CN101243889A - Fleece-flower root medicinal food salted duck egg and preparation method thereof - Google Patents
Fleece-flower root medicinal food salted duck egg and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a multiflower knotweed medicated diet salted duck egg and a preparation method of the salted duck egg. The medicated diet salted duck egg is prepared by the immersion of the feed liquid. The weight ratio of the radix polygoni multiflori, the kudzu root, the chuanxiong rhizome, the tangerine peel of the feed liquid is 6:5:2:2, the feed liquid is processed by immersion, decoction and concentration till the concentration reaches 100 percent, and then table salt with a concentration of 15 percent is dissolved into the feed liquid. Crocks or glass jars are used as vessel, fresh and crackless duck eggs are selected, washed and air dried, the immersing feed liquid are filled into the vessel, and then the vessel is sealed to bloat the duck eggs for 25 to 30 days. The boating craft of the medicated diet salted duck egg in the invention has the advantages that: the craft is feasible, easy to operation and scale production, the Chinese herbal medicine is abundant, easily obtained and cheap; the medicated diet prescription can meet the national legal norm for health care food and is safe and nontoxic; compared with the common salted duck eggs in the same batch, the medicated diet salted duck eggs has higher lecithin content and lower cholesterol content; the Chinese herbal medicine components in the medicated diet salted duck eggs can improve the metabolism of bodies and enhance the function of the liver, the spleen and the kidney, thus, the increase and the deposition of the cholesterol are avoided and the fluidity of the blood and the elasticity of the blood vessel is improved.
Description
Technical field
The present invention relates to a kind of have nourishing healthy, prophylactic medicinal food salted duck egg and preparation method thereof.
Background technology
Duck's egg is that nutritional labeling is higher in the eggs, and the lower a kind of food of cholesterol level, and is nutritious, contains protein, lecithin, VitA, VitB
1, VitB
2, mineral matter such as nutrient such as VitC, VitD and calcium, potassium, iron.Relevant studies show that, compare with the homogenous quantities egg, its contained protein is suitable with it, but contained mineral matter is abundanter than egg, and content of cholesterol then is lower than egg, be about 1/3 of homogenous quantities egg and " wear political affairs, pay fine jade, Gan Fei, etc. the comparison of Nutrients of Different Fowl Eggs. amino acid and living resources, 2003,25 (3): 24 ".According to the judgement of present nutrition, duck's egg obviously more meets modern crowd's nourishing healthy demand.Data shows that with Salted duck egg or lime-preserved egg that traditional handicraft is processed into, its content of cholesterol does not have significant change.Duck's egg is if combine with manufacture craft with the theory of Chinese herbal cuisine, and content before and after pickling changes if the effect of traditional Chinese medicine ingredients makes cholesterol.Then more may further improve the nutrient structure of duck's egg, and can be on the basis of embodying the herbal cuisine theory, the function of the health care prevention of performance herbal cuisine is treated in supporting to produce residence, and the residence medicine is in the effect of food.
Summary of the invention
The objective of the invention is Chinese herbal cuisine is combined with traditional Salted duck egg processing technology, develop a kind ofly, and have nourishing healthy, anti-disease medicinal food salted duck egg of function and preparation method thereof such as cure the disease simultaneously for daily edible.
