CN101234075A - Method for producing attapulgite mother chrysanthemum toothpaste - Google Patents

Method for producing attapulgite mother chrysanthemum toothpaste Download PDF

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Publication number
CN101234075A
CN101234075A CNA2008100189060A CN200810018906A CN101234075A CN 101234075 A CN101234075 A CN 101234075A CN A2008100189060 A CNA2008100189060 A CN A2008100189060A CN 200810018906 A CN200810018906 A CN 200810018906A CN 101234075 A CN101234075 A CN 101234075A
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China
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attapulgite
toothpaste
speed
mother chrysanthemum
wild chrysanthemum
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CN100539991C (en
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袁长兵
贾剑
许庆华
许盛英
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Huai'an University Science & Technology Park Management Co Ltd
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Abstract

The invention discloses a method for producing attapulgite wild chrysanthemum indicum toothpaste, which has the following key points of the technical proposal: the ingredients is carried out the processes of proportioning, stirring at low speed, crushing and pulping, grinding, stirring at high speed, vacuum degassing and then is canned for obtaining the finished products of the attapulgite wild chrysanthemum indicum toothpaste. The attapulgite wild chrysanthemum indicum toothpaste is consisted of pasty attapulgite clay, fresh wild chrysanthemum indicum, alcohol, honey, sodium dodecyl sulfate and demin-water. The attapulgite wild chrysanthemum indicum toothpaste is characterized by being clean, soft and smoothness, strong foaming power, good stability, being cool and refreshing, as well as that paste does not overflow out of the toothpaste, no water is separated, fragrance, color and luster are normal and no mark is left on slides. The attapulgite wild chrysanthemum indicum toothpaste is able to directly adsorb and clear away a plurality of offensive odor and tastes in mouth cavities, prevent bleeding gum and has certain auxiliary effects for preventing mouth diseases. The production method is applicable to producing the attapulgite wild chrysanthemum indicum toothpaste, Chinese herbal toothpastes and other medicated toothpastes.

