CN101177828A - Polybutylene terephthalate fiber elastic fabric - Google Patents
Polybutylene terephthalate fiber elastic fabric Download PDFInfo
- Publication number
- CN101177828A CN101177828A CNA2006100976175A CN200610097617A CN101177828A CN 101177828 A CN101177828 A CN 101177828A CN A2006100976175 A CNA2006100976175 A CN A2006100976175A CN 200610097617 A CN200610097617 A CN 200610097617A CN 101177828 A CN101177828 A CN 101177828A
- Authority
- CN
- China
- Prior art keywords
- fabric
- yarn
- polybutylene terephthalate
- pbt
- fiber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Woven Fabrics (AREA)
Abstract
The invention discloses an elastic textile of polybutylene terephthalate (PBT) fiber. Either warp yarn or weft yarn made up of the textile is PBT fabricated processing yarn or blended fibber yarn of PBT fabricated processing yarn and other fibers. The elastic textile of the invention not only has good elasticity percentage, elastic recovery percentage and size stability, but also has neat cloth surface, soft texture, etc. The elastic textile can fully present beautiful body line, and greatly enhance extension breadth for exercise and reduces friction with and irritability to the skin when worn.
Description
Technical field
The present invention relates to a kind of elastic fabric.
Background technology
Polybutylene terephthalate (PBT) (PBT) fiber is a kind of novel remodeling polyester fiber.Caused people's attention the earliest as a kind of engineering material of function admirable.Along with the development of fibre in differentiation, characteristics such as PBT fiber excellent elasticity more and more are subjected to attracting attention of people in recent years.But at present because Fabric Design, back arrangement processing increases bullet to fiber, the influence of Fabric Style also lacks clear and definite analysis, technology is also imperfect, make general fabrics design and the PBT fabric that processes spring rate bad (below 15%) to occur, DIMENSIONAL STABILITY relatively poor (dry-hot shrinkage is ± 4~± 5%, and boiling water shrinkage is ± 4~± 5%), or defective such as the fabric face out-of-flatness is wrinkling.Limited of the development of PBT fiber at field of textiles.In order to break this situation, this just makes that the analysis and research of PBT Fabric Design and rear processing finishing technology are imperative.
Summary of the invention
The object of the present invention is to provide a kind of have favorable elasticity rate and DIMENSIONAL STABILITY, surfacing, the elastic fabric of soft polybutylene terephthalate (PBT) fiber.
Technical solution of the present invention is
A kind of elastic fabric of polybutylene terephthalate (PBT) fiber is characterized in that: at least a in the warp thread of composition fabric or the weft yarn is the mixed fiber yarn of polybutylene terephthalate false-twisted yarn or polybutylene terephthalate false-twisted yarn and other fiber.
The spring rate of fabric is 15%~60%, elastic recovery rate more than 80% and 160 dry-hot shrinkages when spending in+1.0%~-3.0%, boiling water shrinkage is in+1.0%~-2.5%.
The polybutylene terephthalate fiber content accounts for 20%~100% of total fabric weight.
The tightness of fabric is 700-2000.
The filament number of polybutylene terephthalate fiber is 0.5~5.6dtex.
The interlacing number of weft yarn is 0~80/meter, and the interlacing number of warp thread is 50~120/meter.
The selection that below divides yarn, Fabric Design, arrangement processing 3 aspects, back are described in detail:
1. the selection of yarn
1) among the present invention, the filament number of the PBT fiber of use is thick more, and feel is hard more.So adopting the fiber number of monofilament is 0.5~5.6dtex, to obtain soft hand feeling.Because filament mutual extrusion when getting over the multi-fibre contraction with the filament radical of fiber number yarn, make the minimizing of shrink space, so thereby influence being chosen in when considering feel of spring rate filament radical of yarn and fabric, because of adopt few filament radical as far as possible.Example: 50D-12f-PBTDTY, 75D-24f-PBTDTY etc.
2) intensity of yarn considers that to the requirement of yarn strength the intensity of yarn is in 2.0~5.0cN/dtex scope from road, back process such as weaving, and degree of stretching is 30%~60%.
