CN101268990A - Condensation type floral water and preparation method thereof - Google Patents
Condensation type floral water and preparation method thereof Download PDFInfo
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- CN101268990A CN101268990A CNA2008100279298A CN200810027929A CN101268990A CN 101268990 A CN101268990 A CN 101268990A CN A2008100279298 A CNA2008100279298 A CN A2008100279298A CN 200810027929 A CN200810027929 A CN 200810027929A CN 101268990 A CN101268990 A CN 101268990A
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Abstract
The invention discloses a condensation type toilet water and a preparation method thereof; the condensation type toilet water mainly consists of the ingredients with the shares by weight: 0.1 to 1 share of menthol, 0.2 to 2 shares of borneol, 20 to 30 shares of alcohol, 0.5 to 5 shares of skin care ingredient, 0.03 to 2 shares of macromolecule resin, 0.1 to 1 share of acidifying or alkalizing agent and 59 to 79.07 shares of water. The preparation method is that the menthol and the borneol which are matched according to the proportion are dissolved in the alcohol, and the macromolecule resin is dispersed in water, after being evenly stirred at high speed, the mixture is added with the skin care ingredient to be stirred evenly and at last is added with the acidifying or alkalizing agent; the pH of the preparation is adjusted to be 6.5 to 7.5; finally, the mixture is mixed into the alcohol that is dissolved with the menthol and the borneol, so as to obtain the finished product. The finished product of the condensation type toilet water is of semisolid condensation form, which is immediately transformed into liquid form when being smeared on the skin, thereby promoting the active ingredient to be released rapidly to take effect; after condensation type toilet water is smeared on the skin, no residue is left on the skin; the condensation type toilet water also can greatly reduce the using quantity of the alcohol, and dose not stimulate the skin, can be directly smeared on the skin without being diluted and is convenient for use.
Description
Technical field
The present invention relates to a kind of condensation type floral water and preparation method thereof.
Background technology
Floral water is refrigerant owing to having, fragrant and the miliaria of dispelling is antipruritic, and advantages such as anthelmintic anophelifuge are popular to people deeply in daily life.At present, the floral water that people use always is liquid, and it has the inconvenience of carrying during use, shortcomings such as easy waste.Application number is that 200410014969.0 Chinese invention patent application discloses a kind of Radix Chloranthi Fortunei dew and manufacturing process thereof, it is with Mentholum, Borneolum Syntheticum, Camphora and essence are dissolved in the ethanol by proportioning, make mixed liquor, be poured in the molten device of rustless steel, making standby gel in advance by the proportioning adding stirs, after leaving standstill, add ethanol again, fully stir and get product, but be difficult to be fabricated into stay-in-grade Radix Chloranthi Fortunei dew according to this invention, and it is the same with traditional floral water, needs the ethanol consumption up to 30%-70%, could use after the skin that the child is tender and lovely need dilute.
Summary of the invention
The technical issues that need to address of the present invention provide a kind ofly can directly use not chafe, skin care effect is arranged, condensation type floral water easy to carry again.
The technical scheme that solves the problems of the technologies described above is as follows:
A kind of condensation type floral water, it mainly is made up of the composition of following weight portion:
Menthol 0.1-1
Borneolum Syntheticum 0-2
Ethanol 20-30
Skin care ingredient 0.5-5
Macromolecule resin 0.03-2
Acid-base modifier 0.1-1
Water 59-79.07.
Preferably, condensation type floral water, it mainly is made up of the composition of following weight portion:
Menthol 0.5-1
Borneolum Syntheticum 0-1.5
Ethanol 20-30
Skin care ingredient 2-3
Macromolecule resin 0.5-1.0
Acid-base modifier 0.5-1
Water 59-79.07.
Wherein, preferably, described skin care ingredient is one or more in allantoin, glycerol, propylene glycol, Polyethylene Glycol, sorbitol, the trehalose; Described macromolecule resin is one or more in polyvinyl alcohol, polyvinylpyrrolidone, hydroxypropyl emthylcellulose, carbopol, sodium carboxymethyl cellulose, hydroxyethyl-cellulose, polyacrylic acid, the sodium polyacrylate; Described acid-base modifier is selected from a kind of in sodium hydroxide, lactic acid, citric acid, triethanolamine, the sodium bicarbonate.
Another technical issues that need to address of the present invention provide a kind of preparation method of above-mentioned condensation type floral water.
The technical scheme that solves the problems of the technologies described above is as follows:
The preparation method of above-mentioned condensation type floral water: with menthol, the Borneolum Syntheticum of proportioning are dissolved in ethanol in proportion, macromolecule resin is scattered in the water, after high-speed stirred is even, adding skin care ingredient again stirs, add acid-base modifier at last, adjust preparation and regulate pH, get preparation, at last preparation and the ethanol mix homogeneously that is dissolved with menthol, Borneolum Syntheticum are got product to 6.5-7.5.
The present invention is prepared into stay-in-grade described condensation type floral water by simple method on a large amount of experimentation bases, it has the following advantages:
1, the present invention uses macromolecule resin to make gel, can utilize the fast characteristics of macromolecule resin modality to discharge effective ingredient, overcomes the defective that discharges effective ingredient in the conventional formulation by the volatilization of a large amount of ethanol.
