CN101292667A - Farming veterinarian disinfectant liquid and its preparation - Google Patents
Farming veterinarian disinfectant liquid and its preparation Download PDFInfo
- Publication number
- CN101292667A CN101292667A CN 200810055233 CN200810055233A CN101292667A CN 101292667 A CN101292667 A CN 101292667A CN 200810055233 CN200810055233 CN 200810055233 CN 200810055233 A CN200810055233 A CN 200810055233A CN 101292667 A CN101292667 A CN 101292667A
- Authority
- CN
- China
- Prior art keywords
- amino
- chlorine dioxide
- acid salt
- nano silver
- propiolactone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a herding veterinarian sterilizing water, which is widely applicable for the disinfection and sterilization of various cultured species in different herding and cultivation industries, and aims at high sterilizing effects, good stability and high safety performance. The ingredients of the sterilizing water of the invention by weight percentage are as follows: 0.4 to 0.9 percent of type B propiolactone, 0.2 to 0.4 percent of amino acid hydrochloride, 0.01 to 0.06 percent of stable chlorine dioxide, 0.1 to 4 percents of activated antibacterial factor Lactoferrin, 0.05 to 0.2 percent of nano silver suspension, and the other is purified water. The preparation method of the sterilizing water of the invention comprises that: the type B propiolactone is heated and dissolved in water, and added with nano silver suspension to form a mixture indicator; the amino acid hydrochloride, the stable chlorine dioxide and the activated antibacterial factor are respectively heated, dissolved and coated, and the coated amino acid dydrochloride is added into the mixture indicator, well stirred, and cooled and packed.
Description
Technical field
The present invention relates to a kind of animal and veterinary thimerosal and preparation method thereof.
Background technology
The existing disinfectant products kind of animal and veterinary industry is more, as bleaching powder, Peracetic acid, sodium dichloro cyanurate, formalin, hydrogen peroxide, potassium permanganate, sym-closene etc., because all toxic and corrosivity of these products, penetrating odor is arranged, influence to water quality is bigger, environment there is pollution, bigger to the livestock-raising growth effect, to being sterilized article certain damage is arranged.Therefore the animal and veterinary industry wishes to have the substituted type sterile products of a kind of high-efficiency low-toxicity, safety and stability always, to reduce the pollution to environment as far as possible, reduces the animal that is sterilized and the influence of article.
Summary of the invention
The present invention seeks to overcome the deficiency of above-mentioned prior art, a kind of germicidal efficiency height, good stability are provided, to human body and cultivated animals nonhazardous, to environment and water nonpollution, animal and veterinary thimerosal that security performance is high, and the preparation method of this thimerosal.
The present invention is mainly by selecting suitable component and rationally be mixed, again through heat, series of process step such as dissolving, polymerization, cooling, bag quilt and making.
The present invention's prescription by weight percentage is: B-mode propiolactone: 0.4-0.9%; Amino-acid salt hydrochlorate: 0.2-0.4%; Stability chlorine dioxide: 0.01-0.06%; Active antibacterial factor lactoferrin: 0.1-4%; Nano Silver suspension: 0.05-0.2%; Add purified water to 100%.
The Nano Silver suspension is to be that aqueous gelatin solution and the concentration of 0.001-0.05g/l is that the silver nitrate of 0.001-0.06mol/l mixes with concentration, adding concentration is that the water-soluble reductant ferrous oxalate of 0.001-0.03g/l reduces silver nitrate, and obtaining particle diameter is 10-50nm nano-Ag particles suspension; Ferrous oxalate be by ferrous sulfate be added in the excessive Potassium Oxalate Solution with etc. mole react, and add oxalic acid solution transferred to about pH=6.0.
Used B-mode propiolactone, amino-acid salt hydrochlorate, stability chlorine dioxide and active antibacterial factor lactoferrin are pulvis, in the prescription all by the weight of pulvis; By weight percentage silver content generally is 0.025-0.2% in the Nano Silver suspension.
