wt% glycine betaine,
The aloe extraction of 0.3wt% dipotassium glycyrrhizinate, 0.07wt% Sodium Hyaluronate, 46wt% sunscreen composition, 4.2wt%
The water of thing, 1.1wt% panthenol and surplus.
Butanediol, glycerine, glycine betaine, dipotassium glycyrrhizinate and Sodium Hyaluronate are mixed to get cosmetic base.
It is after 70 DEG C of water mix, to be heated to 95 DEG C of temperature and keep at such a temperature by cosmetic base and temperature
Base-material is obtained after 36min.
Afterwards, at a temperature of being cooled to 45 DEG C, sunscreen composition, aloe extract, panthenol and base-material are mixed and stirred for
Uniformly after cooling, Sun care spray is obtained.
Embodiment 2
Prepare sunscreen composition：
It is on the waiting list the medicinal material of drying：The radix scutellariae of 30 parts by weight, the moutan root bark of 18 parts by weight, the rhodiola root of 20 parts by weight and 32
The sweet wormwood of parts by weight.Radix scutellariae, moutan root bark, rhodiola root and sweet wormwood are crushed to 50 mesh respectively, it is standby.
The acetic acid solution of radix scutellariae and the 1.5vt% of 540 parts by weight is mixed and heated to 42 DEG C, extracted using supercritical ultrasonics technology
The active ingredient of radix scutellariae obtains the extraction product of radix scutellariae, and specifically, extraction temperature is 42 DEG C, and extraction power is 50W, extraction time
For 28min.Extraction product to radix scutellariae carries out being filtrated to get the first filtrate, and the first filtrate is decolourized to obtain first using activated carbon
Extract solution.
Moutan root bark, rhodiola root and sweet wormwood are mixed to get mixture, the concentration by mixture and 1400 parts by weight is
95vt% ethanol is mixed and heated to 43 DEG C, and the active ingredient that mixture is extracted using supercritical ultrasonics technology obtains the extraction of mixture
Product, specifically, extraction temperature are 43 DEG C, and extraction power is 74W, extraction time 28min.Extraction product to mixture enters
Row is filtrated to get the second filtrate, and the second filtrate is decolourized using activated carbon to obtain the second extract solution.
First extract solution and the second extract solution are mixed to get sunscreen composition.
Prepare Sun care spray：
Each component is on the waiting list according to following proportioning：4.4wt% butanediol, 5.1wt% glycerine, 0.6wt% glycine betaine,
The aloe extraction of 0.8wt% dipotassium glycyrrhizinate, 0.1wt% Sodium Hyaluronate, 50wt% sunscreen composition, 4.6wt%
The water of thing, 2.1wt% panthenol and surplus.
Butanediol, glycerine, glycine betaine, dipotassium glycyrrhizinate and Sodium Hyaluronate are mixed to get cosmetic base.
It is after 75 DEG C of water mix, to be heated to 90 DEG C of temperature and keep at such a temperature by cosmetic base and temperature
Base-material is obtained after 32min.
Afterwards, at a temperature of being cooled to 45 DEG C, sunscreen composition, aloe extract, panthenol and base-material are mixed and stirred for
Uniformly after cooling, Sun care spray is obtained.
Embodiment 3
Prepare sunscreen composition：
It is on the waiting list the medicinal material of drying：The radix scutellariae of 30 parts by weight, the moutan root bark of 23 parts by weight, the rhodiola root of 23 parts by weight and 25
The sweet wormwood of parts by weight.Radix scutellariae, moutan root bark, rhodiola root and sweet wormwood are crushed to 60 mesh respectively, it is standby.
The acetic acid solution of radix scutellariae and the 1.5vt% of 750 parts by weight is mixed and heated to 47 DEG C, extracted using supercritical ultrasonics technology
The active ingredient of radix scutellariae obtains the extraction product of radix scutellariae, and specifically, extraction temperature is 47 DEG C, and extraction power is 50W, extraction time
For 30min.Extraction product to radix scutellariae carries out being filtrated to get the first filtrate, and the first filtrate is decolourized to obtain first using activated carbon
Extract solution.
Moutan root bark, rhodiola root and sweet wormwood are mixed to get mixture, the concentration by mixture and 1633 parts by weight is
850vt% ethanol is mixed and heated to 39 DEG C, and the active ingredient that mixture is extracted using supercritical ultrasonics technology obtains the extraction of mixture
Product is taken, specifically, extraction temperature is 39 DEG C, and extraction power is 73W, extraction time 32min.Extraction product to mixture
Carry out being filtrated to get the second filtrate, the second filtrate is decolourized using activated carbon to obtain the second extract solution.
