CN101268815A - Supercritical carbonic anhydride wall-breaking method for melissa powder - Google Patents
Supercritical carbonic anhydride wall-breaking method for melissa powder Download PDFInfo
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- CN101268815A CN101268815A CNA2008100078551A CN200810007855A CN101268815A CN 101268815 A CN101268815 A CN 101268815A CN A2008100078551 A CNA2008100078551 A CN A2008100078551A CN 200810007855 A CN200810007855 A CN 200810007855A CN 101268815 A CN101268815 A CN 101268815A
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Abstract
The invention discloses a method using supercritical carbon dioxide to perform bee pollen broken-face. Bee pollen is put in an extraction plant of supercritical carbon dioxide, to react for a certain time in supercritical carbon dioxide liquid at the proper pressure and temperature, a vent valve is opened to rapidly empty carbon dioxide, so that a pollen cell expands acutely due to larger pressure difference of the inside and the outside, thereby cracking. The method has the advantages that the operation is simple and convenient, the cost is low, the whole process is performed below 50 DEG C, the broken-face time does not exceed 30 minutes, the influence of the product by thermotropy is reduced, so that the active ingredient is preserved completely, at the same time, bacillus can be killed, the unification of the broken-face and the sterilization processes is realized, the broken-face ratio of the pollen cell is high, but the percentage of damage is low, and the inclusion still exists in a cracked pollen wall under the dry condition, thereby favoring the preservation of the nutritious content.
Description
Technical field
The invention belongs to natural products health products and pharmaceutical technology field, relate to the broken wall of melissa pollen method, can be widely used in the industries such as bio-pharmaceuticals, health food.
Background technology
The melissa powder is to gather the dough that the pollen of the sources of nectar and pollen forms through processing by honeybee, the nutritional labeling of melissa powder is very abundant, almost contain whole nutrients, it is a kind of high-quality nutrient source, not only contain rich in protein, carbohydrate, lipid, vitamin, organic acid, mineral matter, nucleic acid, also contain enzyme and other biological active material, be described as " miniature nutrition library ".Before thousands of year, in ancient countries such as China and Greece, people have begun to eat pollen, and with it as medicinal.Along with going deep into of science and technology development and research, the medical health care function of melissa powder is progressively excavated, as prevents and treats angiocardiopathy, prostatic disorders, hypertension, anaemia, diabetes etc.People have been not content with the health-care effect slowly that edible melissa powder is brought, and the clear and definite active component of abstraction function has become upsurge from the melissa powder, and the prerequisite of effectively extracting active component is the broken wall that carries out the melissa powder.The process for breaking wall of pollen of report has following several both at home and abroad at present:
(1) difference Poluo wall method (number of patent application 96117011.5,02110649.5): utilize the principle of expanding with heat and contract with cold, pollen drops into rapidly after cryogenic freezing in the hot water " bursting ", and this method is destroyed bigger to the nutritional labeling of pollen, and complicated operation.
(2) machinery broken wall law (number of patent application 86103261,90108303.8,95110207.9,96117168.5) is with pollen water furnishing liquid, carries out broken wall by machineries such as colloid mill, high pressure homogenizers again.Make broken wall in this way, pollen needs to handle complicated operation after soaking into liquid.
(4) fermentation enzymolysis broken wall method (number of patent application 03115992.3,87104508,91106215.7,95103910.5,98104558.8,02106399.0) is a kind of application method more widely, the enzyme that utilizes the abundant microorganism of pollen self or produce by microbe inoculation, make the fovilla degraded, osmotic pressure raises and makes pollen broken wall, required time of this method broken wall is long, and is easily influenced quality by living contaminants in the sweat.
Above wall-breaking method is Wet-process wall breaking, require with different solvents with pollen wetting or furnishing liquid, must carry out drying as if making solid pharmaceutical preparation behind the broken wall, cause the increase of product cost.
(5) microwave radiation broken wall method (number of patent application 200710022400.2) is packed pollen to be placed in the micro-wave oven heated baking.This method does not go to pot pollen grain integral body, but the temperature on bag center and top layer is wayward, complex process, and production efficiency is low.