Nano-silver ionic causes the microbial activity composition to destroy or produces by haptoreaction and hinders, when arriving the microbial cell film Deng micro silver ion, because of the latter electronegative, rely on Coulomb attraction, the two is adsorbed mutually, silver ion and mycoprotein enzyme-SH combines, and make this enzyme loss of activity and can't survive; B-mode propiolactone molecule has the tetravalence lactonic ring, and the respond of height is arranged; It can react with the material that contains carboxyl, hydroxyl, amino, sulfydryl, and main and protein reacts, and and microorganism DNA (deoxyribonucleic acid) (DNA), ribonucleic acid (RNA) generation alkylated reaction causes bacteria inactivation rate.Chlorine dioxide can see through cells of microorganisms wall and cell membrane fast, and oxidation destroys biology enzyme or amino acid wherein, thus killing microorganisms.The amino-acid salt hydrochlorate is as the main sterilizing component, amino-acid salt in this component has very high activity in polymerisation, make product be electropositive, so easily by each bacterioid of common electronegative property, viral adsorbed, thereby suppressed the splitting function of bacterium, virus, lost its reproductive function, in addition the film that forms of polymer, stopped up the respiration channel of microorganism, microorganism is choked to death.The active antibacterial factor is the natural polypeptides compound that extracts from animal, and the product after the degradable sterilization decomposes the compound than minor structure, avoids being subjected in the sterilization process interference of organic matter and protein.
The preparation method of animal and veterinary thimerosal of the present invention is:
(1) B-mode propiolactone is heated to about 40 ℃ and soluble in water, make 1% the aqueous solution, be cooled to room temperature then.
(2) add the Nano Silver suspension, become mixed liquor.
(3) amino-acid salt hydrochlorate, stability chlorine dioxide, the active antibacterial factor are heated to about 40 ℃ dissolving, bag quilt respectively; Soon coated on amino-acid salt hydrochlorate surface as stability chlorine dioxide, the active antibacterial factor lactoferrin of wall material, form microcapsule structure.
(4) will wrap by after have active amino-acid salt hydrochlorate and join in the mixed liquor, stir, carry out packing after the cooling.
Thimerosal of the present invention extensively is suitable for the sterilizing of each livestock-raising industry to various breed species.Relevant experiment shows, adding nano-silver antiseptic solution and the common thimerosal that does not add Nano Silver in the thimerosal of the present invention, to compare the sterilizing rate higher, and stability is better, and to human body and cultivated animals nonhazardous, harmless to the breed species that are sterilized sterilization.Usage is easy, is convenient to promote.To environment and water nonpollution, security performance height.
Description of drawings
Fig. 1 is a nano-Ag particles stereoscan photograph (SEM) in the Nano Silver suspension.
Embodiment
Embodiment 1; The present invention's concrete prescription by weight percentage is: Nano Silver suspension 0.05-0.2%; B-mode propiolactone 0.5-0.9%; Stability chlorine dioxide 0.01-0.06%; Amino-acid salt hydrochlorate 0.3-0.4%; Lactoferrin 0.2-4%; Add purified water to 100%.
Compare with the common thimerosal that does not add Nano Silver, the every 100ml of present embodiment thimerosal is 90% to the sterilization rate of animals such as horse, and common thimerosal is 63%.The present embodiment product is primarily aimed at Perissodactyla, such as the strong animal of immunocompetences such as horse, requires dosage fewer.
Embodiment 2; The present invention's another concrete prescription by weight percentage is: Nano Silver suspension 0.05-0.16%; B-mode propiolactone 0.5-0.8%, stability chlorine dioxide 0.01-0.06%, amino-acid salt hydrochlorate 0.2-0.4%, lactoferrin 0.1-4%; Purified water adds to 100%.
Compare with the common thimerosal that does not add Nano Silver, the every 90ml of present embodiment thimerosal is 93% to the sterilization rate of animals such as sheep, and common thimerosal is 70%.The present embodiment product is primarily aimed at cloven-hoofed animal, such as the moderate animal of immunocompetences such as sheep, requires dosage moderate.