First extract solution and the second extract solution are mixed to get sunscreen composition.
Prepare Sun care spray：
Each component is on the waiting list according to following proportioning：5wt% butanediol, 5.5wt% glycerine, 0.5wt% glycine betaine,
The aloe extraction of 1.0wt% dipotassium glycyrrhizinate, 0.14wt% Sodium Hyaluronate, 51wt% sunscreen composition, 3.5wt%
The water of thing, 1.1wt% panthenol and surplus.
Butanediol, glycerine, glycine betaine, dipotassium glycyrrhizinate and Sodium Hyaluronate are mixed to get cosmetic base.
It is after 70 DEG C of water mix, to be heated to 95 DEG C of temperature and keep at such a temperature by cosmetic base and temperature
Base-material is obtained after 40min.
Afterwards, at a temperature of being cooled to 45 DEG C, sunscreen composition, aloe extract, panthenol and base-material are mixed and stirred for
Uniformly after cooling, Sun care spray is obtained.
Embodiment 4
Prepare sunscreen composition：
It is on the waiting list the medicinal material of drying：The radix scutellariae of 54 parts by weight, the moutan root bark of 36 parts by weight, the rhodiola root of 18 parts by weight and 42
The sweet wormwood of parts by weight.Radix scutellariae, moutan root bark, rhodiola root and sweet wormwood are crushed to 45 mesh respectively, it is standby.
The acetic acid solution of radix scutellariae and the 1.5vt% of 900 parts by weight is mixed and heated to 47 DEG C, extracted using supercritical ultrasonics technology
The active ingredient of radix scutellariae obtains the extraction product of radix scutellariae, and specifically, extraction temperature is 47 DEG C, and extraction power is 59W, extraction time
For 30min.Extraction product to radix scutellariae carries out being filtrated to get the first filtrate, and the first filtrate is decolourized to obtain first using activated carbon
Extract solution.
Moutan root bark, rhodiola root and sweet wormwood are mixed to get mixture, the concentration by mixture and 2376 parts by weight is
80vt% ethanol is mixed and heated to 48 DEG C, and the active ingredient that mixture is extracted using supercritical ultrasonics technology obtains the extraction of mixture
Product, specifically, extraction temperature are 48 DEG C, and extraction power is 63W, extraction time 35min.Extraction product to mixture enters
Row is filtrated to get the second filtrate, and the second filtrate is decolourized using activated carbon to obtain the second extract solution.
First extract solution and the second extract solution are mixed to get sunscreen composition.
Prepare Sun care spray：
Each component is on the waiting list according to following proportioning：4.2wt% butanediol, 4.5wt% glycerine, 0.7wt% glycine betaine,
The aloe extraction of 0.6wt% dipotassium glycyrrhizinate, 0.17wt% Sodium Hyaluronate, 34wt% sunscreen composition, 5.0wt%
The water of thing, 2.0wt% panthenol and surplus.
Butanediol, glycerine, glycine betaine, dipotassium glycyrrhizinate and Sodium Hyaluronate are mixed to get cosmetic base.
It is after 72 DEG C of water mix, to be heated to 95 DEG C of temperature and keep at such a temperature by cosmetic base and temperature
Base-material is obtained after 31min.
Afterwards, at a temperature of being cooled to 45 DEG C, sunscreen composition, aloe extract, panthenol and base-material are mixed and stirred for
Uniformly after cooling, Sun care spray is obtained.
Spectrophotometric test is carried out to Sun care spray prepared by embodiment 1.
Sun care spray prepared by Example 1 is appropriate, as treating test sample.It will treat that test sample is applied to 8 μm using membrane process
On 5 thick quartz colorimetric utensils, as sample 1, sample 2, sample 3, sample 4 and sample 5, measure sample 1~5 exist respectively
270nm~400nm range of wavelengths average transmittances.Wherein, treat test sample in quartz colorimetric utensil by 1mg/cm2Amount smear be advisable,
30min is placed after smearing, then carries out spectrophotometric test.Measurement result is shown in Table 1.
The measurement result of the spectrophotometric of the sample of 1 embodiment of table 1
Put down as it can be seen from table 1 Sun care spray sample made from embodiment 1 is sprayed in 270~400nm wave-length coverages
Equal absorbance is 1.898, and therefore, the Sun care spray has good sun-proof result.
