CN101357115B - Golden vinegar pearl shining shampoo milk and preparation method thereof - Google Patents
Golden vinegar pearl shining shampoo milk and preparation method thereof Download PDFInfo
- Publication number
- CN101357115B CN101357115B CN2008100792946A CN200810079294A CN101357115B CN 101357115 B CN101357115 B CN 101357115B CN 2008100792946 A CN2008100792946 A CN 2008100792946A CN 200810079294 A CN200810079294 A CN 200810079294A CN 101357115 B CN101357115 B CN 101357115B
- Authority
- CN
- China
- Prior art keywords
- parts
- vinegar
- vitamin
- ferment
- golden
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Cosmetics (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
The invention discloses gold vinegar pearlescent shampoo milk which comprises the raw materials with the weight mixture ratio: 8-11.5 parts of gold vinegar, 1.9-2.2 parts of serine, 0.9-1.2 parts of threonine, 0.9-1.2 parts of leucine, 0.9-1.2 parts of mature vinegar ferment, 1.4-1.7 parts of docosyl trimethyl ammonium chloride, 10-20 parts of AES, 3.5-7 of 6502, 0.5-1.2 parts of polysiloxane cation protein, 0.4-1.1 parts of CB Climbazole, 0.5-0.9 parts of essence, 0.1-0.4 parts of JM-115, 0.1-0.4 parts of vitamin C, 0.1-0.4 parts of vitamin B1, 0.1-0.4 parts of vitamin E and 55-65 parts of de-ionized water. The preparation method of the gold vinegar pearlescent shampoo milk is as follows: purifying gold vinegar, amino acid, functional mixed elements, emulsification, pearliztion, homogenizing, desaeration, blending of favor, and can pack. The milk of the invention fills domestic blank, not only fully excavates the efficacies of hair care, moistening hair, hair growing, relieving itching of Shanxi mature vinegar of country vinegar, but also further extracts the nutrient content of compound amino acid and ferment to prepare a shampoo and hair care product with top quality which is safer, more efficient, more natural and more environmentally and integrates the functions of shampoo, hair-care, conditioning, relieving itching and anti-losing hair into a whole.
Description
Technical field:
The invention belongs to a kind of hair-washing hair-care articles for use, be specifically related to a kind of golden vinegar pearl shining shampoo milk and preparation method thereof.
Background technology:
Hair is the vitals of human body, and it both had protective effect to human body, is again the significant points of decorating the human body appearance.The healthy development growth of hair needs good nutrient substance to moisten; Reason owing to the age; The pollution of natural environment such as atmosphere, operating pressure, endocrine disturbance that reasons such as health cause or the like; The capital goes wrong the hair normal growth, like withered, tarnish, jag, coming off or the like just need give Direct Nursing from the outside to hair.Present hair care product both domestic and external is a lot.But it is more safe and effective, having distinct Chinese characteristics, particularly state's vinegar Shanxi mature vinegar, to be that the nutrition base further extracts the synthetic nutrition conditioning shampoo articles for use of aminoacid still blank.
Three, summary of the invention:
The present invention is directed against problems such as hair is withered, tarnish, jag, and providing a kind of is the nutrition base with the Shanxi mature vinegar, further extracts the hair shampoo article of the synthetic nutrition recuperating of aminoacid.
The present invention realizes through following technical scheme:
A kind of golden vinegar pearl shining shampoo milk, it is made up of the following weight proportion raw material: golden vinegar 8-11.5 part, serine 1.9-2.2 part; Threonine 0.9-1.2 part, leucine 0.9-1.2 part, old vinegar ferment 0.9-1.2 part; INCROQUAT TMC-80 ECONOL TM22 1.4-1.7 part, AES10-20 part, 65023.5-7 part; Silicone, cationic albumen 0.5-1.2 part, CB climbazole 0.4-1.1 part, essence 0.5-0.9 part; JM-1150.1-0.4 part, vitamin C 0.1-0.4 part, vitaminB10 .1-0.4 part, vitamin E 0.1-0.4 part, deionized water 55-65 part.
A kind of method for preparing of golden vinegar pearl shining shampoo milk:
1. the Fenyang wine Daqu (massive raw stater for alcholic liquor) is mixed by the weight ratio of 1:1 with Sorghum vulgare Pers. and ferment; Article Wen Keda was 30 ℃ in the 3rd day, fermented to summit in the 4th day, and these article extend to four and half; Main fermentation finishes the back sealing descends the article temperature gradually; Get into the after fermentation phase, ferment phase after fermentation phase is prolonged 10 days to 16 days finish, temperature keeps 18-20 ℃.