3) the interlacing number of yarn is few more, and the obstruction that yarn is subjected to when shrinking is also more little, is guaranteeing to adopt the less yarn of interlacing under the normal woven prerequisite so the elasticity of yarn and fabric is also just big more as far as possible.Example: weft yarn time spent interlacing number is 0~80/meter, and the warp thread time spent is 50~120/meter.
2. Fabric Design
1) the present invention can select to carry out weaving through bullet, latitude bullet or longitude and latitude elastic fabric according to purpose.Make the mixed fiber yarn that when elastic fabric warp thread uses PBT false-twisted yarn or false-twisted yarn and other fiber, weft yarn is PET, cotton or other yarn.Weft yarn uses the mixed fiber yarn of PBT false-twisted yarn or false-twisted yarn and other fiber when making the latitude elastic fabric, and weft yarn is PET, cotton or other yarn.Make the four sides when playing longitude and latitude all use the mixed fiber yarn of PBT false-twisted yarn or false-twisted yarn and other fiber.PBT false-twisted yarn or false-twisted yarn and other fiber mix fine or interweave, and be cost-saved on the one hand, can incorporate the advantage of another yarn on the other hand again.
2) the PBT fiber content accounts for 20%~100% of fabric weight among the present invention, considers the performance of the characteristic of PBT, and better content is 50~100%.Content can make the elasticity of fabric and feel be brought into play fully in above-mentioned scope.
3) tissue of fabric can adopt plain weave among the present invention, twill, satin weave or its alternative construction.Heavily flat as 2/2 latitude, 2/1 twill, 2/2 twill, 5 pieces of satin weaves etc.Its middle twill compares with plain weave because relative minimizing of the degree of crook of yarn in fabric (reducing through weft yarn cross-point number in the unit are), the obstruction power when yarn shrinks in the fabric that makes reduces, the free movable ability of yarn strengthens, thereby make the contractility grow of fabric, through after processing back be difficult to produce under the prerequisite of wrinkle and forming high elastic fabric, be preferred tissue.
4) the present invention is in order to obtain 15%~60% spring rate, the tightness of fabric is 700~2000, best warp-wise tightness is 900~1200 when making with the heavy plain weave of 2/2 latitude as 50D/12f warp thread and 75D/24f weft yarn, best broadwise tightness is 700~950, in this scope fabric face do not crease easily and DIMENSIONAL STABILITY good.
5) though of the present invention to weave loom available jet, water spray, looms such as arrow shaft are weaved, but consider the wefting insertion of avoiding under the high-tension that allows the elasticity of weft yarn fully play and the generation that reduces broadwise spring rate difference, so jet, the water jet looms weaving less when selecting wefting insertion to the yarn active force.
3. back arrangement processing
Back arrangement of the present invention can comprise following content: concise, and middle typing, dyeing resin, finished product typing.Can implement bleaching according to the concrete condition of the blending and the object fiber that interweaves in addition, singe operations such as decrement.
1) temperature is 60~100 ℃ during refining, adopts heat alkali liquid, and it is dirty that soaping agent (soaping agent is a non-cationic type surfactant, routine GQ008) is removed when weaving slurry on the yarn and greasy dirt etc.Because fabric is refining under the liquid of higher temperature, yarn has been removed the influence of tension force, and contraction to a certain degree is to the increase of fabric elasticity rate and obtain not having the smooth surface of wrinkle and play a role.
2) the middle typing before the dyeing also is in order to guarantee the smooth surface of fabric on the one hand, be unlikely to fierce the contraction when making dyeing and produce wrinkle, and dry-hot shrinkage is in+1.0%~-3.0% when guaranteeing 160 ℃, and boiling water shrinkage plays main effect+1.0%~-2.5% with interior.Treatment temperature is 140~180 ℃, and the interior constancy of this temperature range is good and kept curling of false twist yarn can the elasticity of fabric not to be caused damage.Though the above HEAT SETTING effect of temperature 180 degree can increase but the feel hardening to some extent, the phenomenon of loss of elasticity is comparatively serious.Along with on dye the prolongation dyestuff of time the fiber dye-uptake presented the downward trend again that raises earlier.The HEAT SETTING processing time is when scope was interior in 40~70 seconds, to make dye molecule reach the highest to the fiber dye-uptake.
