CN1011943B - 变压吸附系统中控制吸附产品再加压的方法和设备 - Google Patents

变压吸附系统中控制吸附产品再加压的方法和设备

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Publication number
CN1011943B
CN1011943B CN88104542A CN88104542A CN1011943B CN 1011943 B CN1011943 B CN 1011943B CN 88104542 A CN88104542 A CN 88104542A CN 88104542 A CN88104542 A CN 88104542A CN 1011943 B CN1011943 B CN 1011943B
Authority
CN
China
Prior art keywords
product
flow
container
valve
pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CN88104542A
Other languages
English (en)
Chinese (zh)
Other versions
CN1031660A (zh
Inventor
乔格·斯托克
迈克尔·怀索尔
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Union Carbide Corp
Original Assignee
Union Carbide Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Union Carbide Corp filed Critical Union Carbide Corp
Publication of CN1031660A publication Critical patent/CN1031660A/zh
Publication of CN1011943B publication Critical patent/CN1011943B/zh
Expired legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/16—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/502—Carbon monoxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40007—Controlling pressure or temperature swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40013—Pressurization
    • B01D2259/40015—Pressurization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40028—Depressurization
    • B01D2259/4003—Depressurization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40043—Purging
    • B01D2259/4005—Nature of purge gas
    • B01D2259/40052—Recycled product or process gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40075—More than ten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40077—Direction of flow
    • B01D2259/40079—Co-current
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40077—Direction of flow
    • B01D2259/40081—Counter-current
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/404—Further details for adsorption processes and devices using four beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/45—Gas separation or purification devices adapted for specific applications
    • B01D2259/4516—Gas separation or purification devices adapted for specific applications for fuel vapour recovery systems
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0454—Controlling adsorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Jellies, Jams, And Syrups (AREA)
  • Fats And Perfumes (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Pressure Welding/Diffusion-Bonding (AREA)
  • Bending Of Plates, Rods, And Pipes (AREA)
  • Auxiliary Devices For And Details Of Packaging Control (AREA)
  • Vending Machines For Individual Products (AREA)
  • Manipulator (AREA)
  • Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
  • Earth Drilling (AREA)
  • Massaging Devices (AREA)
  • Control Of Fluid Pressure (AREA)
CN88104542A 1987-09-01 1988-06-15 变压吸附系统中控制吸附产品再加压的方法和设备 Expired CN1011943B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US091,889 1987-09-01
US07/091,889 US4761165A (en) 1987-09-01 1987-09-01 Pressure swing adsorption control method and apparatus

Publications (2)

Publication Number Publication Date
CN1031660A CN1031660A (zh) 1989-03-15
CN1011943B true CN1011943B (zh) 1991-03-13

Family

ID=22230133

Family Applications (1)

Application Number Title Priority Date Filing Date
CN88104542A Expired CN1011943B (zh) 1987-09-01 1988-06-15 变压吸附系统中控制吸附产品再加压的方法和设备

Country Status (18)

Country Link
US (1) US4761165A (OSRAM)
EP (1) EP0305663B1 (OSRAM)
JP (1) JPH074498B2 (OSRAM)
KR (1) KR930000641B1 (OSRAM)
CN (1) CN1011943B (OSRAM)
AT (1) ATE73684T1 (OSRAM)
AU (1) AU610187B2 (OSRAM)
BR (1) BR8802919A (OSRAM)
CA (1) CA1314493C (OSRAM)
DE (1) DE3869276D1 (OSRAM)
ES (1) ES2030791T3 (OSRAM)
GR (1) GR3004287T3 (OSRAM)
IN (1) IN171513B (OSRAM)
MX (1) MX165284B (OSRAM)
MY (1) MY103103A (OSRAM)
NO (1) NO173639C (OSRAM)
NZ (1) NZ225039A (OSRAM)
ZA (1) ZA884282B (OSRAM)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101306301B (zh) * 2007-05-15 2011-08-10 气体产品与化学公司 集装箱化的气体分离系统

