CN101343202A - Composite type micro-element liquid foliage fertilizer and preparation thereof - Google Patents
Composite type micro-element liquid foliage fertilizer and preparation thereof Download PDFInfo
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- CN101343202A CN101343202A CNA2008100291567A CN200810029156A CN101343202A CN 101343202 A CN101343202 A CN 101343202A CN A2008100291567 A CNA2008100291567 A CN A2008100291567A CN 200810029156 A CN200810029156 A CN 200810029156A CN 101343202 A CN101343202 A CN 101343202A
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Abstract
The invention discloses a composite microelement liquid foliar fertilizer, comprising a nutritional ingredient and an auxiliary concentration ingredient; the nutritional ingredient consists of sulfate and polymerizing sodium borate salt; and the auxiliary concentration ingredient is composed of a preservative, a cosolvent, a penetrating agent, a bactericide, a surface active agent and other supplementary materials. The invention meanwhile provides a simple, easy and low-cost preparation method of the foliar fertilizer. The composite microelement liquid foliar fertilizer has both good stability and unfolding property, and can provide enough zinc, manganese, copper and boron nutrients for crops in the meanwhile, all elements interact with one another, crops can absorb the nutrients rapidly, and the nutrient utilization rate is high. The liquid foliar fertilizer has rather low costs, and can save fertilizer and labor costs for peasants.
Description
Technical field
The invention belongs to field of agricultural production technologies, be specifically related to be applied to a kind of composite type micro-element liquid foliage fertilizer of fruit tree.
Background technology
As everyone knows, in the process of growth of crop, trace element zinc, manganese, copper, boron play an important role, and zinc, manganese, copper movability in making object is little, and boron is the difficult element that moves.Zinc plays an important role to the quality that promotes crop reproductive development and raising resistance and fruit.Manganese is that crop carries out the indispensable participant of photosynthesis, and the activity by regulatory enzyme promotes nitrate to be transformed into ammonium nitrogen, improves the freezing tolerance of crop.Copper has stabilization to chlorophyll and other pigments, can prevent that pigment is damaged, and copper can also promote the growth of floral organ, thereby improves setting percentage.Boron plays an important role to the formation of fruit yield and the raising of fruit quality.Especially in bloom early stage, bear fruit phase and the fruit expanding period of fruit tree, it is especially important that boron just seems.Boron promotes building up of crop reproductive organ and grows, and improves setting percentage, reduces malformed fruit, and the fruit growth size evenly can also improve output simultaneously.In case do to lack wherein a kind of trace element in the object, all can cause corresponding physiological disease, thereby influence the normal growth of crop.This shows that zinc, manganese, copper and boron play an important role in the growth and development process of crop, is the essential trace element of plant growth.Can fruit tree well absorb and make good use of zinc, manganese, copper and boron is the important factor that influences fruit yield height and quality quality, and this also is the emphasis of fruit tree leaves leaven research.
The most microelement foliage fertilizer that provides in the market all is a single-element fertilizer, more than two kinds or three kinds all seldom, four kinds little especially, though can play certain effect by using single trace element fertilizer, the assimilated efficiency of element is not high, loses time and the labour yet, and the high-quality microelement foliage fertilizer that the peasant uses now is nearly all from external import, because factor affecting such as its raw material and technology cost an arm and a leg, fertilizer cost is also higher.Because the limitation of technology, the microelement foliage fertilizer overwhelming majority that domestic manufacturer produces is a solid form, and liquid form few can not adapt to pressing for of China's planting fruit trees industry.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, the composite type micro-element liquid type foliar nutrient of a kind of high-quality and efficient zinc, manganese, copper, boron is provided for crop.
A further object of the invention provides the preparation method of described composite type micro-element liquid foliage fertilizer.
Purpose of the present invention is achieved by the following technical programs:
A kind of composite type micro-element liquid foliage fertilizer is provided, comprises nutritive ingredient and auxiliary concentration components; Described nutritive ingredient is made up of vitriol and polymerization boric acid sodium salt; Described auxiliary concentration components is made up of sanitas, solubility promoter, permeate agent, sterilant, tensio-active agent and other auxiliary materials.