(6) comminution by gas stream (number of patent application 01115014.9) is to utilize the compressed air pump air to produce high pressure draught, sprays into pulverizing chamber through nozzle through velocity of sound, by collision, reaches the purpose of pulverizing pollen at low temperatures.This method operation is complicated, and the fovilla behind the broken wall is exposed in the external environment fully, is easy to generate oxidation deterioration.
Traditional wall-breaking method respectively has its advantage, but shortcoming is obvious equally, and perhaps long processing period, as cold and heat succeed each other facture and autolysis method etc. are used inconvenience aborning; Perhaps produce a large amount of heats in the broken wall process, the forfeiture that causes the pollen enzyme to be lived is as various mechanical means broken walls; Perhaps efficient height but the cost costliness as enzymatic digest method, high-pressure homogeneous processing and high voltage electric field method, increases product cost greatly can't be promoted the use of aborning.
Summary of the invention
The objective of the invention is in order to overcome the shortcoming of prior art, provide a kind of processing cost low, easy and simple to handle, pollen grain integral body is not gone to pot, breaking-wall cell speed is fast and sporoderm-broken rate is high, the supercritical carbonic anhydride wall-breaking method for melissa powder that can use aborning.
Supercritical carbonic anhydride wall-breaking method for melissa powder of the present invention, it is characterized in that: the moisture of melissa powder is controlled at 4～20%, put into the extraction kettle of supercritical carbon dioxide extraction apparatus, 32～50 ℃ of control carbon dioxide temperature, pressure 8～50MPa, act on 5～30 minutes, open the rapid emptying carbon dioxide of air bleeding valve, collect broken pollen and get final product.
Supercritical CO 2 extraction device sees Fig. 1 for details: 1.CO
2Steel cylinder; 2. clarifier; 3. storage tank (ice chest); 4 blenders; 5. clarifier; 6 extraction kettles; 7. air bleeding valve; 8. separating still; 9. Pressure gauge; 10. flowmeter
Advantage of the present invention:
1, the present invention is the dry method broken wall, and the broken pollen drying-free is handled, and has removed the possibility of drying process to the influence of pollen active ingredient.
2, the present invention carries out the pollen cell broken wall with supercritical carbon dioxide as medium, and supercritical carbon dioxide is easy to be penetrated in the cell, reaches the inside and outside pressure balance of cell soon; Suddenly step-down then, this moment cell because of born of the same parents' inside and outside differential pressure is bigger, acutely expand and break, the effect that reaches not only broken wall but also sterilize.
3, pollen integral body does not have destroyedly among the present invention, and inclusion still is present in the pollen wall that breaks under drying condition, helps nutritional labeling and preserves.
4, the present invention is low temperature, broken wall in short-term, and whole process is carried out under lower temperature (below 50 ℃), and broken time short (in 30 minutes) has reduced the heated denaturalization influence of product, and active component is preserved fully.
5, operating pressure of the present invention lower (50MPa is following), flow process is simple, greatly reduces the investment of equipment, has improved production security; Carbon dioxide is a kind of inactive gas, chemical reaction do not take place in the broken wall process, and belongs to non-flammable gases, and tasteless, odorless, nontoxic, security is good, environmentally safe.
6, the present invention is easy and simple to handle, the production efficiency height, and energy savings does not produce the refuse of contaminated environment, and the equipment operating cost is low, less energy consumption, production cost is low, is very suitable for industrialized mass, is a kind of desirable process for breaking wall of pollen.
Electron microscopic observation sees description of drawings for details:
Fig. 2 is the broken pollen electron microscopic morphology not
Fig. 3 behind the inventive method broken wall the pollen cell sporoderm-broken rate up to more than 95%
Fig. 4 pollen cell wall behind this method broken wall breaks in various degree, and content is present in the broken pollen wall
The specific embodiment,
Further specify the present invention below in conjunction with embodiment.