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DE3830506A1 (de) * 1988-09-08 1990-03-15 Bergwerksverband Gmbh Verfahren zur gewinnung von stickstoff aus sauerstoff und stickstoff enthaltenden gasgemischen mittels druckwechseladsorption an kohlenstoff-molekularsieben
US5042994A (en) * 1990-05-25 1991-08-27 Union Carbide Industrial Gases Technology Corporation Control of pressure swing adsorption operations
US5082474A (en) * 1990-08-14 1992-01-21 The Boc Group, Inc Pressurization psa systems for the production of high purity product gas
US5074893A (en) * 1990-09-04 1991-12-24 On Site Gas Systems, Inc. Fluid adsorption system
US5203888A (en) * 1990-11-23 1993-04-20 Uop Pressure swing adsorption process with multiple desorption steps
US5163978A (en) * 1991-10-08 1992-11-17 Praxair Technology, Inc. Dual product pressure swing adsorption process and system
US5174796A (en) * 1991-10-09 1992-12-29 Uop Process for the purification of natural gas
US5330561A (en) * 1992-11-16 1994-07-19 Air Products And Chemicals, Inc. Extended vacuum swing adsorption process
US5656065A (en) * 1995-10-04 1997-08-12 Air Products And Chemicals, Inc. Multibed pressure swing adsorption apparatus and method for the operation thereof
US5879649A (en) * 1995-12-19 1999-03-09 Corning Incorporated Method for purifying polyalkylsiloxanes and the resulting products
FR2756752B1 (fr) * 1996-12-05 2001-09-14 Air Liquide Procede et installation de traitement d'un melange gazeux par adsorption a variation de pression
FR2769851B1 (fr) * 1997-10-21 1999-12-17 Air Liquide Installation de separation d'un melange de gaz
FR2772637B1 (fr) * 1997-12-18 2000-02-11 Air Liquide Procede de separation gazeuse par adsorption avec production a debit variable, notamment pour la production d'oxygene
FR2783723B1 (fr) * 1998-09-25 2000-12-29 Air Liquide Procede de traitement d'un melange gazeux par adsorption a modulation de pression, a debit variable de production
FR2788993B1 (fr) * 1999-01-29 2001-02-23 Air Liquide Procede d'epuration d'un gaz par adsorption
AU2002217475B2 (en) * 2000-12-25 2005-02-17 Sumitomo Seika Chemicals Co., Ltd. Method for separating hydrogen gas
CA2433156A1 (en) * 2000-12-26 2002-07-04 Sumitomo Seika Chemicals Co., Ltd. Method and device for separating object gas
SG109440A1 (en) * 2001-02-01 2005-03-30 Uop Llc Very large-scale pressure swing adsorption processes
CZ299697B6 (cs) * 2001-02-02 2008-10-22 Uop Llc Zpusob separace neadsorbovatelného plynu strídavou tlakovou adsorpcí
EP1228799B1 (en) * 2001-02-02 2005-05-04 Uop Llc Very large-scale pressure swing adsorption processes
CN1642851B (zh) * 2002-02-05 2010-04-14 加利福尼亚大学董事会 采用自支持加氢气化从含碳材料制备合成运输燃料
US6755895B2 (en) 2002-04-09 2004-06-29 H2Gen Innovations, Inc. Method and apparatus for pressure swing adsorption
JP2004066125A (ja) * 2002-08-07 2004-03-04 Sumitomo Seika Chem Co Ltd 目的ガスの分離方法
US6699307B1 (en) * 2002-10-11 2004-03-02 H2Gen Innovations, Inc. High recovery PSA cycles and apparatus with reduced complexity
FR2856937B1 (fr) * 2003-07-02 2005-08-19 Air Liquide Appareil pour la separation par adsorption a variation de pression d'au moins un constituant d'un melange gazeux
EP1835980A4 (en) * 2005-01-12 2011-02-16 Lummus Technology Inc METHODS AND APPARATUS FOR IMPROVED CONTROL OF PSA FLOW VARIATIONS
FR2883489B1 (fr) * 2005-03-25 2008-01-11 Air Liquide Procede de reglage d'une installation de traitement par adsorption d'un gaz soumis a un ecoulement a travers ladite installation
JP5575399B2 (ja) * 2006-03-06 2014-08-20 ランマス・テクノロジー・インコーポレイテッド Ｐｓａ圧力測定及び制御システム
US7879138B2 (en) * 2006-07-20 2011-02-01 Air Products And Chemicals, Inc. Pressure swing adsorption method and system with multiple-vessel beds
US7695545B2 (en) * 2007-03-14 2010-04-13 Air Products And Chemicals, Inc. Adsorption process to recover hydrogen from feed gas mixtures having low hydrogen concentration
MY171684A (en) * 2007-11-16 2019-10-23 Univ Kebangsaan Malaysia Compact pressure swing adsorption system for hydrogen purification
CN103002970B (zh) * 2010-05-05 2016-01-20 鲁姆斯科技公司 吸附剂床的分级泄料
US8496733B2 (en) 2011-01-11 2013-07-30 Praxair Technology, Inc. Large scale pressure swing adsorption systems having process cycles operating in normal and turndown modes
US8551217B2 (en) 2011-01-11 2013-10-08 Praxair Technology, Inc. Six bed pressure swing adsorption process operating in normal and turndown modes
US8435328B2 (en) 2011-01-11 2013-05-07 Praxair Technology, Inc. Ten bed pressure swing adsorption process operating in normal and turndown modes
US8491704B2 (en) 2011-01-11 2013-07-23 Praxair Technology, Inc. Six bed pressure swing adsorption process operating in normal and turndown modes
US8961627B2 (en) 2011-07-07 2015-02-24 David J Edlund Hydrogen generation assemblies and hydrogen purification devices
US10717040B2 (en) 2012-08-30 2020-07-21 Element 1 Corp. Hydrogen purification devices
US20140065020A1 (en) 2012-08-30 2014-03-06 David J. Edlund Hydrogen generation assemblies
US9187324B2 (en) 2012-08-30 2015-11-17 Element 1 Corp. Hydrogen generation assemblies and hydrogen purification devices
US11738305B2 (en) 2012-08-30 2023-08-29 Element 1 Corp Hydrogen purification devices
CN105268282A (zh) * 2015-09-18 2016-01-27 北京环宇京辉京城气体科技有限公司 一种低温变压吸附制备超纯氢的方法
KR102018322B1 (ko) * 2017-11-14 2019-09-04 한국에너지기술연구원 흡착 공정을 위한 흡착탑 시스템 및 흡착 공정을 이용한 혼합 가스 분리 방법
CN110694428B (zh) * 2019-09-30 2020-06-23 湖南省计量检测研究院 一种氢分离设备的工作方法
US12623181B2 (en) 2023-06-02 2026-05-12 Element 1 Corp Hydrogen purification devices

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AR207266A1 (es) * 1974-10-30 1976-09-22 Union Carbide Corp Procedimiento oscilante adiabatico de presion para la separacion de aire
JPS5299973A (en) * 1976-02-18 1977-08-22 Toray Ind Inc Adsorption and separation apparatus of mixed gas
DE2823211A1 (de) * 1978-05-27 1979-12-06 Bayer Antwerpen Nv Verfahren zum betrieb einer druck- wechsel-adsorptionsanlage
DE2851847A1 (de) * 1978-11-30 1980-06-12 Linde Ag Verfahren zum betrieb einer zyklisch arbeitenden druckwechsel-adsorptionsanlage
DE3040495C2 (de) * 1980-10-28 1986-10-23 Linde Ag, 6200 Wiesbaden Ventilsteuerung
DE3205451A1 (de) * 1982-02-16 1983-08-25 Linde Ag, 6200 Wiesbaden Verfahren zum betreiben einer zyklisch arbeitenden druckwechsel-adsorpitionsanlage
DE3222560A1 (de) * 1982-06-16 1983-12-22 Bergwerksverband Gmbh, 4300 Essen Verfahren zur abtrennung und gewinnung von relativ stark an adsorptionsmitteln adsorbierbaren gasen aus ansonsten im wesentlichen nur leichter adsorbierbare gase enthaltenden gasgemischen sowie anlage zum durchfuehren dieses verfahrens
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101306301B (zh) * 2007-05-15 2011-08-10 气体产品与化学公司 集装箱化的气体分离系统

Also Published As

Publication number Publication date
EP0305663B1 (en) 1992-03-18
MX165284B (es) 1992-11-04
ATE73684T1 (de) 1992-04-15
ES2030791T3 (es) 1992-11-16
NO173639C (no) 1994-01-12
IN171513B (OSRAM) 1992-10-31
EP0305663A1 (en) 1989-03-08
US4761165A (en) 1988-08-02
KR930000641B1 (ko) 1993-01-29
GR3004287T3 (OSRAM) 1993-03-31
NZ225039A (en) 1989-10-27
NO173639B (no) 1993-10-04
AU610187B2 (en) 1991-05-16
BR8802919A (pt) 1989-03-21
JPH074498B2 (ja) 1995-01-25
CN1031660A (zh) 1989-03-15
ZA884282B (en) 1989-03-29
NO882643D0 (no) 1988-06-15
CA1314493C (en) 1993-03-16
DE3869276D1 (de) 1992-04-23
NO882643L (no) 1989-03-02
KR890004759A (ko) 1989-05-09
JPS6463019A (en) 1989-03-09
MY103103A (en) 1993-04-30
AU1773188A (en) 1989-03-02

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C15 Extension of patent right duration from 15 to 20 years for appl. with date before 31.12.1992 and still valid on 11.12.2001 (patent law change 1993)
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