The present invention filters out to have and tonifies the liver and kidney, strengthening the spleen and stomach, and the promoting flow of qi and blood circulation is dredged through health-care effects such as vein relaxings, but and is defined as the edible Chinese prescription that maybe can enter the Ricipe for health care food kind of medicine through health ministry.Through preliminary experiment, Chinese medicine preparation is decided to be: prepared fleece flower root, the root of kudzu vine, Ligusticum wallichii, dried orange peel.Prepared fleece flower root is a monarch drug in a prescription in the side, and the flat power of property is slow, has filling liver kidney, and effects such as benefiting essence-blood are the good merchantable brand that health care is prolonged life, and consumption is suitable big.Though it is a tonic, the efficacy of a drug is gentle, and is oiliness not dry; The root of kudzu vine, Ligusticum wallichii are ministerial drug, and root of kudzu vine nature and flavor are sweet flat, can the expelling pathogenic factors from muscles and skin Shujin, promote the production of body fluid to quench thirst, and good expander, hypotensive effect are arranged, and act on gentlely, be usually used in controlling stiff nape and back and diabete etc., modern hypertension and cervical spondylopathy, the diabetes etc. of being used for more; The up head of Ligusticum wallichii energy, wind-expelling pain-stopping, dredging the channel, vital energy regualting and blood circulation-promoting, the title that " gas medicine in the blood " arranged, be used to control syndrome of qi stagnation and blood stasis more, modern is many to control atherosclerotic, cerebral thrombosis and hyperlipidemia, can effectively prevent and treat cardiovascular and cerebrovascular disease, and Ligusticum wallichii smell hero is strong, the efficacy of a drug is stronger, so should not use more; The hot perfume of dried orange peel is bitter dry, is longer than regulating qi-flowing for strengthening spleen, and is eliminating dampness and eliminating phlegm, helps digestion, is apt to control the taste stagnation of the circulation of vital energy, can make the stagnant property of the greasy heap soil or fertilizer over and around the roots of taste of tonic again, is adjutant, and consumption is suitable little.
Pickle with traditional handicraft and be as the criterion, it is 15% of amount of liquid medicine that technology tentatively is decided to be brine concentration, contains 15g salt in promptly every 100ml soup.
According to above-mentioned analysis, determine that the technical scheme that realizes the object of the invention is:
A kind of fleece-flower root medicinal food salted duck egg, form by the feed liquid immersion, described feed liquid is: the part by weight of prepared fleece flower root, the root of kudzu vine, Ligusticum wallichii, dried orange peel is 6: 5: 2: 2, (100% concentration is 1g crude drug/ml) to be soaked in water, to decoct, to be concentrated to concentration 100%, add the salt dissolving, brine concentration is 15% (its proportion is 1.17 ± 0.01)) be medicinal food salted duck egg and soak feed liquid.
The method for salting of fleece-flower root medicinal food salted duck egg of the present invention, it is pickled step and comprises:
1) be 6: 5: 2 with prepared fleece flower root, the root of kudzu vine, Ligusticum wallichii, dried orange peel by mass ratio: it is 1g crude drug/ml that 2 decoctings extract soup to concentration, and adds the salt dissolving, and brine concentration is 15%, must soak feed liquid;
2), be container with crock or glass altar, choose freshly, the complete crackless duck's egg of shell is cleaned and is dried, and inserts container, pours the immersion feed liquid for preparing into, sealing was pickled 25～30 days, got final product, and pickled in winter, spring 30 days, pickled in summer, autumn 25 days.
On the basis of above-mentioned technical maturity, be easier to operation in order to make technology, described soup can also be condensed into medicinal extract, perhaps again in 60～80 ℃ of oven dry, beat powder, it is standby to seal preservation; The medicinal extract or the dry powder that obtain are dissolved in the water, and by yield solution being transferred to concentration is 1g crude drug/ml, and brine concentration is 15% (its proportion is 1.17 ± 0.01), during the dissolving dry extract, adds water with salt, decocts 10 minutes.
The % of concentration described in the present invention is meant that 100ml solution contains the gram of solute (g) number.
By studies have shown that, its Chinese medicine preparation can be penetrated in the Salted duck egg well and go, and can change the structure of material composition in the duck's egg again, and main is to reduce wherein cholesterol level, increases lecithin content; And be that national legislation is clearly for can be used as the kind of food supplement.
Description of drawings
Fig. 1 is test sample among the embodiment 3, reference substance, negative need testing solution liquid chromatogram
Among the figure, be followed successively by from top to bottom: liquid medicine egg white need testing solution, medicine mud egg white need testing solution, liquid medicine yolk need testing solution, medicine mud yolk need testing solution, reference substance solution, commercially available salted egg egg white need testing solution, commercially available salted egg yolk need testing solution, commercially available bright egg egg white need testing solution, commercially available bright egg yolk need testing solution, root of kudzu vine medicinal material need testing solution
The specific embodiment
Following embodiment pickling process route: Chinese medicine immersion → Chinese medicine decocts → concentrates decoction liquor → adding salt dissolving → duck's egg and goes into altar → adding soup → sealing and keep in Dark Place.
In curing process, the concentration of Chinese medicine preparation immersion liquid gets 100% and 75% two kind of concentration respectively, in order to the penetrating power of contrast soup, and whether the change of salt egg main component is had any different.And the Chinese medicine compound prescription immersion liquid carried out the measurement of proportion, the specific gravity difference before and after relatively pickling is for the preparation and the recycling of soup provides reliable data.
After medicinal food salted duck egg is pickled, by to its color of shell, the quality that has or not breakage, albumen and yolk and color, mouthfeel taste, suppleness, the detection of aspects such as free from extraneous odour or fragrance is arranged, prove the pickling process feasibility.
Measure the main traditional Chinese medicine ingredients (as Puerarin) in the herbal cuisine egg, whether can penetrate in the Salted duck egg with proof Chinese medicine compound prescription soup.
The cholesterol before and after detection is pickled in the duck's egg and the content of lecithin, and compare, the content of main component in the duck's egg whether can be changed with proof Chinese medicine compound prescription soup.
Embodiment 1:
Get prepared fleece flower root 600g, root of kudzu vine 500g, Ligusticum wallichii 200g, dried orange peel 200g place stainless-steel pan, add warm water about 40 ℃ to the submergence medicinal material, after soaking more than 30 minutes, respectively add twice of water 2000ml slow fire boiling, decocting time begins to calculate with boiling, decocting for the first time is 25 ± 5 minutes, and decocting for the second time is 35 ± 5 minutes.Mix twice decoction liquor and be concentrated into 1500ml, after the adding salt 225g dissolving, be the medicinal food salted duck egg soak, soak is cooled to room temperature.
Get 15 pieces of about 1000g of duck's egg and place the water seal altar, and on duck's egg, press, in order to avoid come-up is poured soak into, the submergence duck's egg with weight.The altar mouth keeps in Dark Place after adding water-stop.
The result's following (table 1) who measures.
The proportion of table 1 Chinese medicine preparation immersion liquid before and after pickling
On the basis of above-mentioned technical maturity, be easier to operation in order to make technology, also soup can be condensed into medicinal extract, powder is beaten in oven dry, and bake out temperature is 60～80 ℃, and will progressively heat up, and hermetically drying is preserved standby.Medicinal extract is dissolved in the water before pickling, concentration and salinity are transferred to required numerical value get final product.Dissolving is during dry extract, adds the about 1450ml of water, with salt 225g, decocts 10 minutes, and makes its proportion reach 1.17.
General proterties comparative experiments
The difference of its appearance character of salt egg that the comparison distinct methods is pickled.In experiment, 2 kinds of prescriptions have been adopted in the Chinese medicine compound prescription immersion liquid simultaneously, and medicinal material and constant rate in the prescription 1 are prepared fleece flower root 600g, root of kudzu vine 500g, Ligusticum wallichii 200g, dried orange peel 200g, remove dried orange peel in the prescription 2, and liquor strength is constant, is 100%.Purpose is to observe the influence of dried orange peel to experimental result.Result's following (table 2).
The appearance character of table 2 distinct methods institute salt manufacturing egg relatively
The result shows that the method for Chinese medicine compound prescription immersion liquid pickle salt egg is feasible, and its mouthfeel is similar to the ordinary salt water law to outward appearance, and fragrance slightly.
Embodiment 3
Root of kudzu vine assay in the salted egg
1.1 instrument and reagent
High performance liquid chromatograph (Agilent 1100serious): quaternary pump (G1311A Quat Pump) single pump (G1310A Iso Pump) UV-detector (G1314A VWD) column oven (G1316A COLCOM) degasser (G1322A DEGASSER)
Chromatographic work station ChemStation for LC Re.A.09.01);
Chromatographic column: Zobax SB-C18 (5 μ m, 250mm * 4.6mm ID)
Assay balance (sartorious BP211D) SK8200H ultrasonic washing instrument (450W 59kHz Shanghai High Kudos Science Instrument Co., Ltd.)
Reference substance Puerarin (110831-200302 of Nat'l Pharmaceutical ﹠ Biological Products Control Institute)
It is pure that all reagent are analysis; Water is redistilled water
Test sample and the self-control of negative control product
1.2 chromatographic condition and system suitability test
Chromatographic condition contains Puerarin each kind chromatographic condition and repetition test with reference to 2005 editions one one of Pharmacopoeia of People's Republic of China, selects as follows:
Chromatographic column: Zobax SB-C18 (5 μ m, 150mm * 4.6mm ID)
Phase flows: methanol-water (20: 80)
Flow velocity: 1.0ml/min; Column temperature: 40 ℃; Detect wavelength: 250nm.
Under selected condition, but other chromatographic peak baseline separation in Puerarin and the need testing solution, and the separating degree of Puerarin and its adjacent chromatographic peak is greater than 1.5; Calculate by puerarin peak, theoretical cam curve (N) meets the assay requirement, get negative need testing solution sample introduction simultaneously, the result shows that negative control product solution (commercially available salted egg albumen need testing solution, commercially available preserved egg yellow need testing solution, commercially available fresh egg white need testing solution, commercially available fresh yolk need testing solution) does not have respective peaks and occurs in the puerarin peak position.The high-efficient liquid phase chromatogram of test sample, reference substance, negative control product etc. is seen Fig. 1
1.3 the preparation of reference substance solution
Precision takes by weighing puts the Puerarin reference substance 0.00215g that is dried to constant weight in the phosphorus pentoxide vacuum drying apparatus, puts in the 100ml measuring bottle, adds methyl alcohol and is diluted to scale, promptly.
1.4 the preparation of need testing solution is with reference to thin-layer chromatography need testing solution preparation method
Get one piece of preserving salted egg, shell, divide and get yolk, egg white, weigh respectively, all soaked 1 day with 200ml methyl alcohol, stir, jolting is frequently filtered, filtrate evaporate to dryness, an amount of methyl alcohol dissolving, be transferred in the 25ml measuring bottle, add methyl alcohol and be diluted to scale, get an amount of 12000rpm, get supernatant, promptly.
1.5 taking by weighing, the investigation precision of linear relationship puts the Puerarin reference substance 0.00215g that is dried to constant weight in the phosphorus pentoxide vacuum drying apparatus, put in the 100ml measuring bottle, add 50% methyl alcohol and be diluted to scale, promptly get reference substance solution, get 1 μ l, 2 μ l, 3 μ l, 4 μ l, 5 μ l sample introduction respectively, press condition mensuration under the chromatographic condition item, the results are shown in Table 3-1.
The investigation result of table 3-1 linear relationship
Calibration curve is: Y=406.58X-2.81, and r=0.99957, the result shows that Puerarin becomes good linear relationship with peak area in 0.215 μ g～1.075 μ g scopes.
1.6 assay method calibration curve standard measure is got each 10 μ l of need testing solution, injects liquid chromatograph, the condition of press under the chromatographic condition item is measured, substitution calibration curve as a result, and the amount of calculating Puerarin is calculated as follows content:
m×VX/(VIn×M)
The amount of m Puerarin (μ g); VIn sampling volume (10 μ l); The volume of VX need testing solution (25ml)
M example weight (g yolk or egg white)
Respectively pickle sample 1.7 assay is got, make need testing solution, press operation under chromatographic condition item and the assay method item, measure, the results are shown in Table 3-2 by the preparation below method of need testing solution.
Table 3-2 assay result
/ expression peak area＜10 can not be measured.
Respectively pickle sample 1.8 get, make need testing solution, press operation under chromatographic condition item and the assay method item, measure, the results are shown in Table 3 by the preparation below method of need testing solution.
Each sample root of kudzu vine assay result of table 3
The result shows, all can detect Puerarin acid in the salt egg that liquid medicine is pickled.
Execute example 4
The content of lecithin, cholesterine, aliphatic acid relatively reaches the influence experiment of dried orange peel to main component in the salt egg in the duck's egg.Get 4 samples for every group, repeat once to get average.Experimental technique with reference to Li Zhonghong etc. (Zhang Caixia is etc. the approximate Determination on content of cholesterine lecithin and aliphatic acid in the yolk for Li Zhonghong, Li Xuejun. gansu science and technology, 2003,19 (9): method 125～126).Experimental result is as follows.
Table 4 Chinese medicine preparation is to the influence of egg yolk lecithin, cholesterine, content of fatty acid
Unit: gram/100 grams
The result shows, the salt egg that the Chinese medicine compound prescription immersion liquid is made, lecithin wherein and content of fatty acid are high than the ordinary salt egg, and cholesteric content is lower than ordinary salt egg.And the content that lecithin in the made salt egg of dried orange peel side's group is arranged is than no dried orange peel Fang Zugao, and cholesterol level is high slightly.(the prescriptions of traditional Chinese medicine soup is all finished in an experiment the content influence of main component the main component influence and the dried orange peel of duck's egg)
Liquor strength is to the influence experiment of main component in the salt egg
Table 5 concentration is to the influence (unit: g/100g) of egg yolk lecithin, cholesterine, content of fatty acid
The result shows that in three kinds of immersion liquid, the content of the lecithin in the infuse salted egg of the Chinese medicine compound prescription immersion liquid of 75% concentration institute, cholesterine, aliphatic acid is all high than other two kinds of immersion liquid; Cholesterol content in the infuse salted egg of Chinese medicine compound prescription immersion liquid institute of 100% concentration is minimum.
Experimental result proves that herbal cuisine pickling process of the present invention is feasible.
The salted egg that the Chinese medicine preparation soup is pickled gained mouthfeel with in appearance with common salted egg there was no significant difference, there is no obvious peculiar smell (taste that mainly refers to Chinese medicine); Its edibility part is basic identical with common salted egg on smell and suppleness, and dried orange peel fragrance slightly, has more increased the sense organ inducing action of salted egg.In curing process, need only herbal cuisine pickling process in strict accordance with salted egg, grasp the concentration of immersion liquid, sealing is complete, and salted egg does not have rotten situation to occur, does not need to prolong the time of pickling yet.
Testing result shows, the existence of Puerarin is all arranged in every batch of test sample, and the puerarin content in each salted egg is about 10% (Deng Shiqin of clinical treatment amount, Zheng Qiping, Li Jianming. the clinical observation on the therapeutic effect of Puerarin treatment acute cerebral infarction. practical general family medicine, 2007,5 (4): 345), meet the content standard of health food Chinese traditional medicine.Thereby proved that also pickling process is feasible, drug ingedient can see through eggshell and infiltrate in the egg.
Experimental result shows, the soup that contains the Chinese medicine compound prescription liquid of dried orange peel and 75% concentration is more obvious to the content influence of the lecithin in the salt egg, cholesterine and aliphatic acid, the content that lecithin in the compound feed liquid of dried orange peel and the salt egg that 75% compound feed liquid is pickled and aliphatic acid arranged all than other group for high.Illustrate that dried orange peel more helps the infiltration of medicine, liquor strength is that the permeability of 75% medicine is better; And that immersion liquid concentration is cholesterol content in 100% the infuse salted egg is minimum, also is noticeable phenomenon.As seen liquor strength is tangible to the permeability of medicine and to the influence of the nutrient in the duck's egg.