Embodiment 1:
With fresh melissa powder vacuum drying to moisture is 6.20%, gets the 300g dry pollen 1L extractor of packing into, under the condition of 35 ℃ of extraction kettle temperature, is that 99% carbon dioxide boosts to extraction kettle pressure 15MPa with purity; Keep-up pressure and open the rapid emptying carbon dioxide of extractor air bleeding valve behind the 5min, collect pollen and get final product.Detect through Electronic Speculum, pollen cell is broken wall.
Embodiment 2:
Taking by weighing the dry melissa powder 300g 1L extractor of packing into, under the condition of 35 ℃ of extraction kettle temperature, is that 99% carbon dioxide boosts to extraction kettle pressure 30MPa with purity; Keep-up pressure and open the rapid emptying carbon dioxide of extractor air bleeding valve behind the 5min, collect pollen and get final product.Detect through Electronic Speculum, pollen cell is broken wall.
Embodiment 3:
With fresh melissa powder vacuum drying to moisture is 6.20%, gets dry back pollen 300g 11 extractors of packing into, under the condition of 40 ℃ of extraction kettle temperature, is that 99% carbon dioxide boosts to extraction kettle pressure 30MPa with purity; Keep-up pressure and open the rapid emptying carbon dioxide of extractor air bleeding valve behind the 10min; Taking-up pollen gets final product.Detect through Electronic Speculum, pollen cell is broken wall.
Embodiment 4:
The dry melissa powder 300g 1L extractor of packing under the condition of 40 ℃ of extraction kettle temperature, is that 99% carbon dioxide boosts to extraction kettle pressure 45MPa with purity; Keep-up pressure and open extractor behind the 10min and take out pollen and get final product.Detect through Electronic Speculum, pollen cell is broken wall.
Embodiment 5:
With pollen grain vacuum drying to moisture is 6.20%, with the dried pollen 300g 1L extractor of packing into, under the condition of 45 ℃ of extraction kettle temperature, is that 99% carbon dioxide boosts to extraction kettle pressure 5MPa with purity; Keep-up pressure and open the rapid emptying carbon dioxide of extractor air bleeding valve behind the 30min, take out pollen.Detect through Electronic Speculum, pollen cell is broken wall.
Claims (5)
1. supercritical carbonic anhydride wall-breaking method for melissa powder, it is characterized in that: the moisture of melissa powder is controlled at 4～20%, pack in the extraction kettle of supercritical carbon dioxide extraction apparatus, feed carbon dioxide pressurization carrying out pollen cell broken wall, each parameter area of its supercritical carbon dioxide fluid pollen cell wall breaking technology is respectively: breaking-wall cell pressure is 8～50MPa, 32～50 ℃ of broken wall temperature, 5～30 minutes time; Open the rapid emptying carbon dioxide of air bleeding valve then, thereby the pollen cell outer wall is broken greatly because of wall external and internal pressure difference.
2. broken wall of melissa pollen method according to claim 1 is characterized in that: described melissa powder is not subjected to the restriction of pollen kind for any kind of commercial or non-commercial melissa powder.
3. broken wall of melissa pollen method according to claim 1 is characterized in that: breaking-wall cell pressure is 8～50MPa, preferred 30～40MPa.
4. broken wall of melissa pollen method according to claim 1 is characterized in that: broken wall is temperature required to be 30～50 ℃, preferred 35～40 ℃.
5. broken wall of melissa pollen method according to claim 1 is characterized in that: the required pressure hold time of broken wall is 5～30 minutes, preferred 15～25 minutes.
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| CN102071099A (en) * | 2011-01-07 | 2011-05-25 | 中国科学院西北高原生物研究所 | Process for quickly breaking cell walls of Chinese wolfberry seeds and extracting seed oil |
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| CN104996635A (en) * | 2015-07-31 | 2015-10-28 | 合肥旭腾环保科技有限公司 | Sesame-flavored camellia pollen beverage and preparation process thereof |
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Effective date of registration: 20180724 Address after: 710075 B 22004, Tang Feng International Plaza, 18 Fenghui South Road, Xi'an new and high tech Zone, Shaanxi. Patentee after: Kangtai Shaanxi bio Pharmaceutical Engineering Co., Ltd. Address before: 100093 North gully of Xiangshan, Haidian District, Beijing Patentee before: Bee Research Institute of CAAS |