The preferred Zinc vitriol of described vitriol, Manganous sulfate monohydrate, Salzburg vitriol and tetraacethyl diethylamine disodium.
Described sanitas optimization citric acid; The preferred propylene glycol of described solubility promoter, phenylcarbinol, formic acid, acetate and diethylene glycol monoethyl ether; The preferred N.F,USP MANNITOL of described permeate agent; The preferred N of described sterilization and tensio-active agent, N-dimethyl tetradecy lamine and N, N-dimethyl cetylamine.
Described other auxiliary materials comprise spices, pigment, tinting material and water.The preferred vanillin food grade,1000.000000ine mesh of described spices; The indigo of described pigment preferred 1% and 1% lemon yellow; The preferred diethylene glycol monoethyl ether of described tinting material.
The invention provides a preferred version of described composite type micro-element liquid foliage fertilizer moiety, form according to described parts by weight by following component:
28 parts of Zinc vitriols;
15 parts of Manganous sulfate monohydrates;
8 parts of Salzburg vitriols;
3 parts of tetraacethyl diethylamine disodiums;
4 parts of polymerization boric acid sodium salts;
0.36 part of citric acid;
0.5 part in formic acid;
0.5 part of acetate;
2.2 parts of propylene glycol;
0.5 part in N.F,USP MANNITOL;
1.0 parts of phenylcarbinols;
0.36 part of diethylene glycol monoethyl ether;
1.2 parts of vanillin food grade,1000.000000ine meshs;
N, 1.5 parts of N-dimethyl tetradecy lamines;
N, 1.4 parts of N-dimethyl cetylamines;
0.1 part of 1% indigo;
1% lemon yellow 0.15 part;
Water surplus.
The present invention provides the preparation method of described composite type micro-element liquid foliage fertilizer simultaneously,
Specifically may further comprise the steps:
(1) earlier water is added reactor, adding tetraacethyl diethylamine disodium then stirs until dissolving fully, add Zinc vitriol more successively, Manganous sulfate monohydrate, Salzburg vitriol, polymerization boric acid sodium salt adds after waiting a kind of material of adding to dissolve fully a kind of down again, treat after four kinds of salt dissolve fully solution to be filtered, form A liquid;
(2) will assist concentration components according to citric acid, formic acid, acetate, propylene glycol, N.F,USP MANNITOL, phenylcarbinol, diethylene glycol monoethyl ether, vanillin food grade,1000.000000ine mesh, N, N-dimethyl tetradecy lamine, N, the order of N-dimethyl cetylamine is dissolved in the water successively, forms B liquid;
(3) B liquid is slowly poured in the A liquid, the limit bevelling stirs, and stirs 15 minutes, mixedly can form C liquid after even;
(4) with the lemon yellow of 1% indigo and 1% C liquid is deployed into blue-greenish colour, can obtains finished product.
Beneficial effect of the present invention is discussed below:
The present invention with propylene glycol, phenylcarbinol, formic acid and acetate as solubility promoter, vitriol and polymerization boric acid sodium salt are dissolved in wherein successively, with citric acid as sanitas, make permeate agent with N.F,USP MANNITOL, with N, N-dimethyl tetradecy lamine and N, N-dimethyl cetylamine is as sterilization and tensio-active agent, make solubility promoter and tinting material with diethylene glycol monoethyl ether, form stable and sprawl effective liquid preparation.