Chinese medicine preparation is reasonable.The Chinese medicine preparation of this research is with nourishing liver and kidney, and vital energy regualting and blood circulation-promoting is dredged through vein relaxing, and the invigorating the spleen and stomach major function can be played building up healthful vital energy, strengthens the dirty function of liver,spleen,kidney three, the effect that stagnation resolvation is promoted blood circulation.Proper with middle-aged and old function degradations, insufficiency of vital energy and blood, it is relative that passages through which vital energy circulates loses smooth physiological and pathological feature, demonstrated fully the traditional Chinese medical science " normal treatment " and the dialectical principle of executing meals.So can play certain health care effect, and may prevent and reduce the generation of cardiovascular and cerebrovascular disease.
Contain the main component in the compound soup in the herbal cuisine salted egg.In herbal cuisine salted egg, detected the main component Puerarin in the Chinese medicine preparation.The traditional Chinese medicine ingredients that contains in the proof Chinese medicine preparation can be gone by pickling to penetrate in the duck's egg.So can guarantee that the Chinese medicine health-care effect is brought into play.
Change has taken place in the main nutrients structure in the herbal cuisine salted egg.As contain than the higher lecithin of common salted egg and oleic acid and lower cholesterol.Aliphatic acid in its yolk, based on monounsaturated fatty acids, oleic acid accounts for 50%, and linoleic acid is 10%.Oleic acid is similar to the polyunsaturated fatty acid effect, and the effect that reduces cholesterolemia, triglyceride, LDL-C is arranged, and does not have the fraud that reduces HDL-C.And its contained lecithin can reduce cholesterolemia, can promote the absorption of liposoluble vitamin again.And high cholesterol is the important risk factor that illnesss such as hyperlipidemia, hypertension take place.So herbal cuisine salted egg not only can promote the metabolism of body by the effect of Chinese medicine, prevent cholesterol deposition in vivo, and its special lipid structure more meets the nutrition and the prophylactic demand of the elderly and associated patient.
Claims (3)
1, a kind of fleece-flower root medicinal food salted duck egg, form by the feed liquid immersion, described feed liquid is: the part by weight of prepared fleece flower root, the root of kudzu vine, Ligusticum wallichii, dried orange peel is 6: 5: 2: 2, being soaked in water, decocting, being concentrated to concentration is 1g crude drug/ml, add the salt dissolving, brine concentration is 15%, is medicinal food salted duck egg and soaks feed liquid.
2, the method for salting of the described fleece-flower root medicinal food salted duck egg of claim 1 is characterized in that, pickles step and comprises:
1) be 6: 5: 2 with prepared fleece flower root, the root of kudzu vine, Ligusticum wallichii, dried orange peel by mass ratio: it is 1g crude drug/ml that 2 decoctings extract soup to concentration, and adds the salt dissolving, and brine concentration is 15%, must soak feed liquid;
2), be container with crock or glass altar, choose freshly, the complete crackless duck's egg of shell is cleaned and is dried, and inserts container, pours the immersion feed liquid for preparing into, sealing was pickled 25～30 days, got final product, and pickled in winter, spring 30 days, pickled in summer, autumn 25 days.
3, the method for salting of fleece-flower root medicinal food salted duck egg as claimed in claim 2 is characterized in that, described soup is condensed into medicinal extract, perhaps again in 60～80 ℃ of oven dry, beat powder, sealing is preserved standby; The medicinal extract or the dry powder that obtain are dissolved in the water, and by yield solution being transferred to concentration is 1g crude drug/ml, and brine concentration is 15%, during the dissolving dry extract, adds water with salt, decocts 10 minutes.
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2008
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