2, finished product is the semi-solid gel state, is applied in skin and can changes into liquid state immediately, promotes the onset of effective ingredient rapid release, smears back skin noresidue.
3, condensation type floral water of the present invention can significantly reduce the ethanol consumption, and chafe need not dilute directly to be coated with and put on the skin, and is easy to use.
4, when preparation can add skin care ingredient that traditional floral water, Radix Chloranthi Fortunei dew do not have for example allantoin, glycerol, propylene glycol, Polyethylene Glycol, sorbitol, trehalose etc., can releive or eliminate the pruritus sense of discomfort of skin, the red and swollen or skin of chapping of maintenance.
The specific embodiment
Embodiment 1
Menthol 0.1 gram, Borneolum Syntheticum 0.5 gram are dissolved in ethanol 20 grams, macromolecule resin hydroxypropyl emthylcellulose 0.7 gram, polyvinyl alcohol 0.2 gram is scattered in the 76.8 gram water, after high-speed stirred is even, adding propylene glycol 0.5 gram stirs, add lactic acid 0.7 gram at last, adjust preparation, be mixed into the ethanol that is dissolved with menthol, Borneolum Syntheticum at last and get product to PH6.5.
Embodiment 2
Menthol 0.5 gram, Borneolum Syntheticum 1 gram are dissolved in ethanol 20 grams, macromolecule resin hydroxypropyl emthylcellulose 0.6 gram, polyacrylic acid 0.06 gram is scattered in the 72.04 gram water, after high-speed stirred is even, adding allantoin 5 grams stirs, add triethanolamine 1.0 grams at last, adjust preparation, be mixed into the ethanol that is dissolved with menthol, Borneolum Syntheticum at last and get product to PH7.0.
Embodiment 3
Menthol 0.9 gram, Borneolum Syntheticum 2.0 grams are dissolved in ethanol 20 grams, macromolecule resin hydroxyethyl-cellulose 0.8 gram, sodium polyacrylate 0.1 gram is scattered in the 73.8 gram water, after high-speed stirred is even, adding sorbitol 2.5 grams stirs, last adding citric acid 0.7 gram is adjusted preparation to PH7.5, is mixed into the ethanol that is dissolved with menthol, Borneolum Syntheticum at last and gets product.
Embodiment 4
Menthol 0.8 gram, Borneolum Syntheticum 0 gram are dissolved in ethanol 23 grams, macromolecule resin polyvinylpyrrolidone 0.01 gram, carbopol 0.02 gram is scattered in the 60 gram water, after high-speed stirred is even, adding glycerol 2 grams stirs, add sodium bicarbonate 0.9 gram at last, adjust preparation, be mixed into the ethanol that is dissolved with menthol, Borneolum Syntheticum at last and get product to PH7.0.
Embodiment 5
Menthol 1.0 grams, Borneolum Syntheticum 2.0 grams are dissolved in ethanol 30 grams, macromolecule resin polyvinyl alcohol 1.2 grams, sodium carboxymethyl cellulose 0.8 gram is scattered in the 68 gram water, after high-speed stirred is even, adding Polyethylene Glycol 3.0 grams stirs, last adding citric acid 0.1 gram is adjusted preparation to PH6.5, is mixed into the ethanol that is dissolved with menthol, Borneolum Syntheticum at last and gets product.
Embodiment 6
The foregoing description 1-5 gained condensation type floral water is tested.
After testing, the condensation type floral water for preparing has following physical behavior:
| Viscosity | 60mPas or more than |
| Turbidity | Gel liquid is clear in the time of 10 ℃, and is haze-free |
| Color stability | (48 ± 1) ℃, it is constant that 24h keeps original color and luster |
| Heat-resisting | 40 ℃, 24h, no segregation phenomenon |
| Cold-resistant | -5 ℃ ± 2 ℃, 24h recovers room temperature and can normally use. |
| Centrifugal test | 30min is not stratified in 2000 commentaries on classics/min rotation |
Claims (9)
1. condensation type floral water is characterized in that: mainly be made up of the composition of following weight portion:
Menthol 0.1-1
Borneolum Syntheticum 0-2
Ethanol 20-30
Skin care ingredient 0.5-5
Macromolecule resin 0.03-2
Acid-base modifier 0.1-1
Water 59-79.07.
2. condensation type floral water according to claim 1 is characterized in that: mainly be made up of the composition of following weight portion:
Menthol 0.5-1
Borneolum Syntheticum 0-1.5
Ethanol 20-30
Skin care ingredient 2-3
Macromolecule resin 0.5-1.0
Acid-base modifier 0.5-1
Water 59-79.07.
3. condensation type floral water according to claim 1 is characterized in that: described macromolecule resin is one or more in polyvinyl alcohol, polyvinylpyrrolidone, hydroxypropyl emthylcellulose, carbopol, sodium carboxymethyl cellulose, hydroxyethyl-cellulose, polyacrylic acid, the sodium polyacrylate.