3) owing to compared among the PBT two methyl many with PET, make intermolecular cohesiveness reduce, when relatively low dyeing temperature, just can obtain PET fiber resulting Color under high-temperature and high-pressure conditions, according to the mixed fibre situation dyeing treatment conditions that interweave is 120~135 ℃, and the time is 20~50 minutes.
4) can use during resin finishing antistatic additive (CATION or anionic antistatic agent, routine DEATRON) and softener (silicon system or non-silicon anionic softener are as TF438) to adjust the feel of fabric.
5) the finished product setting temperature is 150~180 ℃, and the time is 40~70 seconds.
The present invention have general fabrics design and back arrangement processing incomparable advantage: have the excellent elasticity rate, elastic recovery rate and good DIMENSIONAL STABILITY, surfacing, characteristics such as soft.The lines that can fully represent the human body grace when wearing strengthen the elongation amplitude of people when moving widely, reduce friction and stimulation with skin.
4. the explanation of related assays method
1) fabric elasticity rate
The cloth specimen of getting 5cm*30cm is through each 3 of broadwises.The folder mouth spacing that the strength and elongation instrument is set is 20cm, and draw speed is 20cm/min, and sample cloth is sandwiched in the mouth, and hanging up loading just is that 5cm*1m size cloth specimen is heavy, makes the stretching cloth, measures and presss from both sides a mouthful spacing L (cm), calculating elastic rate when being stretched to 14.7N.Spring rate=(L-20)/20*100%.The mean value of 3 cloth of the broadwise of learning from else's experience.
2) fabric elasticity response rate
The cloth specimen of getting 5cm*30cm is through each 3 of broadwises.The folder mouth spacing that the strength and elongation instrument is set is 20cm, and draw speed is 20cm/min, and sample cloth is sandwiched in the mouth, and hanging up loading just is that 5cm*1m size cloth specimen is heavy.Make the stretching cloth, original position placement 3 minutes were placed 1 minute and then be returned in 80% back that is stretched to spring rate.Stretch repeatedly as stated above after 5 times, move the above loading position of initial loading again to.Measure residual elongation, the calculating elastic response rate from the curve of loading-elongation of record.Elastic recovery rate=(L1-L)/L*100%.The mean value of 3 cloth of the broadwise of learning from else's experience.L is that spring rate is elongation in 80% o'clock, and L1 is 5 residual elongations in back that stretch.
3) 160 dry-hot shrinkages when spending
3 in sampling 25cm*25cm fabric sample is done the mark of 20cm mark at fabric through each 3 place of broadwise, put into the air flow dryers of 160 degree and handled 3 minutes, takes out the length L (cm) of back each mark of amount and also calculates dry-hot shrinkage.Boiling water shrinkage=(L-20)/20*100% is respectively got the mean value of 3 place's marks through broadwise.
4) boiling water shrinkage
3 in sampling 25cm*25cm fabric sample is done the mark of 20cm mark at fabric through each 3 place of broadwise, with boiling water treating 3 minutes, and the length L (cm) of each mark of amount and calculate boiling water shrinkage after the air dry.Boiling water shrinkage=(L-20)/20*100% is respectively got the mean value of 3 place's marks through broadwise.
The invention will be further described below in conjunction with embodiment.
Embodiment 1:
1) several 95/meter of yarn: warp thread: 150D-48F-DTY (PET) interlacing
Weft yarn: several 25/meter of 75D-24F-PBT interlacing
2) fabric specification and weaving
Tissue: 2/2 twill
Density: through close * filling density=100*82 root/2.54cm
The warp-wise tightness: 1245, broadwise tightness: 710
Mix rate: PET/PBT=23/77
Adopt 4 pieces along piercing into the capable weaving on air-jet loom of gaiting
3) the dyeing afterfinish method comprises the following steps:
A. concise: adopt the NaOH heat alkali liquid of 4% concentration and soaping agent (non-cationic type surfactant GQ008) to remove slurry, dirty and fabric is to a certain degree shunk.Temperature is 95 degree, and the processing time is 60 seconds
B. typing in the middle of: concise dried cloth is carried out the form stable treatment.Temperature is that 180 to spend the time be 60 seconds
C. dyeing processing: adopt under 120 degree and dye middle look, dyeing time is 30 minutes
D. resin finishing: above-mentioned cloth was handled 100 seconds under 140 degree with antistatic DEATRON and softener TF438
E. finished product typing: above-mentioned cloth is carried out last finished product typing, and the temperature of processing is 170 degree, and the processing time is 60 seconds.The finished product that obtains is 115*89 root/2.54cm through close * filling density, and the spring rate of fabric is 25%, and-2.0%, boiling water shrinkage is-1.5% at 87%, 160 dry-hot shrinkage when spending for elastic recovery rate.