Microelement foliage fertilizer main component among the present invention is vitriol and polymerization boric acid sodium salt, the applicant draws this foliage fertilizer by a large amount of field tests has good effect to crop, various matter interactions in the concentrated assistant, form a kind of special structure, help crop more and well absorb zinc, manganese, copper, four kinds of elements of boron, assimilated efficiency is all than single use trace element fertilizer height, for the peasant has saved artificial and fertilizer cost.Propylene glycol among the present invention, phenylcarbinol etc. are good solvents, do the stable performance that solvent can make formulation with propylene glycol and phenylcarbinol.N.F,USP MANNITOL has good infiltration and diffusion, and it promotes infiltration and the diffusion of solution on blade, promotes crop to trace elements absorbed, the especially absorption of boron.N, N-dimethyl tetradecy lamine and N, N-dimethyl cetylamine is a kind of sterilant, it can help to kill the unwanted bacteria on crop blade face.N, N-dimethyl tetradecy lamine and N, N-dimethyl cetylamine or tensio-active agent, it has soup and well sprawls effect, the nutrition absorption excellent in efficiency.As sanitas, it makes this invention that good preservative effect be arranged with citric acid in the present invention.The present invention also with vanillin food grade,1000.000000ine mesh as spices, it comes this product with other product differentiation from smell.Indigo with 1% and 1% lemon yellow furnishing blue-greenish colour are as the characteristic color of this invention.
In sum, the invention has the beneficial effects as follows:
(1) the present invention can provide the required zinc that grows, manganese, copper and boron nutrient for crop, has good stability and plate-out ability, and crop absorbs fast, and the plant recovery of nutrient height well guarantees the needs that grow of fruit tree;
(2) the present invention can provide the required zinc that grows, manganese, copper and boron nutrient simultaneously for crop, has solved the time and the labour costs that use single-element fertilizer.
(3) the present invention has filled up the vacancy of domestic market, well imported product outside the subrogate country.
Embodiment
Further describe the present invention below in conjunction with specific embodiment.
1 one kinds of composite type micro-element liquid foliage fertilizers of embodiment, mainly form according to described parts by weight by following component:
28 parts of Zinc vitriols;
15 parts of Manganous sulfate monohydrates;
8 parts of Salzburg vitriols;
3 parts of tetraacethyl diethylamine disodiums;
4 parts of polymerization boric acid sodium salts;
0.36 part of citric acid;
0.5 part in formic acid;
0.5 part of acetate;
2.2 parts of propylene glycol;
0.5 part in N.F,USP MANNITOL;
1.0 parts of phenylcarbinols;
0.36 part of diethylene glycol monoethyl ether;
1.2 parts of vanillin food grade,1000.000000ine meshs;
N, 1.5 parts of N-dimethyl tetradecy lamines;
N, 1.4 parts of N-dimethyl cetylamines;
0.1 part of 1% indigo;
1% lemon yellow 0.15 part;
Water surplus.
Concrete preparation method is as follows:
(1) earlier water is added reactor, adding tetraacethyl diethylamine disodium then stirs until dissolving fully, add Zinc vitriol more successively, Manganous sulfate monohydrate, Salzburg vitriol, polymerization boric acid sodium salt adds after waiting a kind of material of adding to dissolve fully a kind of down again, treat after four kinds of salt dissolve fully solution to be filtered, form A liquid;
(2) will assist concentration components according to citric acid, formic acid, acetate, propylene glycol, N.F,USP MANNITOL, phenylcarbinol, diethylene glycol monoethyl ether, vanillin food grade,1000.000000ine mesh, N, N-dimethyl tetradecy lamine, N, the order of N-dimethyl cetylamine is dissolved in the water successively, forms B liquid;
(3) B liquid is slowly poured in the A liquid, the limit bevelling stirs, and stirs 15 minutes, mixedly can form C liquid after even;
(4) with the lemon yellow of 1% indigo and 1% C liquid is deployed into blue-greenish colour, can obtains finished product.
The test effect of embodiment 2 composite type micro-element liquid foliage fertilizers of the present invention on lichee
In beautiful fruit field, west, Shenzhen, spray the glutinous rice wrapped in lotus leaves of the age of tree about 13 years for 1000 times with composite type micro-element liquid foliage fertilizer dilution of the present invention, use at fruit development period, obtain good effect.Can find out that by table 1, table 2 yield increased increases by 13.8%, the pol comparison is according to increasing by 6.9%.