4. condensation type floral water according to claim 1 is characterized in that: described skin care ingredient is one or more in allantoin, glycerol, propylene glycol, Polyethylene Glycol, sorbitol, the trehalose.
5. according to each described condensation type floral water of claim 1-4, it is characterized in that: described acid-base modifier is selected from a kind of in sodium hydroxide, lactic acid, citric acid, triethanolamine, the sodium bicarbonate.
6. one kind prepares the method for condensation type floral water according to claim 1, it is characterized in that, may further comprise the steps:
(1) with menthol, the Borneolum Syntheticum of proportioning are dissolved in ethanol in proportion;
(2) macromolecule resin is scattered in the water, after high-speed stirred is even, adds skin care ingredient again and stirs, and adds acid-base modifier at last, regulates pH to 6.5-7.5, gets preparation;
(3) will be dissolved with the ethanol and step (2) the gained preparation mix homogeneously of menthol, Borneolum Syntheticum, promptly get the condensation type floral water finished product.
7. condensation type floral water according to claim 6 is characterized in that: described macromolecule resin is one or more in polyvinyl alcohol, polyvinylpyrrolidone, hydroxypropyl emthylcellulose, carbopol, sodium carboxymethyl cellulose, hydroxyethyl-cellulose, polyacrylic acid, the sodium polyacrylate.
8. condensation type floral water according to claim 6 is characterized in that: described skin care ingredient is one or more in allantoin, glycerol, propylene glycol, Polyethylene Glycol, sorbitol, the trehalose.
9. according to each described condensation type floral water of claim 6-8, it is characterized in that: described acid-base modifier is selected from a kind of in sodium hydroxide, lactic acid, citric acid, triethanolamine, the sodium bicarbonate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100279298A CN101268990B (en) | 2008-05-07 | 2008-05-07 | Condensation type floral water and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100279298A CN101268990B (en) | 2008-05-07 | 2008-05-07 | Condensation type floral water and preparation method thereof |
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| Publication Number | Publication Date |
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| CN101268990A true CN101268990A (en) | 2008-09-24 |
| CN101268990B CN101268990B (en) | 2010-08-18 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008100279298A Expired - Fee Related CN101268990B (en) | 2008-05-07 | 2008-05-07 | Condensation type floral water and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102366389A (en) * | 2011-11-01 | 2012-03-07 | 重庆泰尔森制药有限公司 | Preparation method for compound mosquito repelling and itching relieving floral water |
| CN105997529A (en) * | 2016-06-24 | 2016-10-12 | 南京为绿生物科技有限公司 | Membrane type healthy itching-relieving mosquito repellent |
| CN108272696A (en) * | 2018-04-15 | 2018-07-13 | 啵噜噜（广州）婴儿用品科技有限公司 | A kind of external preparation with mosquito-expelling and antipruritic |
| CN114617798A (en) * | 2022-04-13 | 2022-06-14 | 广东博然堂生物科技有限公司 | Energy-saving type smoothie gel and preparation method thereof |
-
2008
- 2008-05-07 CN CN2008100279298A patent/CN101268990B/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102366389A (en) * | 2011-11-01 | 2012-03-07 | 重庆泰尔森制药有限公司 | Preparation method for compound mosquito repelling and itching relieving floral water |
| CN102366389B (en) * | 2011-11-01 | 2013-03-20 | 重庆泰尔森制药有限公司 | Preparation method for compound mosquito repelling and itching relieving floral water |
| CN105997529A (en) * | 2016-06-24 | 2016-10-12 | 南京为绿生物科技有限公司 | Membrane type healthy itching-relieving mosquito repellent |
| CN108272696A (en) * | 2018-04-15 | 2018-07-13 | 啵噜噜（广州）婴儿用品科技有限公司 | A kind of external preparation with mosquito-expelling and antipruritic |
| CN114617798A (en) * | 2022-04-13 | 2022-06-14 | 广东博然堂生物科技有限公司 | Energy-saving type smoothie gel and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101268990B (en) | 2010-08-18 |
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Owner name: FOSHAN BIOURS BIOSCIENCES CO., LTD. Free format text: FORMER OWNER: GUANGZHOU BIOURS BIOSCIENCES CO., LTD. Effective date: 20140609 |
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Inventor after: Huang Qing Inventor before: Zuo Ting |
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Free format text: CORRECT: INVENTOR; FROM: ZUO TING TO: HUANG QING Free format text: CORRECT: ADDRESS; FROM: 510630 GUANGZHOU, GUANGDONG PROVINCE TO: 528137 FOSHAN, GUANGDONG PROVINCE |
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Effective date of registration: 20140609 Address after: 528137 Guangdong city in Foshan Province, Leping Town, Sanshui District, West East Road No. 13 building two floor F1 block B 201, 202, No. 203, block B, No. 302 on the third floor Patentee after: Foshan Biours Biosciences Co., Ltd. Address before: 510630 Guangdong province Guangzhou Science City Road innovation base building A 604 month Patentee before: Guangzhou Pai'ao Biological Science and Technology Co., Ltd. |
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