Embodiment 3; The present invention's another concrete prescription by weight percentage is: Nano Silver suspension 0.05-0.10%, B-mode propiolactone 0.4-0.8%, stability chlorine dioxide 0.01-0.05%, amino-acid salt hydrochlorate 0.2-0.4%; Lactoferrin 0.2-3%; Add purified water to 100%.
Compare with the common thimerosal that does not add Nano Silver, the every 60ml of present embodiment thimerosal is 92% to the sterilization rate of poultries such as chicken, and common thimerosal is 71%.Present embodiment is primarily aimed at poultries such as chicken, immunocompetence relatively a little less than, require dosage also less.
Claims (3)
1, a kind of animal and veterinary thimerosal is characterized in that prescription by weight percentage is: B-mode propiolactone: 0.4-0.9%; Amino-acid salt hydrochlorate: 0.2-0.4%; Stability chlorine dioxide: 0.01-0.06%; Active antibacterial factor lactoferrin: 0.1-4%; Nano Silver suspension: 0.05-0.2%; Add purified water to 100%;
The Nano Silver suspension is to be that aqueous gelatin solution and the concentration of 0.001-0.05g/l is that the silver nitrate of 0.001-0.06mol/l mixes with concentration, adding concentration is that the water-soluble reductant ferrous oxalate of 0.001-0.03g/l reduces silver nitrate, and obtaining particle diameter is 10-50nm nano-Ag particles suspension;
Used B-mode propiolactone, amino-acid salt hydrochlorate, stability chlorine dioxide and active antibacterial factor lactoferrin are pulvis, in the prescription all by the weight of pulvis; By weight percentage silver content generally is 0.025-0.2% in the Nano Silver suspension.
2, animal and veterinary thimerosal as claimed in claim 1, it is characterized in that ferrous oxalate be by ferrous sulfate be added in the excessive Potassium Oxalate Solution with etc. mole react, and add oxalic acid solution transferred to about pH=6.0.
3, the preparation method of animal and veterinary thimerosal as claimed in claim 1 is characterized in that:
(1) B-mode propiolactone is heated to about 40 ℃ and soluble in water, make 1% the aqueous solution, be cooled to room temperature then;
(2) add the Nano Silver suspension, become mixed liquor;
(3) amino-acid salt hydrochlorate, stability chlorine dioxide, the active antibacterial factor are heated to about 40 ℃ dissolving, bag quilt respectively; Soon coated on amino-acid salt hydrochlorate surface as stability chlorine dioxide, the active antibacterial factor lactoferrin of wall material, form microcapsule structure;
(4) will wrap by after have active amino-acid salt hydrochlorate and join in the mixed liquor, stir, carry out packing after the cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810055233 CN101292667A (en) | 2008-06-18 | 2008-06-18 | Farming veterinarian disinfectant liquid and its preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810055233 CN101292667A (en) | 2008-06-18 | 2008-06-18 | Farming veterinarian disinfectant liquid and its preparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101292667A true CN101292667A (en) | 2008-10-29 |
Family
ID=40063419
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200810055233 Pending CN101292667A (en) | 2008-06-18 | 2008-06-18 | Farming veterinarian disinfectant liquid and its preparation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101292667A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102499261A (en) * | 2011-11-17 | 2012-06-20 | 中国科学院宁波材料技术与工程研究所 | Preparation method for antibacterial agent |
| US8992831B2 (en) | 2009-09-25 | 2015-03-31 | E. I. Du Pont De Nemours And Company | Stabilized chlorine dioxide to preserve carbohydrate feedstocks |
| CN107242233A (en) * | 2017-07-10 | 2017-10-13 | 四川蓝博兴科技有限公司 | Composite leather mildewproof bacteria remover and preparation method thereof |