The contrast of table 1 output
| Handle | Single plant yield (Kg) | 30 fruit ear output (Kg) | Average simple grain is heavy (g) really | Stimulation ratio (%) | 30 fruit ear fruit quantity (grain) | The average setting amount of every fringe (grain) |
| Compound trace element fertilizer | 49.2 | 6.2 | 26.3 | 13.8 | 235 | 7.83 |
| Contrast (spray clear water) | 21.6 | 3.4 | 23.1 | -------- | 148 | 4.93 |
Table 2 pulp pol contrast (representing) with soluble solid
The test effect of embodiment 3 composite type micro-element liquid foliage fertilizers of the present invention on paddy rice
On Agricultural University Of South China education experiment farm, spray paddy rice for 1000 times with the fertile dilution of composite type micro-element liquid of the present invention, by table 3 as can be seen, yield increased increases by 8.3%, and the comparison of the real grain of every fringe number is according to increasing by 6, and setting percentage also is significantly increased.
Table 3
The test effect of embodiment 4 composite type micro-element liquid foliage fertilizers of the present invention on vegetables
On Agricultural University Of South China education experiment farm, spray green cucumber for 1000 times with the fertile dilution of composite type micro-element liquid of the present invention, by table 4 as can be seen, yield increased increases by 19.6%, and the income comparison increases 362 yuan according to mu.
Table 4
| Handle | Area (mu) | Gross output (Kg) | Folding per mu yield (Kg) | 7 average prices (unit) | Per mu yield value (unit) | Comparison is according to increasing (%) | Comparison increases (unit) according to mu |
| Compound trace element fertilizer | 0 .12 | 281.5 | 2345.9 | 0.94 | 2205.4 | 19.6 | 362.7 |
| Contrast | 0 .15 | 294.0 | 1960.0 | 0.94 | 1842.4 | ------ | ----------- |
Claims (7)
1, a kind of composite type micro-element liquid foliage fertilizer is characterized in that comprising nutritive ingredient and auxiliary concentration components; Described nutritive ingredient is made up of vitriol and polymerization boric acid sodium salt; Described auxiliary concentration components is made up of sanitas, solubility promoter, permeate agent, sterilant, tensio-active agent and other auxiliary materials.
2, composite type micro-element liquid foliage fertilizer according to claim 1 is characterized in that described vitriol is Zinc vitriol, Manganous sulfate monohydrate, Salzburg vitriol and tetraacethyl diethylamine disodium.
3, composite type micro-element liquid foliage fertilizer according to claim 1 is characterized in that described sanitas is a citric acid; Described solubility promoter is propylene glycol, phenylcarbinol, formic acid, acetate and diethylene glycol monoethyl ether; Described permeate agent is a N.F,USP MANNITOL; Described sterilization and tensio-active agent are N, N-dimethyl tetradecy lamine and N, N-dimethyl cetylamine.
4, composite type micro-element liquid foliage fertilizer according to claim 1 is characterized in that described other auxiliary materials comprise spices, pigment, tinting material and water.
5, composite type micro-element liquid foliage fertilizer according to claim 4 is characterized in that described spices is vanillin food grade,1000.000000ine mesh; Described pigment is the lemon yellow of 1% indigo and 1%; Described tinting material is a diethylene glycol monoethyl ether.
6, according to claim 1,2,3,4 or 5 described composite type micro-element liquid foliage fertilizers, it is characterized in that forming according to described parts by weight by following component:
28 parts of Zinc vitriols;
15 parts of Manganous sulfate monohydrates;
8 parts of Salzburg vitriols;
3 parts of tetraacethyl diethylamine disodiums;
4 parts of polymerization boric acid sodium salts;
0.36 part of citric acid;
0.5 part in formic acid;
0.5 part of acetate;
2.2 parts of propylene glycol;
0.5 part in N.F,USP MANNITOL;
1.0 parts of phenylcarbinols;
0.36 part of diethylene glycol monoethyl ether;
1.2 parts of vanillin food grade,1000.000000ine meshs;
N, 1.5 parts of N-dimethyl tetradecy lamines;
N, 1.4 parts of N-dimethyl cetylamines;
0.1 part of 1% indigo;
1% lemon yellow 0.15 part;
Water surplus.