Comparative example 1
Prepare Sun care spray：
4.2wt% butanediol, 5.5wt% glycerine, 0.3wt% glycine betaine, 0.3wt% dipotassium glycyrrhizinate,
0.07wt% Sodium Hyaluronate, 46wt% sunscreen composition, 4.2wt% aloe extract, 1.1wt% panthenol and remaining
The water of amount.
Butanediol, glycerine, glycine betaine, dipotassium glycyrrhizinate and Sodium Hyaluronate are mixed to get cosmetic base.
It is after 70 DEG C of water mix, to be heated to 95 DEG C of temperature and keep at such a temperature by cosmetic base and temperature
Base-material is obtained after 36min.
Afterwards, at a temperature of being cooled to 45 DEG C, after aloe extract, panthenol and base-material are mixed and stirred for into uniformly cooling,
Obtain the Sun care spray of comparative example.
Spectrophotometric test is carried out to Sun care spray prepared by comparative example 1.Test operation is grasped with the test of embodiment 1
Make, similarly, the sample of comparative example is 5, respectively as control sample 1, control sample 2, control sample 3, control sample 4 and control sample
5, measurement result is shown in Table 2.
The measurement result of the spectrophotometric of the sample of 2 comparative example of table 1
Put down from table 2 it can be seen that Sun care spray sample made from comparative example 1 is sprayed in 270~400nm wave-length coverages
Equal absorbance is 0.592.It is appreciated that Sun care spray prepared by the embodiment 1 of the same terms, in 270~400nm wavelength models
Possesses preferable sun-proof result in enclosing.
Comparative example 2
Sun care spray prepared by Example 1, unitary packaging and two-component packaging 100 are carried out respectively.Prepare same specification 5
Unitary packs sample and 5 two-component packaging samples.Also, 5 unitary are packed into sample and 5 two-component packaging samples all use
After 1/3, by whole samples incubated 15 days at a temperature of 45 DEG C, sample is observed.Observed result is shown in Table 3.
The observed result of table 3
From table 3 it is observed that the sample color situation of change of two-component packaging 100 is substantially better than the sample of unitary packaging,
Illustrate that two-component packaging 100 can effectively solve the problem that the problems such as Sun care spray is contaminated in use and is oxidized, binary
Packaging 100 ensures that product has the effect of more stable.
It is therefore preferable that Sun care spray is packed from two-component packaging 100.
In summary, the preparation method of the sunscreen composition of the embodiment of the present invention, by being extracted to obtain to radix scutellariae
One extract solution, the mixture of moutan root bark, rhodiola root and sweet wormwood is extracted to obtain the second extract solution, by the first extract solution and
The mixing of second extract solution can quickly prepare sunscreen composition.
The sunscreen composition of the embodiment of the present invention, is a kind of natural sun-prevention composition of good properties, sun-proof result it is good and
Anti- light action is good, and ultraviolet radiation absorption intensity is big and all has strong absorption in 270~400nm wave-length coverage.Meanwhile with elimination
Ultraviolet radioactive skin and the effect of caused free radical.
The Sun care spray of the embodiment of the present invention, using the extract solution of radix scutellariae, moutan root bark, rhodiola root and sweet wormwood as sun-proof
Active component, have the advantages that not block pore and do not cause allergy, be a kind of safe sunscreen product.With excitant
Low, few side effects and it is safe and reliable the features such as, the stimulation to human body skin and the generation of allergic phenomena can be avoided.It is moreover, anti-
The problems such as dermatitis, allergy or phototoxic reaction can effectively be solved by shining spray.
The preparation method of the Sun care spray of the embodiment of the present invention, it is made using above-mentioned sunscreen composition as active component.
Embodiments described above is part of the embodiment of the present invention, rather than whole embodiments.The reality of the present invention
The detailed description for applying example is not intended to limit the scope of claimed invention, but is merely representative of the selected implementation of the present invention
Example.Based on the embodiment in the present invention, what those of ordinary skill in the art were obtained under the premise of creative work is not made
Every other embodiment, belongs to the scope of protection of the invention.
Claims (10)
- A kind of 1. preparation method of sunscreen composition, it is characterised in that including：Radix scutellariae is extracted to obtain the first extract solution, the mixture of moutan root bark, rhodiola root and sweet wormwood is extracted to obtain Second extract solution, first extract solution and second extract solution are mixed.
- 2. the preparation method of sunscreen composition according to claim 1, it is characterised in that the radix scutellariae, the tree peony root The mass ratio of skin, the rhodiola root and the sweet wormwood is 1.5~3.5：1.5~2.5：1~2.3：2~4.