| CN107572637A (en) * | 2016-07-04 | 2018-01-12 | 郑彬红 | A kind of quantum bactericide |
| CN110484748A (en) * | 2019-09-06 | 2019-11-22 | 中南大学 | A method of the selective recovery silver from discarded circuit board |
| CN116790577A (en) * | 2023-08-17 | 2023-09-22 | 中国海关科学技术研究中心 | RNA preservation solution and application thereof |
-
2008
- 2008-06-18 CN CN 200810055233 patent/CN101292667A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8992831B2 (en) | 2009-09-25 | 2015-03-31 | E. I. Du Pont De Nemours And Company | Stabilized chlorine dioxide to preserve carbohydrate feedstocks |
| US9504710B2 (en) | 2009-09-25 | 2016-11-29 | E I Du Pont De Nemours And Company | Stabilized chlorine dioxide to preserve carbohydrate feedstocks |
| CN102499261A (en) * | 2011-11-17 | 2012-06-20 | 中国科学院宁波材料技术与工程研究所 | Preparation method for antibacterial agent |
| CN107572637A (en) * | 2016-07-04 | 2018-01-12 | 郑彬红 | A kind of quantum bactericide |
| CN107242233A (en) * | 2017-07-10 | 2017-10-13 | 四川蓝博兴科技有限公司 | Composite leather mildewproof bacteria remover and preparation method thereof |
| CN110484748A (en) * | 2019-09-06 | 2019-11-22 | 中南大学 | A method of the selective recovery silver from discarded circuit board |
| CN116790577A (en) * | 2023-08-17 | 2023-09-22 | 中国海关科学技术研究中心 | RNA preservation solution and application thereof |
| CN116790577B (en) * | 2023-08-17 | 2023-11-17 | 中国海关科学技术研究中心 | RNA preservation solution and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101292667A (en) | Farming veterinarian disinfectant liquid and its preparation | |
| CN100415100C (en) | Active disinfectant germicide and method for preparing same | |
| Ivanov | Treatment of broiler litter with organic acids | |
| CN103011379A (en) | Aquaculture detoxification water purification agent | |
| CN108191073A (en) | A kind of water body for aquaculture removing toxic substances resisting stress pulvis and its manufacture craft | |
| CN109197894A (en) | Instant compound Potassium Monopersulfate disinfectant of environmental protection and preparation method thereof | |
| CN112335677A (en) | Chlorine dioxide solution and preparation method thereof | |
| CN109221102A (en) | A kind of antibacterial new material | |
| CN101027988A (en) | Disinfectant for livestock cultivation | |
| WO2000033852A1 (en) | Compound and method for degrading amino acids | |
| EP1044689A1 (en) | Solid iodophor preparations and process for producing the same | |
| CN103004889A (en) | Aquatic husbandry cultivation sterilization liquid | |
| CN107079908A (en) | A kind of aquatic products thimerosal and preparation method thereof | |
| CN101461382A (en) | Compound high-efficient disinfecting liquid for avian influenza | |
| CN101743971B (en) | Compound disinfector of peroxyacetic acid and glutaric dialdehyde | |
| US20080311082A1 (en) | Process for Treating Animal Waste | |
| CN102450281A (en) | Triumph ecological guanidine treasure | |
| CN101755757A (en) | Compound peracetic acid bromine chlorine hydantoin disinfectant | |
| CN110790350A (en) | Aquaculture water quality improver and preparation method thereof, and preparation method of powder and tablet of aquiculture water quality improver | |
| CN101461376A (en) | Biological catalytic enzyme disinfecting liquid | |
| CN105410036A (en) | Husbandry cultivation disinfection liquid and preparation method thereof | |
| CN115072667B (en) | Preparation method of reactive chlorine dioxide solid preparation using sodium chlorate as raw material | |
| CN102369953A (en) | Environment-friendly sterilizing, disinfecting and freshness-preserving agent and preparation method thereof | |
| RU2123864C1 (en) | Disinfectant | |
| KR100453738B1 (en) | Remedy of the quality of water for a a fish farm |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Open date: 20081029 |