7, the preparation method of the described composite type micro-element liquid foliage fertilizer of a kind of claim 6 is characterized in that may further comprise the steps:
(1) earlier water is added reactor, adding tetraacethyl diethylamine disodium then stirs until dissolving fully, add Zinc vitriol more successively, Manganous sulfate monohydrate, Salzburg vitriol, polymerization boric acid sodium salt adds after waiting a kind of material of adding to dissolve fully a kind of down again, treat after four kinds of salt dissolve fully solution to be filtered, form A liquid;
(2) will assist concentration components according to citric acid, formic acid, acetate, propylene glycol, N.F,USP MANNITOL, phenylcarbinol, diethylene glycol monoethyl ether, vanillin food grade,1000.000000ine mesh, N, N-dimethyl tetradecy lamine, N, the order of N-dimethyl cetylamine is dissolved in the water successively, forms B liquid;
(3) B liquid is slowly poured in the A liquid, the limit bevelling stirs, and stirs 15 minutes, mixedly can form C liquid after even;
(4) with the lemon yellow of 1% indigo and 1% C liquid is deployed into blue-greenish colour, can obtains finished product.
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| CN101665390B (en) * | 2009-09-08 | 2012-08-22 | 华南农业大学 | Suspension type liquid compound fertilizer and preparation method thereof |
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| CN103664359A (en) * | 2013-11-25 | 2014-03-26 | 华南农业大学 | High-phosphorus high-zinc liquid compound fertilizer and preparation method thereof |
| CN105110868B (en) * | 2015-07-24 | 2018-06-19 | 南宁宇益源农业科技发展有限公司 | A kind of environmental type foliar fertilizer and preparation method thereof |
| CN105110868A (en) * | 2015-07-24 | 2015-12-02 | 南宁宇益源农业科技发展有限公司 | Green environment-friendly leaf fertilizer, and preparation method thereof |
| CN106259329A (en) * | 2016-07-20 | 2017-01-04 | 湖南农业大学 | A kind of Oryza sativa L. resistance cadmium agent |
| CN109265232A (en) * | 2017-07-17 | 2019-01-25 | 湖南林之神生物科技有限公司 | A kind of liquid formulations being exclusively used in tea oil tree are fertile and its apply |
| CN107691139A (en) * | 2017-08-04 | 2018-02-16 | 农业部环境保护科研监测所 | Carry out the method that leaf is produced with rape safe and high quality in cadmium mild or moderate pollution vegetable plot |
| CN107691139B (en) * | 2017-08-04 | 2019-10-15 | 农业部环境保护科研监测所 | Carry out the method that leaf is produced with rape safe and high quality in cadmium mild or moderate pollution vegetable plot |
| CN107628896A (en) * | 2017-09-12 | 2018-01-26 | 四川鑫圣生物科技有限公司 | A kind of garlic special fertilizer and preparation method thereof |
| CN108456067A (en) * | 2018-03-30 | 2018-08-28 | 蚌埠市代双莲藕种植专业合作社 | A kind of lotus rhizome foliar fertilizer |
| CN112174737A (en) * | 2020-10-10 | 2021-01-05 | 河南华智营养科技有限公司 | Micro-fertilizer for foliar spraying of unmanned aerial vehicle |
| CN112715539A (en) * | 2021-01-28 | 2021-04-30 | 菲吉乐科(南京)生物科技有限公司 | Auxiliary penetrating agent suitable for bacteriophage to penetrate into tuber crops and preparation method and application thereof |
| CN113040140A (en) * | 2021-01-28 | 2021-06-29 | 菲吉乐科(南京)生物科技有限公司 | Auxiliary penetrating agent suitable for bacteriophage to be immersed into lianas and woody plants and preparation method and application thereof |
| CN112715539B (en) * | 2021-01-28 | 2022-06-17 | 菲吉乐科(南京)生物科技有限公司 | Auxiliary penetrating agent suitable for bacteriophage to penetrate into tuber crops and preparation method and application thereof |
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