- 3. the preparation method of sunscreen composition according to claim 1 or 2, it is characterised in that 45~60 mesh will be crushed to The radix scutellariae and 0.9~2.9vt% acetic acid solution according to mass ratio be 1：After 15~25 mixing, in 38~49 DEG C of temperature 25~35min is extracted under lower and 40~60W power, the extraction product to the radix scutellariae is carried out being filtrated to get the first filtrate, made First extract solution is obtained after being decolourized with activated carbon to first filtrate.
- 4. the preparation method of sunscreen composition according to claim 1 or 2, it is characterised in that 45~60 mesh will be crushed to The mixture and 60~95vt% ethanol according to mass ratio be 1：15~25 mixing after, at a temperature of 38~49 DEG C and 25~35min is extracted under 60~80W power, the extraction product to the mixture carries out being filtrated to get the second filtrate, uses Activated carbon obtains second extract solution after being decolourized to second filtrate.
- A kind of 5. sunscreen composition, it is characterised in that the preparation of the sunscreen composition according to any one of Claims 1 to 4 Method is made.
- A kind of 6. Sun care spray, it is characterised in that including：3~5wt% butanediol, 4~6wt% glycerine, 0.2~1.2wt glycine betaine, 0.3~1.3wt% glycyrrhizic acid two Potassium, 0.05~0.2wt% Sodium Hyaluronate, 30~55wt% sunscreen composition as claimed in claim 5,3~5wt% Aloe extract, 1~2.5wt% panthenol and the water of surplus.
- A kind of 7. preparation method of Sun care spray, it is characterised in that including：Sunscreen composition as claimed in claim 5, aloe extract, panthenol and base-material are mixed at a temperature of 40~50 DEG C Close.
- 8. the preparation method of Sun care spray according to claim 7, it is characterised in that be by cosmetic base and temperature 60~80 DEG C of water mixing simultaneously obtains base-material after 30~40min of holding at a temperature of 95~100 DEG C.
- 9. the preparation method of Sun care spray according to claim 8, it is characterised in that by butanediol, glycerine, beet Alkali, dipotassium glycyrrhizinate and Sodium Hyaluronate are mixed to get the cosmetic base.
- 10. the preparation method of Sun care spray according to claim 7, it is characterised in that also including the use of two-component packaging The Sun care spray is packed.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710673312.2A CN107412060B (en) | 2017-08-08 | 2017-08-08 | Sunscreen spray and preparation method thereof |
| PCT/CN2017/109784 WO2019029029A1 (en) | 2017-08-08 | 2017-11-07 | Sunscreen composition, preparation method therefor, sunscreen spray and preparation method therefor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710673312.2A CN107412060B (en) | 2017-08-08 | 2017-08-08 | Sunscreen spray and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107412060A true CN107412060A (en) | 2017-12-01 |
| CN107412060B CN107412060B (en) | 2020-07-24 |
Family
ID=60437735
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710673312.2A Active CN107412060B (en) | 2017-08-08 | 2017-08-08 | Sunscreen spray and preparation method thereof |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN107412060B (en) |
| WO (1) | WO2019029029A1 (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108478508A (en) * | 2018-05-29 | 2018-09-04 | 佛山市顺德区香江精细化工实业有限公司 | A kind of after-sun spray and preparation method thereof |
| CN109394972A (en) * | 2018-12-19 | 2019-03-01 | 辽宁石油化工大学 | A kind of Chinese medicine sunscreen formulas and its preparation method and application |
| CN114010513A (en) * | 2021-11-12 | 2022-02-08 | 杨伟业 | Itching-relieving skin-care spray and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2330606Y (en) * | 1997-01-22 | 1999-07-28 | 李�浩 | Double-component packing pot |
| CN101361702A (en) * | 2008-09-11 | 2009-02-11 | 赖福平 | Nano sunscreen foundation cream and preparation method thereof |
| CN201538516U (en) * | 2009-07-01 | 2010-08-04 | 李新建 | Binary packaging tank |
| CN106420381A (en) * | 2016-08-08 | 2017-02-22 | 辛成业 | Novel applications of artemisinin ingredients or composition of artemisinin ingredients in skin care |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102406577B (en) * | 2011-11-28 | 2013-06-05 | 广东轻工职业技术学院 | Chinese medicine composite with sun-screening function and preparation method and application of extract thereof |