Embodiment 2:
A kind of elastic fabric of polybutylene terephthalate (PBT) fiber, warp thread, the weft yarn of forming fabric all adopt the polybutylene terephthalate false-twisted yarn, and the polybutylene terephthalate fiber content accounts for 100% of total fabric weight; Or warp thread, weft yarn all adopt the mixed fiber yarn of polybutylene terephthalate false-twisted yarn and other fiber, and the polybutylene terephthalate fiber content accounts for 20~95% (examples 20%, 50%, 95%) of total fabric weight.
The tightness of fabric is 700-2000 (example 700,1300,2000).The filament number of polybutylene terephthalate fiber is 0.5~5.6dtex (routine 0.5dtex, 3dtex, 5.6dtex).The interlacing number of weft yarn is 0~80/meter (example 0,40,80), and the interlacing number of warp thread is 50~120/meter (examples 50,80,120).
Above-mentioned fabrics is put in order after dyeing with embodiment 1 same procedure, the spring rate of the fabric that obtains is in 15%~60% (example 15%, 35%, 60%), elastic recovery rate is in (example 80%, 90%, 95%) more than 80%, and 160 dry-hot shrinkages when spending are+1.0%~-3.0% with interior (example 1% ,-1% ,-3%), boiling water shrinkage+1.0%~-2.5% with interior (example 1% ,-1% ,-2.5%).
Comparative example 1
Warp thread:
1) several 100/meter of yarn: warp thread: 50D-72F-DTY (PET) interlacing
Weft yarn: several 80/meter of 150D-48F-PBT interlacing
2) fabric specification and weaving
Tissue: 2/1 twill
Density: through close * filling density=209*102 root/2.54cm
The warp-wise tightness: 2560, broadwise tightness: 1249
Mix rate: PET/PBT=41/59
Adopt 6 pieces along piercing into the capable weaving on air-jet loom of gaiting
3) the dyeing afterfinish method comprises the following steps:
A. concise: adopt the NaOH heat alkali liquid of 4% concentration and soaping agent (non-cationic type surfactant GQ008) to remove slurry, dirty and fabric is to a certain degree shunk.Temperature is 95 degree, and the processing time is 60 seconds
B. typing in the middle of: concise dried cloth is carried out the form stable treatment.Temperature is that 160 to spend the time be 60 seconds
C. dyeing processing: adopt under 120 degree and dye middle look, dyeing time is 30 minutes
D. resin finishing: above-mentioned cloth was handled 100 seconds under 140 degree with antistatic DEATRON and softener TF438
E. finished product typing: above-mentioned cloth is carried out last finished product typing, and the temperature of processing is 160 degree, and the processing time is 60 seconds.The finished product that obtains is 227*116 root/2.54cm through close * filling density, and the spring rate of fabric is 8%, and-4.0%, boiling water shrinkage is-3.5% at 75%, 160 dry-hot shrinkage when spending for elastic recovery rate.
Claims (6)
1. the elastic fabric of a polybutylene terephthalate (PBT) fiber is characterized in that: forming at least a in the warp thread of fabric or the weft yarn is the mixed fiber yarn of polybutylene terephthalate false-twisted yarn or polybutylene terephthalate false-twisted yarn and other fiber.
2. the elastic fabric of polybutylene terephthalate (PBT) fiber according to claim 1, it is characterized in that: the spring rate of fabric is 15%~60%, elastic recovery rate more than 80% and 160 dry-hot shrinkages when spending in+1.0%~-3.0%, boiling water shrinkage is in+1.0%~-2.5%.
3. the elastic fabric of polybutylene terephthalate (PBT) fiber according to claim 1 and 2 is characterized in that: the polybutylene terephthalate fiber content accounts for 20%~100% of total fabric weight.