2. old vinegar that aging is good adopts the method for the vacuum and low temperature golden vinegar of purifying, and extracting temperature is 60 ℃ ± 5 ℃, and vacuum be-0.08MPa to reach golden vinegar standard, the end of purifying.
3. the old vinegar ferment extracts: the old vinegar Daqu (massive raw stater for alcholic liquor) is pulverized with solute: solvent is to soak 48 hours containing in the alcoholic acid solution of 10-20% of 1:1.5; Refluxed once in per 4 hours; Temperature remains on 40-50 ℃, and the isolated by filtration clear liquid is sloughed ethanol with clear liquid and reclaimed reuse in agitated reactor.Then, temperature 45-55 ℃, be concentrated into original volume 1/3 and finish to extract at vacuum-0.08MPa.
4. the golden vinegar 8-11.5 part that will purify and serine 1.9-2.2 part, threonine 0.9-1.2 part, leucine 0.9-1.2 part, old vinegar ferment 0.9-1.2 part; INCROQUAT TMC-80 ECONOL TM22 1.4-1.7 part is mixed, and adds AES10-20 part again, 65023.5-7 part, silicone, cationic albumen 0.5-1.2 part; CB climbazole 0.4-1.1 part, essence 0.5-0.9 part, JM-1150.1-0.4 part; Vitamin C 0.1-0.4 part, vitaminB10 .1-0.4 part, vitamin E 0.1-0.4 part, deionized water 55-65 part, the blending constituent material proportioning and homogenizing is carried out emulsifying processing; The control oil phase added water elder generation homogenizing 15 minutes at 115 ℃ in the emulsion process, recovered normal the stirring again.
5.40 it is canned that perfumery below ℃ finishes post curing 6 hours.
The present invention compared with prior art, have following beneficial effect: this project begins from deep processing of farm products, adopts proportioning raw materials such as Daqu (massive raw stater for alcholic liquor) Sorghum vulgare Pers. at high proportion; Prolong yeast phase, make strain can change into starch, sugar etc. nutrient substance such as aminoacid fully, again the old vinegar that is changed into by grain is carried out deep processing; Produce golden vinegar after the purification, hair is had good nutrition, restoration care effect by concentrated aminoacid, particularly serine in the golden vinegar, threonine, leucine; N-fatty acid, threonine have surface activity and the double effects of preserving moisture, and leucine is lateral to show certain lipotropy with ramose carbochain, so be prone to absorb for hair; Use after one month; The hair light is jag not, and alopecia obviously reduces, no dandruff.
Four, the specific embodiment:
Embodiment 1:
A kind of golden vinegar pearl shining shampoo milk, it is made up of the following weight proportion raw material: 10 parts of golden vinegar, 2 parts of serines, 1 part of threonine; 1 part of leucine, 1 part in old vinegar ferment, 1.5 parts of INCROQUAT TMC-80 ECONOL TM22s, AES15 part; 65025 parts, 1 part in silicone, cationic albumen, 0.6 part of CB climbazole; 0.7 part in essence, JM-1150.3 part, 0.3 part of vitamin C, vitaminB10 .3 part, 0.3 part of vitamin E, 60 parts of deionized waters; Wherein golden vinegar total acid 6g/100ml, total amino nitrogen 0.25g/100ml, fixed acid 2.4g/100ml.
A kind of method for preparing of golden vinegar pearl shining shampoo milk:
1. the Fenyang wine Daqu (massive raw stater for alcholic liquor) is mixed by the weight ratio of 1:1 with Sorghum vulgare Pers. and ferment; Article Wen Keda was 30 ℃ in the 3rd day; Fermented to summit in the 4th day, these article extend to four and half, and main fermentation finishes the back sealing descends the article temperature gradually; Get into the after fermentation phase with ferment phase after fermentation phase prolongation end in 10 days to 16 days, temperature keeps 18-20 ℃.
2. old vinegar that aging is good adopts the method for the vacuum and low temperature golden vinegar of purifying, and extracting temperature is 60 ℃ ± 5 ℃, and vacuum be-0.08MPa, reaches the end of purifying of golden vinegar standard, and wherein the concrete preparation technology of golden vinegar sees Chinese patent 200810055592.1.
3. the old vinegar ferment extracts: the old vinegar Daqu (massive raw stater for alcholic liquor) is pulverized with solute: solvent is to soak 48 hours containing in the alcoholic acid solution of 10-20% of 1:1.5; Refluxed once in per 4 hours; Temperature remains on 40-50 ℃, and the isolated by filtration clear liquid is sloughed ethanol with clear liquid and reclaimed reuse in agitated reactor.Then, temperature 45-55 ℃, be concentrated into original volume 1/3 and finish to extract at vacuum-0.08MPa.
4. 2 parts of 10 parts of the golden vinegar that will purify and serines, 1 part of threonine, 1 part of leucine, 1 part in old vinegar ferment; 1.5 parts of mixing of INCROQUAT TMC-80 ECONOL TM22 add AES15 part again, and 65025 parts, 1 part in silicone, cationic albumen; 0.6 part of CB climbazole, 0.7 part in essence, JM-1150.3 part; 0.3 part of vitamin C, vitaminB10 .3 part, 0.3 part of vitamin E, 60 parts of deionized waters, the blending constituent material proportioning and homogenizing is carried out emulsifying processing; The control oil phase is at 115 ℃ in the emulsion process, and first homogenizing is 15 minutes behind the adding water, recovers normal again and stirs.
5.40 it is canned that perfumery below ℃ finishes post curing 6 hours.
Embodiment 2:
A kind of golden vinegar pearl shining shampoo milk, it is made up of the following weight proportion raw material: 11.5 parts of golden vinegar, 2.2 parts of serines, 1.2 parts of threonine; 1.2 parts of leucines, 1.2 parts in old vinegar ferment, 1.2 parts of INCROQUAT TMC-80 ECONOL TM22s, 20 parts of AES; 6,502 3.5 parts, 1.2 parts in silicone, cationic albumen, 0.5 part of CB climbazole; 0.4 part in essence, 0.1 part of JM-115,0.1 part of vitamin C, 0.1 part of vitamin B1,0.1 part of vitamin E, 55 parts of deionized waters; Wherein golden vinegar total acid 6g/100ml, total amino nitrogen 0.25g/100ml, fixed acid 2.4g/100ml.
A kind of method for preparing of golden vinegar pearl shining shampoo milk:
1. the Fenyang wine Daqu (massive raw stater for alcholic liquor) is mixed by the weight ratio of 1:1 with Sorghum vulgare Pers. and ferment; Article Wen Keda was 30 ℃ in the 3rd day; Fermented to summit in the 4th day, these article extend to four and half, and main fermentation finishes the back sealing descends the article temperature gradually; Get into the after fermentation phase with ferment phase after fermentation phase prolongation end in 10 days to 16 days, temperature keeps 18-20 ℃.
2. old vinegar that aging is good adopts the method for the vacuum and low temperature golden vinegar of purifying, and extracting temperature is 60 ℃ ± 5 ℃, and vacuum be-0.08MPa, reaches the end of purifying of golden vinegar standard, and wherein the concrete preparation technology of golden vinegar sees Chinese patent 200810055592.1.
3. the old vinegar ferment extracts: the old vinegar Daqu (massive raw stater for alcholic liquor) is pulverized with solute: solvent is to soak 48 hours containing in the alcoholic acid solution of 10-20% of 1:1.5; Refluxed once in per 4 hours; Temperature remains on 40-50 ℃, and the isolated by filtration clear liquid is sloughed ethanol with clear liquid and reclaimed reuse in agitated reactor.Then, temperature 45-55 ℃, be concentrated into original volume 1/3 and finish to extract at vacuum-0.08MPa.
4. 2.2 parts of 11.5 parts of the golden vinegar that will purify and serines, 1.2 parts of threonine, 1.2 parts of leucines, 1.2 parts in old vinegar ferment; 1.2 parts of mixing of INCROQUAT TMC-80 ECONOL TM22 add 20 parts of AES again, and 65023.5 parts, 1.2 parts in silicone, cationic albumen; 0.5 part of CB climbazole, 0.4 part in essence, 0.1 part of JM-115; 0.1 part of vitamin C, 0.1 part of vitamin B1,0.1 part of vitamin E, 55 parts of deionized waters, the blending constituent material proportioning and homogenizing is carried out emulsifying processing; The control oil phase is at 115 ℃ in the emulsion process, and first homogenizing is 15 minutes behind the adding water, recovers normal again and stirs.
5.40 it is canned that perfumery below ℃ finishes post curing 6 hours.