| CA2896646A1 (en) * | 2012-12-27 | 2014-07-03 | Hayashibara Co., Ltd. | Skin-exterior anti-ageing composition and production method therefor |
| CN103893064A (en) * | 2014-03-22 | 2014-07-02 | 南通蛇类治疗研究所 | Nutrient Chinese medicinal ferment enzyme sunscreen cream |
| CN106236644A (en) * | 2016-08-26 | 2016-12-21 | 广州市美集化妆品科技有限公司 | It is a kind of that water is tender runs through essence |
| CN106821867A (en) * | 2017-04-03 | 2017-06-13 | 南通蛇类治疗研究所 | Natural plant enzyme enzyme suncream |
-
2017
- 2017-08-08 CN CN201710673312.2A patent/CN107412060B/en active Active
- 2017-11-07 WO PCT/CN2017/109784 patent/WO2019029029A1/en active Application Filing
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2330606Y (en) * | 1997-01-22 | 1999-07-28 | 李�浩 | Double-component packing pot |
| CN101361702A (en) * | 2008-09-11 | 2009-02-11 | 赖福平 | Nano sunscreen foundation cream and preparation method thereof |
| CN201538516U (en) * | 2009-07-01 | 2010-08-04 | 李新建 | Binary packaging tank |
| CN106420381A (en) * | 2016-08-08 | 2017-02-22 | 辛成业 | Novel applications of artemisinin ingredients or composition of artemisinin ingredients in skin care |
Non-Patent Citations (2)
| Title |
|---|
| 左德发: "长白山天然植物在化妆品中的应用", 《日用化学工业》 * |
| 杨小峰等: "青蒿吸收紫外线分析研究", 《长春工业大学学报》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108478508A (en) * | 2018-05-29 | 2018-09-04 | 佛山市顺德区香江精细化工实业有限公司 | A kind of after-sun spray and preparation method thereof |
| CN109394972A (en) * | 2018-12-19 | 2019-03-01 | 辽宁石油化工大学 | A kind of Chinese medicine sunscreen formulas and its preparation method and application |
| CN114010513A (en) * | 2021-11-12 | 2022-02-08 | 杨伟业 | Itching-relieving skin-care spray and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107412060B (en) | 2020-07-24 |
| WO2019029029A1 (en) | 2019-02-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100581536C (en) | Camellia skin-care essence oil | |
| CN107412060A (en) | A kind of sunscreen composition, its preparation method, Sun care spray and preparation method thereof | |
| CN103006520A (en) | Vegetal whitening skin care product and preparation process thereof | |
| US7198780B2 (en) | Self-tanning composition in sheeted substrate | |
| CN110339076A (en) | A kind of sunscreen composition and the preparation method and application thereof with broad-spectrum light protective action | |
| CN109355136A (en) | A kind of preparation method and its handmade soap of lily feet flower essential oil | |
| KR20120062565A (en) | Skin massage composition with high antioxidant activity and the mask pack comprising the same | |
| CN101803646A (en) | Fat-reducing health protecting tea and preparation method thereof | |
| CN104367522B (en) | Stretch mark removing beauty powder and preparation method thereof | |
| IL185775A (en) | Pomegranate-derived products for the treatment of skin sores and lesions | |
| CN110368339A (en) | Face mask of traditional Chinese medicine composition and preparation method thereof, application method | |
| CN101784256A (en) | Botanical powdered hair dye composition | |
| KR20090060981A (en) | Tape of protecting ultraviolet rays | |
| CN107326126B (en) | A kind of Chinese herbal medicine leather and fur conditioning liquid and preparation method thereof | |
| CN105832638B (en) | Whitening pearl facial mask beautifying liquid with deep water supplement moisture-keeping functions and its preparation method | |
| EP0967988A1 (en) | Ointment for the treatment of burns and of other skin diseases | |
| CN106860183A (en) | A kind of skin makeup paste formulation and its processing technology | |
| CN110368332A (en) | Face mask of traditional Chinese medicine composition and preparation method thereof, application method | |
| CN1284345A (en) | Plaque dispelling mixture | |
| KR20070074005A (en) | Woody fiber cosmetics and thereof manufacturing method | |
| CN107094812A (en) | A kind of fruit tree insecticide and preparation method thereof | |
| CN1153055A (en) | Chinese medicinal herb coat aerosol for treatment of mild burn scald, soft tissue damage and frostbite | |
| CN107714548A (en) | A kind of plant sun frost and preparation method thereof | |
| CN107582458A (en) | A kind of sunscreen composition and preparation method thereof | |
| CN107213075A (en) | Paste in Whitening, spot face |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |