CN101342129A - Concave-convex stick peppermint recuperating shampoo - Google Patents

Concave-convex stick peppermint recuperating shampoo Download PDF

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Publication number
CN101342129A
CN101342129A CNA2008100218345A CN200810021834A CN101342129A CN 101342129 A CN101342129 A CN 101342129A CN A2008100218345 A CNA2008100218345 A CN A2008100218345A CN 200810021834 A CN200810021834 A CN 200810021834A CN 101342129 A CN101342129 A CN 101342129A
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attapulgite
sludge slurry
mint
sodium
hair
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CN101342129B (en
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许庆华
贾剑
许盛英
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Abstract

The invention discloses attapulgite mint conditioning shampoo, which has the technical proposal that the attapulgite mint conditioning shampoo is composed of modified pasty attapulgite clay, mint, aloe, cocamidopropyl amine oxide, coconut diethanolamide, polyquaternium-7, citric acid, nipagin methyl ester, nipagine propyl ester and deionized water. The attapulgite mint conditioning shampoo has the production method of purification, sodium modification, acidification, feed proportioning, pulverization and beating, grinding, high-speed stirring, emulsification, vacuum degassing and canning for obtaining the finished product of attapulgite mint conditioning shampoo. The attapulgite mint conditioning shampoo can speed up blood circulation of scalp, has very strong penetrability and antistatic action as well as can improve the handle of hair, facilitates the hair being combed, and plays roles of conditioning and nursing hair and retaining hair beauty. The attapulgite mint conditioning shampoo is suitable for hairdressing and nursing.