Embodiment 3:
A kind of golden vinegar pearl shining shampoo milk, it is made up of the following weight proportion raw material: 8 parts of golden vinegar, 1.9 parts of serines, 0.9 part of threonine; 0.9 part of leucine, 0.9 part in old vinegar ferment, 1.4 parts of INCROQUAT TMC-80 ECONOL TM22s, 10 parts of AES; 6,502 7 parts, 0.5 part in silicone, cationic albumen, 1.1 parts of CB climbazoles; 0.8 part in essence, 0.4 part of JM-115,0.4 part of vitamin C, 0.4 part of vitamin B1,0.4 part of vitamin E, 65 parts of deionized waters; Wherein golden vinegar total acid 6g/100ml, total amino nitrogen 0.25g/100ml, fixed acid 2.4g/100ml.
A kind of method for preparing of golden vinegar pearl shining shampoo milk:
1. the Fenyang wine Daqu (massive raw stater for alcholic liquor) is mixed by the weight ratio of 1:1 with Sorghum vulgare Pers. and ferment; Article Wen Keda was 30 ℃ in the 3rd day; Fermented to summit in the 4th day, these article extend to four and half, and main fermentation finishes the back sealing descends the article temperature gradually; Get into the after fermentation phase with ferment phase after fermentation phase prolongation end in 10 days to 16 days, temperature keeps 18-20 ℃.
2. old vinegar that aging is good adopts the method for the vacuum and low temperature golden vinegar of purifying, and extracting temperature is 60 ℃ ± 5 ℃, and vacuum be-0.08MPa, reaches the end of purifying of golden vinegar standard, and wherein the concrete preparation technology of golden vinegar sees Chinese patent 200810055592.1.
3. the old vinegar ferment extracts: the old vinegar Daqu (massive raw stater for alcholic liquor) is pulverized with solute: solvent is to soak 48 hours containing in the alcoholic acid solution of 10-20% of 1:1.5; Refluxed once in per 4 hours; Temperature remains on 40-50 ℃, and the isolated by filtration clear liquid is sloughed ethanol with clear liquid and reclaimed reuse in agitated reactor.Then, temperature 45-55 ℃, be concentrated into original volume 1/3 and finish to extract at vacuum-0.08MPa.
4. 1.9 parts of 8 parts of the golden vinegar that will purify and serines, 0.9 part of threonine, 0.9 part of leucine, 0.9 part in old vinegar ferment; 1.4 parts of mixing of INCROQUAT TMC-80 ECONOL TM22 add 10 parts of AES again, and 6,502 7 parts, 0.5 part in silicone, cationic albumen; 1.1 parts of CB climbazoles, 0.8 part in essence, 0.4 part of JM-115; 0.4 part of vitamin C, 0.4 part of vitamin B1,0.4 part of vitamin E, 65 parts of deionized waters, the blending constituent material proportioning and homogenizing is carried out emulsifying processing; The control oil phase is at 115 ℃ in the emulsion process, and first homogenizing is 15 minutes behind the adding water, recovers normal again and stirs.
5.40 it is canned that perfumery below ℃ finishes post curing 6 hours.
Claims (2)
1. golden vinegar pearl shining shampoo milk, it is characterized in that: it is made up of the following weight proportion raw material: golden vinegar 8-11.5 part, serine 1.9-2.2 part; Threonine 0.9-1.2 part, leucine 0.9-1.2 part, old vinegar ferment 0.9-1.2 part; INCROQUAT TMC-80 ECONOL TM22 1.4-1.7 part, AES10-20 part, 65023.5-7 part; Silicone, cationic albumen 0.5-1.2 part, CB climbazole 0.4-1.1 part, essence 0.5-0.9 part; JM-1150.1-0.4 part, vitamin C 0.1-0.4 part, vitaminB10 .1-0.4 part, vitamin E 0.1-0.4 part, deionized water 55-65 part.
