CN101263900B - Preparation of corn filament soft capsule - Google Patents

Preparation of corn filament soft capsule Download PDF

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Publication number
CN101263900B
CN101263900B CN2008100506357A CN200810050635A CN101263900B CN 101263900 B CN101263900 B CN 101263900B CN 2008100506357 A CN2008100506357 A CN 2008100506357A CN 200810050635 A CN200810050635 A CN 200810050635A CN 101263900 B CN101263900 B CN 101263900B
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soft capsule
corn
ball
preparation
cornsilk
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Expired - Fee Related
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CN2008100506357A
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CN101263900A (en
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刘静波
林松毅
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Jilin University
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Jilin University
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Abstract

The invention relates to a cornsilk soft capsule and a method for the production thereof, belonging to the technical field of functional food processing. The cornsilk soft capsule comprises capsulation liquid and capsule shell cellophane and comprises the components: cornsilk powder, gelatin, glycerol, vegetable oil, beeswax, Vitamin E, Vitamin C, pigment, methyl p-hydroxybenzoate and other components. The method for the production thereof is that as the main ingredient, the cornsilk powder is produced into the cornsilk soft capsule by cornsilk powder preparation, capsulation liquid blending, capsule shell cellophane preparation and soft capsule pill preparation, making effective use of cornsilk. The produced cornsilk soft capsule which contains cornsilk flavonoid, carbohydrate, sterols and other functional components and the functional properties thereof has convenient usage, simple storage, long shelf life and other advantages of soft-capsule health care food formulation as well as broad market prospect.

Description

The preparation method of corn filament soft capsule
Technical field
The invention belongs to the functional food machining technology, particularly the corn capillament excipient is in the production technology of capsule health food containing formulation.
Background technology
Corn capillament is a traditional Chinese medicine, contains multiple efficacies compositions such as sterols, carbohydrate, flavonoids, organic acid, vitamin, alkaloid, saponin(e, inositol, kryptoxanthin, allantoin, and its medical value is mainly reflected in the following aspects:
(1) hypoglycemic, hypotensive, effect for reducing blood fat
" Chinese medicine voluminous dictionary " record, application corn capillament treatment diabetes among the people have obtained curative effect preferably.Zoopery shows that the corn capillament polysaccharide can be regulated the glycometabolism of diabetic mice, promotes gluconeogenesis, and the blood sugar rising extremely of alloxan institute is had obvious blood sugar reducing function; The total saponin(e of corn capillament has hypoglycemic activity preferably, and the pancreas islet damage of antagonism causal diabetes model has the significant protection effect, also is one of main active of corn capillament hypoglycemic.In addition, the corn capillament water extract has tangible hypotensive effect to hypertension, and the normotensive is not had influence.
(2) immunoregulation effect
Medical research shows: the apoptosis of body tissue cell, the generation of disease are more or less all formed relevant with immunologic function with the structure of body immune system.If the apoptosis that the immune system of normal body can not pair cell is regulated and control, pathology will take place in the respective organization organ, like tumour, hepatitis.Functional component safety non-toxics such as the polysaccharide that contains in the corn capillament, flavones have better immunocompetence and oxidation resistance, can significantly improve immunity of organisms.Mainly show as, alleviating fatigue, antitumor, anti-ageing.
(3) clearing heat secreting bile effect
The corn capillament polysaccharide can obviously strengthen choleresis, promotes gall-bladder to shrink, and reduces gall-bladder weight, has tangible clearing heat secreting bile effect.
(4) diuresis, defaecation suppress the calculus effect
The corn capillament water extract can prolong the gastric emptying time, and enterocinesia is quickened, and defecation frequency increases; Reduce the kidney oxalic acid content and suppress the formation of calcium oxalate crystal, thereby suppress the generation of Oxalates calculus.
In addition, " Chinese medicine voluminous dictionary " record, corn capillament low toxicity; Food and Drug Administration confirms that corn capillament is safe, nontoxic material, and the made medicine of corn capillament extract is also confirmed as non-prescribed medicine.Corn capillament generally acknowledges it is safe in the U.S..
At present, on the domestic and international market also be not the soft capsule product that primary raw material is developed with the corn capillament.
Summary of the invention
The technical problem that the present invention will solve is: disclose a kind of component and each constituent content of corn filament soft capsule, openly prepare the method for corn filament soft capsule.The corn filament soft capsule that the present invention developed not only contains functional component and effect characteristics thereof such as corn capillament flavonoids, carbohydrate, sterols, but also drinking conveniently of having taken into account that the capsule health food containing formulation had, characteristics such as storage practice is simple, long shelf-life.
The technical scheme that the present invention adopts is following:
A kind of corn filament soft capsule; Form by capsulation solution and softgel shell glued membrane; It is characterized in that; With the corn capillament powder is major ingredient, and the mass parts of each component of described capsulation solution and content thereof is counted: 9~20 parts in corn capillament powder, 80~91 parts of vegetable oil, 2~7.5 parts in beeswax, 0.2~0.5 part of vitamin E, 0~0.5 part of vitamin C; Described each component of softgel shell glued membrane and count: 2 parts in gelatin, 0.2~0.3 part in water, 0.6~1.5 part of glycerine, 0.015~0.025 part of pigment, 0.005~0.015 part of methyl p-hydroxybenzoate by mass parts.
Described corn capillament powder is that corn capillament obtains through screening, immersion, cleaning, oven dry, pulverizing, and granularity control is at 70~200 orders.
The preparation method of corn filament soft capsule is a major ingredient with the corn capillament powder; Process through the preparation of corn capillament powder, capsulation solution allotment, the preparation of softgel shell glued membrane, the preparation of soft capsule ball makes corn filament soft capsule;
Described corn capillament powder prepares process, be corn capillament is rejected the part of going mouldy, the flowing water that is soaked in water again flushing repeatable operation 2~4 times, adopt oven dry pulverize or wet feed pulverize dry to granularity at 70~200 orders;
Described capsulation solution allocation process, be with beeswax 70~90 ℃ of thawings, press mass ratio and add corn capillament powder, vegetable oil, vitamin E, vitamin C, make mixing of materials even 20~50 ℃ of stirrings, pass through colloid mill again 5~10 times, 20~50 ℃ of insulations;
Described softgel shell glued membrane prepares process; Be to get the raw materials ready for 0.005~0.015 part in each 2 parts in constituent mass ratio gelatin, 2 parts in water, 0.6~1.5 part of glycerine, 0.015~0.025 part of pigment, methyl p-hydroxybenzoate; Earlier gelatin and water are fed in the vacuum adhesive disolving tank, the immersion through 5~40 minutes is expanded gelatin, 50~80 ℃ of following stirring and dissolving; Add glycerine, pigment, methyl p-hydroxybenzoate again, behind the mixing again through making the softgel shell glued membrane under the soft capsule host computer control;
Described soft capsule ball prepares process, be to utilize encapsulating machine to prepare the corn filament soft capsule ball, through typing, wash ball, the ball that dries in the air, the process of choosing ball make finished product.This process is identical in the pelletizing process of existing capsule pill food.
Prepare in the process at the corn capillament powder, generally want soaking flushing 2~4 times, this serves as control soaking flushing operating technology main points in the national regulation allowed band with residues of pesticides each item control indexes; In the corn capillament grinding mode, can select for use oven dry to pulverize or select for use wet feed to pulverize the mode of oven dry, to moisture 3%~5%; If bake out temperature should be controlled at 50 ℃~90 ℃ when selecting for use oven dry to pulverize, if when selecting for use wet feed to pulverize oven dry, bake out temperature should be controlled at 40 ℃~80 ℃.
In the capsulation solution allocation process, can also carry out 7~15Mpa homogenization processing after the colloid mill, make each component mix more evenly.
Prepare in the process at the soft capsule ball, can be more specifically, utilize encapsulating machine to prepare the corn filament soft capsule ball, be delivered in the typing converter and finalized the design 8~18 hours; Being dipped in concentration after the typing is to wash ball in 75%~95% ethanol 10~30 seconds; Be 35~45% in relative humidity, temperature is the ball 10~24 hours of drying in the air under 21~25 ℃ of environment, examines ball afterwards.During the inspection ball, reject inhomogeneous, the not full soft capsule ball of soft capsule ball shape.
Jilin Province is main corn producing region, surplus a year cultivated area reaches 4,000 ten thousand mu, except that corn and intensive processing product research exploitation thereof, to the utilization still not yet in effect of corn stigma (corn capillament) resource, generally takes to burn or waste treatment.So the present invention develops the corn filament soft capsule product, can ten thousand tons of corn capillaments surplus the Jilin Province annual 90 be carried out scale development and utilization as the functional food new resources, this will produce huge economic benefit and social benefit.
The present invention has effectively utilized the corn capillament resource; Prepared corn filament soft capsule product; Not only contain functional component and effect characteristics thereof such as corn capillament flavonoids, carbohydrate, sterols; But also drinking conveniently of having taken into account that the capsule health food containing formulation had, characteristics such as storage practice is simple, long shelf-life really embody economic benefit and social benefit that the corn capillament intensive processing is contained, and market prospects are extremely wide.
The specific embodiment
Embodiment 1:
Get dried corn capillament and reject the part of going mouldy, the flowing water that is soaked in water again flushing repeatable operation 2 times is dried to moisture 3%, is crushed to granularity 90 orders; Temperature is controlled at 80~90 ℃ during oven dry.
The 12g beeswax 70 ℃ of thawings, is added corn capillament powder 80g, vegetable oil 320g, vitamin E 2g, make mixing of materials even 50 ℃ of stirrings, pass through colloid mill again 10 times, 50 ℃ of insulations obtain the capsulation solution of soft capsule.
Gelatin 80g, water 80g are fed in the vacuum adhesive disolving tank; Immersion through 40 minutes is expanded gelatin; 80 ℃ of following stirring and dissolving, add glycerine 40g, methyl p-hydroxybenzoate 0.2g, brilliant black pigment 0.6g again and mix, again through preparation softgel shell glued membrane under the soft capsule host computer control.
Utilize encapsulating machine to prepare the corn filament soft capsule ball, behind the typing 18h, be dipped in and wash ball in 75% ethanol and take out after 10 seconds; And at 21 ℃ of balls that dry in the air; Control relative humidity is 45%, dries in the air to 24h, reject soft capsule ball shape inhomogeneous, not full be the corn filament soft capsule finished product.
Embodiment 2
Get dried corn capillament 60g, reject the part of going mouldy, the flowing water that is soaked in water again flushing repeatable operation 4 times is dried to moisture 5%, is crushed to granularity 200 orders; Temperature is controlled at 60~70 ℃ during oven dry.
The 10g beeswax 90 ℃ of thawings, is added corn capillament powder 40g, vegetable oil 358g, vitamin E 1g, vitamin C 1g, make mixing of materials even 40 ℃ of stirrings, pass through colloid mill again 8 times, 40 ℃ of insulations obtain the capsulation solution of soft capsule.
Earlier gelatin 100g and water 200g are fed in the vacuum adhesive disolving tank; Immersion through 30 minutes is expanded gelatin; 60 ℃ of following stirring and dissolving, add glycerine 50g, brilliant black pigment 0.4g, methyl p-hydroxybenzoate 0.6g again, pass through preparation softgel shell glued membrane under the soft capsule host computer control behind the mixing again.
Utilize encapsulating machine to prepare the corn filament soft capsule ball, behind the typing 8h, be dipped in and wash ball in 95% ethanol and take out after 30 seconds; And at 25 ℃ of balls that dry in the air; Control relative humidity is 35%, dries in the air to 10h, reject soft capsule ball shape inhomogeneous, not full be the corn filament soft capsule finished product.
Embodiment 3
Get dried corn capillament 100g, reject the part of going mouldy, the flowing water that is soaked in water again flushing repeatable operation 3 times selects for use wet feed to pulverize oven dry, and granularity control is at 100 orders, and bake out temperature should be controlled at 60 ℃.
The 20g beeswax 70 ℃ of thawings, is added corn capillament powder 60g, vegetable oil 380g, vitamin E 2g, vitamin C 2.2g, make mixing of materials even 40 ℃ of stirrings, pass through colloid mill again 5 times, 40 ℃ of insulations obtain the capsulation solution of soft capsule.
Earlier gelatin 50g and water 120g are fed in the vacuum adhesive disolving tank; Immersion through 5 minutes is expanded gelatin; 80 ℃ of following stirring and dissolving, add glycerine 50g, pale brown pigment 0.2g, methyl p-hydroxybenzoate 0.3g again, pass through preparation softgel shell glued membrane under the soft capsule host computer control behind the mixing again.
Utilize encapsulating machine to prepare the corn filament soft capsule ball, behind the typing 12h, be dipped in and wash ball in 85% ethanol and take out after 20 seconds; And at 23 ℃ of balls that dry in the air; Control relative humidity is 40%, dries in the air to 12h, reject soft capsule ball shape inhomogeneous, not full be the corn filament soft capsule finished product.
Embodiment 4
Get dried corn capillament 200g, reject the part of going mouldy, the flowing water that is soaked in water again flushing repeatable operation 4 times selects for use wet feed to pulverize oven dry, and granularity control is at 80 orders, and bake out temperature should be controlled at 80 ℃.
The 100g beeswax 80 ℃ of thawings, is added corn capillament powder 150g, vegetable oil 1200g, vitamin E 5g, vitamin C 4g, make mixing of materials even 20 ℃ of stirrings, pass through colloid mill again 10 times, 20 ℃ of insulations obtain the capsulation solution of soft capsule.
Earlier gelatin 100g and water 200g are fed in the vacuum adhesive disolving tank; Immersion through 20 minutes is expanded gelatin; 50 ℃ of following stirring and dissolving, add glycerine 30g, pale brown pigment 0.9g, methyl p-hydroxybenzoate 0.8g again, pass through preparation softgel shell glued membrane under the soft capsule host computer control behind the mixing again.
Utilize encapsulating machine to prepare the corn filament soft capsule ball, behind the typing 10h, be dipped in and wash ball in 95% ethanol and take out after 30 seconds; And at 25 ℃ of balls that dry in the air; Control relative humidity is 45%, dries in the air to 10h, reject soft capsule ball shape inhomogeneous, not full be the corn filament soft capsule finished product.

Claims (3)

1. the preparation method of a corn filament soft capsule is a major ingredient with the corn capillament powder; Process through the preparation of corn capillament powder, capsulation solution allotment, the preparation of softgel shell glued membrane, the preparation of soft capsule ball makes corn filament soft capsule;
Described corn capillament powder prepares process, be corn capillament is rejected the part of going mouldy, the flowing water that is soaked in water again flushing repeatable operation 2~4 times, adopt oven dry pulverize or wet feed pulverize dry to granularity at 70~200 orders;
Described capsulation solution allocation process, be with beeswax 70~90 ℃ of thawings, press mass ratio and add corn capillament powder, vegetable oil, vitamin E, vitamin C, make mixing of materials even 20~50 ℃ of stirrings, pass through colloid mill again 5~10 times, 20~50 ℃ of insulations; Wherein, the mass parts of each component of capsulation solution and content thereof is counted: 9~20 parts in corn capillament powder, 80~91 parts of vegetable oil, 2~7.5 parts in beeswax, 0.2~0.5 part of vitamin E, 0~0.5 part of vitamin C;
Described softgel shell glued membrane prepares process; Be to get the raw materials ready for 0.005~0.015 part in each 2 parts in constituent mass ratio gelatin, 2 parts in water, 0.6~1.5 part of glycerine, 0.015~0.025 part of pigment, methyl p-hydroxybenzoate; Earlier gelatin and water are fed in the vacuum adhesive disolving tank, the immersion through 5~40 minutes is expanded gelatin, 50~80 ℃ of following stirring and dissolving; Add glycerine, pigment, methyl p-hydroxybenzoate again, behind the mixing again through making the softgel shell glued membrane under the soft capsule host computer control;
Described soft capsule ball prepares process, be to utilize encapsulating machine to prepare the corn filament soft capsule ball, through typing, wash ball, the ball that dries in the air, the process of choosing ball make finished product.
2. according to the preparation method of the described corn filament soft capsule of claim 1, it is characterized in that described corn capillament powder prepares process, bake out temperature was controlled at 50 ℃~90 ℃ when oven dry was pulverized; Bake out temperature was controlled at 40 ℃~80 ℃ when wet feed was pulverized oven dry.
3. according to the preparation method of claim 1 or 2 described corn filament soft capsules, it is characterized in that described soft capsule ball prepares process, is to utilize encapsulating machine to prepare the corn filament soft capsule ball, is delivered in the typing converter to finalize the design 8~18 hours; Being dipped in concentration after the typing is to wash ball in 75%~95% ethanol 10~30 seconds; Be 35~45% in relative humidity, temperature is the ball 10~24 hours of drying in the air under 21~25 ℃ of environment, examines ball afterwards.
CN2008100506357A 2008-04-24 2008-04-24 Preparation of corn filament soft capsule Expired - Fee Related CN101263900B (en)

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CN101897912A (en) * 2010-07-27 2010-12-01 浙江大学 Bamboo shoot sterol soft capsules and application thereof
CN103355450A (en) * 2013-05-14 2013-10-23 吉林大学 Method for preparing maize filament tea bag

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1742950A (en) * 2004-09-01 2006-03-08 闵伟红 Chinese medicine preparation made from corn stigma and preparing method

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1742950A (en) * 2004-09-01 2006-03-08 闵伟红 Chinese medicine preparation made from corn stigma and preparing method

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
范碧亭主编.第十三章 第二节 三 软胶囊剂的制法.《中药药剂学》.1997, *
鲁晓翔,陈甲,连喜军,张彦青.玉米须黄酮微胶囊制备条件的研究.《食品科学》.2007,第28卷(第9期),132-136. *

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