Description

Concave-convex stick peppermint recuperating shampoo
Technical field
The present invention relates to shampoo, be specifically related to a kind of concave-convex stick peppermint recuperating shampoo.
Background technology
Shampoo is a kind of oil-in-water type product, is opaque emulsion form, and it is with its strong detergency, and has the effect of hair care hair care concurrently and very popular.
Remove the dirt and the superfluous oils and fats of hair, require shampoo to have certain cleaning strength, but undue defat meeting destroys the apparent condition of hair, scalp irritation, can cause alopecia, broken hair, scalp is itched and is stimulated eyes. so the necessary detergency of shampoo is moderate, fine and smooth thick foam is easier is simultaneously accepted by consumers in general, in recent years, the inherent quality of people's pay attention to day by day shampoo, particularly the zest to eyes and skin is little, and requires the oils and fats of shampoo removal skin within reason and hair, and is relatively gentleer to skin and mucosa, shampoo can impel hair soft and high resilience, and can increase the gloss of hair and be easy to rinsing.Recuperating shampoo can clean people's scalp and the dirt on the hair, has introduced the effect of hair care again, and has made the easy combing of hair, plays conditioning, nursing, keeps hair effect attractive in appearance.
Gong Ying shampoo is synthetic with industrial chemicals mostly in the market, is difficult to satisfy the demands of consumers, and improper use also can cause bad phenomenon generations such as the dry bifurcated of hair, easily broken, curling and scalp allergy.
Chinese patent publication number CN1021385, open day is on October 12nd, 1988, name is called " a kind of highly effective liquid detergent and production method ", discloses " a kind of high-efficient washing spirit that is used for the sanitary purpose washing aspect of being made special auxiliary agent by inorganic mineral raw material bentonite and attapulgite.It is to make anion surfactant by preparing a certain amount of sodium lauryl sulphate, and CMC makes thickening, stabilizing agent, and lanoline is made conditioner and a certain amount of bentonite and attapulgite and made special auxiliary agent, spice, pigment and mix through heated and stirred.The present invention is cheap, and its cost of material only is about 75% of general shampoo and a shampoo paste.Strong detergency, consumption are few, nontoxic.”
The weak point of above-mentioned patent is not select for use in this technology to make special auxiliary agent through the inorganic mineral raw material bentonite and the attapulgite of purifying and modification is handled, and its dispersibility and suspendability are all poor, therefore can have influence on the product quality of highly effective liquid detergent.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, a kind of concave-convex stick peppermint recuperating shampoo is provided.
Concave-convex stick peppermint recuperating shampoo is made up of modified cream attapulgite clay, Herba Menthae, Aloe, cocamidopropyl propyl amide amine oxide, lauric acid amide of ethanol, polyquaternary ammonium salt-7, citric acid, methyl hydroxybenzoate, propylparaben and deionized water.
The production method of concave-convex stick peppermint recuperating shampoo is purification, sodium, acidify, batching, pulverizing making beating, grinding, high-speed stirred, emulsifying, vacuum outgas, cannedly is the finished product of concave-convex stick peppermint recuperating shampoo.
Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m 2More than/the g.Use " wet beneficiation craft of attapulgite " and " attapulgite ore pul making production technology ", the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of attapulgite sludge slurry; Through the lip lipstick attapulgite clay after sodium processing and the acidification, it is the special good natural magnesium aluminium silicate gel of a kind of thixotropy and gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
Herba Menthae is a herbaceos perennial, and stem and leaf contains protein, multivitamin, Oleum menthae and trace element, can quicken the scalp blood circulation, and refreshment is removed impurity after tapping, and it is standby to clean chopping.
Contain microcomponents such as the hydrated product Fructus Vitis viniferae acid of polysaccharide, sweet sugared dew, alduronic acid, hydrated protein enzyme, bio-hormone, hormone, proteins,vitamins,minerals in the Aloe, Aloe has the natural moisture preserving factor, it can replenish hair moisture, recover the function of collagen protein, prevent that hair is sparse, withered and yellow, matt.Remove impurity after tapping, it is standby to clean chopping.
The cocamidopropyl propyl amide amine oxide has good foaming, thickening, conditioning and antistatic property, can significantly improve the comprehensive washability of product, under general consumption, to skin and hair as mild as a dove.Good with anion, cation, amphion and non-ionic surface active agent intermiscibility, have good antistatic behaviour, be ideal conditioner.
Lauric acid amide of ethanol is amber thick liquid, and is soluble in water, has functions such as good foaming, steady bubble, infiltration decontamination, anti-hard water.Belong to non-ionic surface active agent, the compatibility thickening effect is obvious especially with it when anion surfactant is acidity, can with kinds of surface activating agent compatibility.
Polyquaternary ammonium salt-the 7th, a kind of cationic copolymer, the charge density height, in the very wide scope of pH value, can both keep good stability, can with most of cationes and amphoteric surfactant compatibility, can be hair conditioning performance preferably is provided, the hair that can give people is with softness, and the silkiness shape is felt.
Citric acid has gentle frank tart flavour, can improve and adjust the pH value of shampoo, improves the performance of surfactant.
Methyl hydroxybenzoate has the broad-spectrum antibacterial effect, to Gram-positive, and negative bacteria, yeast and mycete have very strong inhibitory action, and the low and safety economy of working concentration uses effect duration long.Methyl hydroxybenzoate is compatible with various chemical substances easily, and the composite use of methyl hydroxybenzoate and propylparaben is to reach better antiseptic effect.
The present invention is achieved by following technical proposals:
1, the batching of concave-convex stick peppermint recuperating shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30~60%, Herba Menthae 5~25%, Aloe 2~10%, cocamidopropyl propyl amide amine oxide 0.5~5%, lauric acid amide of ethanol 0.5~5%, polyquaternary ammonium salt-70.5~5%, citric acid 0.01~1%, methyl hydroxybenzoate 0.05~0.5%, propylparaben 0.05~0.5% and deionized water 10~40%.
Described modified cream attapulgite clay is on attapulgite ore pul making production technology basis, and attapulgite sludge slurry is carried out sodium processing, acidification, washing and sieve decontamination, and the mud of process post precipitation is modified cream attapulgite clay.
Attapulgite ore pul making production technology is: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is attapulgite sludge slurry finished product.
Above-mentioned production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15~35% and water 65~85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1~7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95~99.5% and sodium hydroxide 0.5~5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1~3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92~99.5% after the sodium and concentration are 98% sulphuric acid 0.5~8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25~65% and water 35~75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5~40% and water 60~95%.
The pH value of the immersion water of emitting is neutral meta-acid, can be used to produce the raw material of transparent shampoo.
2, the production method of concave-convex stick peppermint recuperating shampoo: 1. the batching adding of concave-convex stick peppermint recuperating shampoo being pulverized in the beater and pulverize, is the mixture of concave-convex stick peppermint recuperating shampoo behind the pulverizing making beating mix homogeneously; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex stick peppermint recuperating shampoo.
Concave-convex stick peppermint recuperating shampoo uses modified cream attapulgite clay to be primary raw material, does not need to add in addition thickening agent and wetting agent, not only can improve the quality of shampoo, can also reduce production costs greatly.
Behind the processing of attapulgite sludge slurry process sodium, acidification, washing and the sieve decontamination, lip lipstick attapulgite clay becomes a kind of thixotropy and the special good natural magnesium aluminium silicate gel of gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
Concave-convex stick peppermint recuperating hair washing perfume (or spice) can quicken the scalp blood circulation, and penetration is very strong, and existing antistatic property can improve the feel of hair again, makes the easy combing of hair, plays conditioning, nursing and the effect attractive in appearance of maintenance hair.Be easy to carry out rinsing after using the concave-convex stick peppermint recuperating shampoo hair washing, impel hair softness Paint Gloss.
People are in the hair washing process, concave-convex stick peppermint recuperating shampoo has exquisiteness and abundant foam, not only can make hair well absorb nutrition in the concave-convex stick peppermint recuperating shampoo, relatively gentleer to eyes, hair and skin, nonirritant, and concave-convex stick peppermint recuperating shampoo can also adsorb and remove foreign material such as sweat mixed with dirt on the hair, dust, microorganism, dandruff, abnormal flavour, keeps the cleaning of scalp and hair and attractive in appearance
Concave-convex stick peppermint recuperating shampoo is applicable to the hair caring nursing.
The specific embodiment
The invention will be further described below in conjunction with embodiment:
1, the batching of concave-convex stick peppermint recuperating shampoo is made up of following component by weight percentage: modified cream attapulgite clay 35%, Herba Menthae 15%, Aloe 8%, cocamidopropyl propyl amide amine oxide 4.5%, polyquaternary ammonium salt-72.5%, lauric acid amide of ethanol 1%, citric acid 0.3%, methyl hydroxybenzoate 0.15%, propylparaben 0.05% and deionized water 33.5%.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 30% and water 70%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 3 days through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 98% and sodium hydroxide 2%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 2 days through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 97% after the sodium and concentration are 98% sulphuric acid 3%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 40 and water 60% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30% and water 70%.
2, the production method of concave-convex stick peppermint recuperating shampoo: 1. the batching adding of concave-convex stick peppermint recuperating shampoo being pulverized in the beater and pulverize, is the mixture of concave-convex stick peppermint recuperating shampoo behind the pulverizing making beating mix homogeneously; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex stick peppermint recuperating shampoo.

Claims (1)

1, a kind of concave-convex stick peppermint recuperating shampoo, it is characterized in that the batching of concave-convex stick peppermint recuperating shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30~60%, Herba Menthae 5~25%, Aloe 2~10%, cocamidopropyl propyl amide amine oxide 0.5~5%, lauric acid amide of ethanol 0.5~5%, polyquaternary ammonium salt-7 0.5~5%, citric acid 0.01~1%, methyl hydroxybenzoate 0.05~0.5%, propylparaben 0.05~0.5% and deionized water 10~40%;
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15~35% and water 65~85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1~7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95~99.5% and sodium hydroxide 0.5~5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1~3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92~99.5% after the sodium and concentration are 98% sulphuric acid 0.5~8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25~65% and water 35~75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5~40% and water 60~95%.
CN2008100218345A 2008-08-25 2008-08-25 Attapulgite peppermint recuperating shampoo Expired - Fee Related CN101342129B (en)

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