2. the method for preparing of a golden vinegar pearl shining shampoo milk: it is characterized in that:
(1) the Fenyang wine Daqu (massive raw stater for alcholic liquor) is mixed by the weight ratio of 1:1 with Sorghum vulgare Pers. and ferment; Article Wen Keda was 30 ℃ in the 3rd day; Fermented to summit in the 4th day, these article extend to four and half, and main fermentation finishes the back sealing descends the article temperature gradually; Get into the after fermentation phase with ferment phase after fermentation phase prolongation end in 10 days to 16 days, temperature keeps 18-20 ℃;
(2) old vinegar that aging is good adopts the method for the vacuum and low temperature golden vinegar of purifying, and the purification temperature is 60 ℃ ± 5 ℃, and vacuum be-0.08MPa, reaches the end of purifying of golden vinegar standard;
(3) the old vinegar ferment extracts: the old vinegar Daqu (massive raw stater for alcholic liquor) is pulverized with solute: solvent is to soak 48 hours containing in the alcoholic acid solution of 10-20% of 1:1.5; Refluxed once in per 4 hours, temperature remains on 40-50 ℃, the isolated by filtration clear liquid; Clear liquid is sloughed ethanol reclaim reuse in agitated reactor; Then, temperature 45-55 ℃, be concentrated into original volume 1/3 and finish to extract at vacuum-0.08MPa;
(4) the golden vinegar 8-11.5 part that will purify and serine 1.9-2.2 part, threonine 0.9-1.2 part, leucine 0.9-1.2 part; Old vinegar ferment 0.9-1.2 part, INCROQUAT TMC-80 ECONOL TM22 1.4-1.7 part is mixed, and adds AES10-20 part again; 65023.5-7 part, silicone, cationic albumen 0.5-1.2 part, CB climbazole 0.4-1.1 part; Essence 0.5-0.9 part, JM-1150.1-0.4 part, vitamin C is part, vitaminB10 .1-0.4 part, vitamin E 0.1-0.4 part, deionized water 55-65 part G.1-0.4; The blending constituent material proportioning and homogenizing is carried out emulsifying processing, and the control oil phase is at 115 ℃ in the emulsion process; First homogenizing is 15 minutes behind the adding water, recovers normal again and stirs;
It is canned that perfumery below (5) 40 ℃ finishes post curing 6 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100792946A CN101357115B (en) | 2008-09-01 | 2008-09-01 | Golden vinegar pearl shining shampoo milk and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100792946A CN101357115B (en) | 2008-09-01 | 2008-09-01 | Golden vinegar pearl shining shampoo milk and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101357115A CN101357115A (en) | 2009-02-04 |
| CN101357115B true CN101357115B (en) | 2012-02-08 |
Family
ID=40329804
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008100792946A Expired - Fee Related CN101357115B (en) | 2008-09-01 | 2008-09-01 | Golden vinegar pearl shining shampoo milk and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101357115B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103655435B (en) * | 2013-04-28 | 2015-08-26 | 钱臻 | A kind of biofermentation hair conditioner and preparation method thereof |
-
2008
- 2008-09-01 CN CN2008100792946A patent/CN101357115B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN101357115A (en) | 2009-02-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105018314B (en) | A kind of purple rice wine rich in anthocyanidin and preparation method thereof | |
| JP2010505441A (en) | Method for producing kaempferol-3-O-rutinoside and skin external preparation composition containing the same | |
| CN103865712B (en) | Taishan radix cynanchi bungei health-care yellow wine and preparation method thereof | |
| CN101357115B (en) | Golden vinegar pearl shining shampoo milk and preparation method thereof | |
| CN102816667A (en) | Ganoderma lucidum polysaccharide nutrition sweet wine and production process | |
| CN108517264A (en) | A kind of fruit wine of nutrition and health care and preparation method thereof | |
| JP2005514943A (en) | Method for producing water-alcohol solutions and products based thereon | |
| CN107890439B (en) | Extraction method of aesculus hippocastanum seed extract and hair washing composition thereof | |
| CN106010914B (en) | A kind of preparation method of mulberry leaf blueness wine | |
| CN103343073A (en) | Production method of longan brandy | |
| KR20100065437A (en) | Manufacturing method for beauty product of nutritive gel type using caviar extracton | |
| CN110585074B (en) | Application of rose essential oil balm in cosmetics | |
| KR100858059B1 (en) | Preparing method of diosmetin from lemon peel and the cosmetic composition containing thereof as active ingredient | |
| CN103834523A (en) | Medlar rice wine | |
| CN106701414A (en) | Flowery-fragrant fenggang wine suitable for women to drink and making method thereof | |
| CN106235319A (en) | A kind of manufacture method of Eugenia javanica Lam ferment | |
| CN106065388A (en) | A kind of looks improving and the skin nourishing wild strawberry sparkling wine and preparation method thereof | |
| CN101972223B (en) | Plant cell agerasia essence | |
| CN102051275B (en) | Novel application of Artemisia rupestris L extract | |
| CN101781617B (en) | Preparation method of thick corn wine | |
| CN1281731C (en) | Nourishing tonic wine made from forest frog and its preparation method | |
| CN111991326A (en) | Maotai-flavor vinasse extract toning lotion | |
| CN1261625A (en) | Saffron wine and its preparing method | |
| CN114276468B (en) | Natural component and application thereof in whitening and increasing skin elasticity | |
| CN114306122B (en) | Freckle-removing whitening component and application thereof in preparation of cosmetics |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20120208 Termination date: 20170901 |