Description

The production method of attapulgite mother chrysanthemum toothpaste
Technical field:
The present invention relates to toothpaste, be specifically related to a kind of production method of attapulgite mother chrysanthemum toothpaste.
Background technology:
Chinese herbal medicine is abundant in the China source, and a lot of ancient prescription curative effects are all very definite, and toxic and side effects is littler than Western medicine, and common people also accept, so Chinese herbal medicine is preventing that the oral disease field has the excellent research DEVELOPMENT PROSPECT really.
Chinese herbal medicine adding ingredient in the toothpaste relates to processes such as Chinese herbal medicine collection, processing, effective ingredient refinement, and it has determined directly whether the elite composition that adds in the toothpaste can play a role.
The Chinese herbal medicine that is adopted in the Chinese herbal toothpaste is the Chinese herbal medicine finished product after drying mostly, also has the infusion method of employing to extract its soak or its concentrated solution, still contains a large amount of effective ingredient in the garbage behind the medicinal herb soak, causes bigger economic loss.
The abrasivus that Chinese herbal toothpaste is commonly used has calcium carbonate, calcium phosphate dibasic dihydrate, no hydration calcium hydrogen phosphate, calcium pyrophosphate, anhydride silica, aluminium hydroxide etc., because these abrasivus hardness height, granule is coarse, there is not stickiness, absorption property is poor, and life-time service easily causes wearing and tearing to the enamel of dental surface.
Summary of the invention:
The objective of the invention is to overcome weak point in the prior art, a kind of production method of attapulgite mother chrysanthemum toothpaste is provided.
The production method of attapulgite mother chrysanthemum toothpaste is, batching, stirring at low speed, pulverizing making beating, grinding, high-speed stirred, vacuum outgas, canned be the finished product of attapulgite mother chrysanthemum toothpaste.
Attapulgite mother chrysanthemum toothpaste is made up of lip lipstick attapulgite clay, fresh Flos Chrysanthemi Indici, ethanol, Mel, sodium lauryl sulphate and deionized water.
Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m 2More than/the g, most cation, hydrone and a certain size organic molecule all can directly be adsorbed in the duct.
Use attapulgite ore pul making production technology, the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of lip lipstick attapulgite clay, have the characteristics of ultrafine dust, friction little, the no sand feeling of hardness and soft fine and smooth free from extraneous odour.
Lip lipstick attapulgite clay is through powerful stirring at a high speed, become the special good natural gelinite of a kind of thixotropy and gumminess, viscosity is up to more than the 10000mPas, absorption property and performance of keeping humidity have all obtained further raising, attapulgite clay after the high-speed stirred, total characteristic with abrasivus, adhesive and wetting agent, use lip lipstick attapulgite clay to produce toothpaste and do not need to add in addition abrasivus, adhesive and wetting agent, not only can improve the quality of toothpaste, can also reduce production costs greatly.
Flos Chrysanthemi Indici is " broad ectrum antibiotic " in the Chinese herbal medicine, and most dermatophytess, staphylococcus aureus, dysentery bacterium, bacillus pyocyaneus and influenza virus etc. are all had stronger inhibitory action.Have effects such as heat-clearing and toxic substances removing, expelling phlegm for arresting cough, regulating QI to relieve pain, anti-inflammation hemostasia, antibiotic, antiviral.
The molecule of ethanol has very big penetration, can pass the film of bacterium surface, squeezes into antibacterial inside, makes the protein coagulating that constitutes antibacterial life basis, and antibacterial is killed; Ethanol is a kind of good solvent, can dissolve many indissolubles or water-fast material.
Mel rich in proteins, aminoacid, mineral, vitamin, and multiple enzyme, organic acid, aromatic substance, volatile oil, pigment etc.Mel is a kind of natural antibacterial, and high-quality Mel is at room temperature placed the several years can be not corrupt.
Sodium lauryl sulphate belongs to anion surfactant, and is soluble in water, and compatibility is good again with anion, nonionic, has good emulsifying, foaming, infiltration, decontamination and dispersive property, and foaming power is strong.
The present invention is achieved by following technical proposals:
The production method of attapulgite mother chrysanthemum toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with attapulgite mother chrysanthemum toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite mother chrysanthemum toothpaste, the speed controlling of blender is at 500~800 rev/mins, the stirring at low speed time was controlled at 5~15 minutes, and the speed controlling of pulverizing beater is at 2500~3000 rev/mins; The purpose of stirring at low speed is that various batchings are stirred, and helps pulverizing the operate as normal of beater; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.025 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; Multi-functional colloid grinding tool has functions such as the pulverizing of wet processed fluid ultra micron, grinding, emulsifying, dispersion, homogenizing, stirring, mixing, can replace and be better than stone grinder, sand mill, ball mill, dispersing emulsification machine, shearing disperse pump, work efficiencies such as homogeneous emulsifying machine, three-roller, tissue mashing machine; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000~11000 rev/mins, and the high-speed stirred time was controlled at 5~30 minutes; The ultrahigh speed blender has unique blade design and stepless speed-regulating device, can select optimal speed according to manufacturing technique requirent, and after the pasty mixture after the grinding stirred through ultrahigh speed, viscosity was up to more than the 10000mPas; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite mother chrysanthemum toothpaste.
The batching of described attapulgite mother chrysanthemum toothpaste is made up of following component: lip lipstick attapulgite clay 30~60%, fresh Flos Chrysanthemi Indici 5~25%, ethanol 5~15%, Mel 1~10%, sodium lauryl sulphate 0.2~2.5% and deionized water 15~45% by weight percentage.
The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay.
This production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.
Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 15~35%, water 65~85%.
Attapulgite mother chrysanthemum toothpaste uses lip lipstick attapulgite clay to be primary raw material, does not need to add in addition abrasivus, adhesive and wetting agent, not only can improve the quality of toothpaste, can also reduce production costs greatly.
Attapulgite mother chrysanthemum toothpaste uses fresh Flos Chrysanthemi Indici, not only can make full use of the effective ingredient of Flos Chrysanthemi Indici, reduce pollution in the dry in the sun process, go mouldy and production cost, and the Plant fiber who has kept Flos Chrysanthemi Indici, can increase the denseness of lotion of toothpaste, help increasing the friction of toothpaste, improve the friction effect and the stability of toothpaste.
The cleaning of attapulgite mother chrysanthemum toothpaste mastic, soft fine and smooth, strong, refrigerant tasty and refreshing, the good stability of foaming power; Mastic does not overflow the mouth of pipe, does not separate water outlet, and the fragrance color and luster is normal, the slide no marking.
Attapulgite mother chrysanthemum toothpaste can directly adsorb and remove multiple foreign odor flavor, the prevention gingival hemorrhage in the oral cavity, and the prevention oral disease is had certain assosting effect.
The present invention is applicable to and produces attapulgite mother chrysanthemum toothpaste, Chinese herbal toothpaste and other medicines toothpaste.
The specific embodiment:
The invention will be further described below in conjunction with embodiment:
The production method of attapulgite mother chrysanthemum toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with attapulgite mother chrysanthemum toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite mother chrysanthemum toothpaste, the speed controlling of blender is at 600 rev/mins, the stirring at low speed time was controlled at 8 minutes, and the speed controlling of pulverizing beater is at 2800 rev/mins; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 8000 rev/mins, and the high-speed stirred time was controlled at 20 minutes; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite mother chrysanthemum toothpaste.
The batching of described attapulgite mother chrysanthemum toothpaste is made up of following component: lip lipstick attapulgite clay 38%, fresh Flos Chrysanthemi Indici 20%, ethanol 10%, Mel 5.5%, sodium lauryl sulphate 1.5% and deionized water 25% by weight percentage.
Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30%, water 70%.
Main physical and chemical index testing result:
Project Index Testing result
Physical and chemical index Denseness, mm 9~33 29
Squeeze cream pressure, kPa≤ 40 32
Foam volume, mm 〉= 60 72
pH 5.0~10.0 8.3
Stability Mastic does not overflow the mouth of pipe, does not separate water outlet, and the fragrance color and luster is normal Mastic does not overflow the mouth of pipe, does not separate water outlet, and the fragrance color and luster is normal
Cross grit The slide no marking The slide no marking

Claims (1)

1, a kind of production method of attapulgite mother chrysanthemum toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with attapulgite mother chrysanthemum toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite mother chrysanthemum toothpaste, the speed controlling of blender is at 500~800 rev/mins, the stirring at low speed time was controlled at 5~15 minutes, and the speed controlling of pulverizing beater is at 2500~3000 rev/mins; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.025 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000~11000 rev/mins, and the high-speed stirred time was controlled at 5~30 minutes; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite mother chrysanthemum toothpaste;
The batching of described attapulgite mother chrysanthemum toothpaste is made up of following component: lip lipstick attapulgite clay 30~60%, fresh Flos Chrysanthemi Indici 5~25%, ethanol 5~15%, Mel 1~10%, sodium lauryl sulphate 0.2~2.5% and deionized water 15~45% by weight percentage;
The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay;
Described lip lipstick attapulgite clay is made up of following component by weight percentage; Attapulgite clay 15~35%, water 65~85%.
CNB2008100189060A 2008-01-31 2008-01-31 The production method of attapulgite mother chrysanthemum toothpaste Expired - Fee Related CN100539991C (en)

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Application Number Priority Date Filing Date Title
CNB2008100189060A CN100539991C (en) 2008-01-31 2008-01-31 The production method of attapulgite mother chrysanthemum toothpaste

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