4. the elastic fabric of polybutylene terephthalate (PBT) fiber according to claim 1 and 2 is characterized in that: the tightness of fabric is 700-2000.
5. the elastic fabric of polybutylene terephthalate (PBT) fiber according to claim 1 and 2 is characterized in that: the filament number of polybutylene terephthalate fiber is 0.5~5.6dtex.
6. the elastic fabric of polybutylene terephthalate (PBT) fiber according to claim 1 and 2 is characterized in that: the interlacing number of weft yarn is 0~80/meter, and the interlacing number of warp thread is 50~120/meter.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNA2006100976175A CN101177828A (en) | 2006-11-10 | 2006-11-10 | Polybutylene terephthalate fiber elastic fabric |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNA2006100976175A CN101177828A (en) | 2006-11-10 | 2006-11-10 | Polybutylene terephthalate fiber elastic fabric |
Publications (1)
Publication Number | Publication Date |
---|---|
CN101177828A true CN101177828A (en) | 2008-05-14 |
Family
ID=39404237
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNA2006100976175A Pending CN101177828A (en) | 2006-11-10 | 2006-11-10 | Polybutylene terephthalate fiber elastic fabric |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN101177828A (en) |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101748547A (en) * | 2008-12-17 | 2010-06-23 | 东丽纤维研究所(中国)有限公司 | Knitting machine imitated fabric and production method thereof |
CN102534928A (en) * | 2010-12-22 | 2012-07-04 | 东丽纤维研究所(中国)有限公司 | Elastic fabric and production method thereof |
CN102936790A (en) * | 2012-09-29 | 2013-02-20 | 浙江港龙织造科技有限公司 | Processing technology of multifunctional photocatalytic knitwear |
CN102936821A (en) * | 2012-09-29 | 2013-02-20 | 浙江港龙织造科技有限公司 | Photocatalyst fabric dyeing and finishing process |
CN102965790A (en) * | 2011-08-30 | 2013-03-13 | 东丽纤维研究所(中国)有限公司 | Light and thin fabric and production method thereof |
CN101994195B (en) * | 2009-08-21 | 2013-06-12 | 东丽纤维研究所(中国)有限公司 | Elastic fabric and production method thereof |
CN103298988A (en) * | 2010-12-22 | 2013-09-11 | 东丽株式会社 | Three-dimensionally shaped fabric |
CN103541138A (en) * | 2012-07-11 | 2014-01-29 | 东丽纤维研究所(中国)有限公司 | Ultra-soft textile and application thereof |
CN104233601A (en) * | 2013-06-14 | 2014-12-24 | 东丽纤维研究所(中国)有限公司 | Super-soft knitted fabric and processing method thereof |
CN109385726A (en) * | 2017-08-07 | 2019-02-26 | 中国石化仪征化纤有限责任公司 | A kind of preparation method of the blended short fine elastic fabric of PBT/PET |
-
2006
- 2006-11-10 CN CNA2006100976175A patent/CN101177828A/en active Pending
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101748547B (en) * | 2008-12-17 | 2012-12-26 | 东丽纤维研究所(中国)有限公司 | Knitting machine imitated fabric and production method thereof |
CN101748547A (en) * | 2008-12-17 | 2010-06-23 | 东丽纤维研究所(中国)有限公司 | Knitting machine imitated fabric and production method thereof |
CN101994195B (en) * | 2009-08-21 | 2013-06-12 | 东丽纤维研究所(中国)有限公司 | Elastic fabric and production method thereof |
CN102534928A (en) * | 2010-12-22 | 2012-07-04 | 东丽纤维研究所(中国)有限公司 | Elastic fabric and production method thereof |
CN102534928B (en) * | 2010-12-22 | 2015-04-29 | 东丽纤维研究所(中国)有限公司 | Elastic fabric and production method thereof |
CN103298988A (en) * | 2010-12-22 | 2013-09-11 | 东丽株式会社 | Three-dimensionally shaped fabric |
CN102965790B (en) * | 2011-08-30 | 2014-12-17 | 东丽纤维研究所(中国)有限公司 | Light and thin fabric and production method thereof |
CN102965790A (en) * | 2011-08-30 | 2013-03-13 | 东丽纤维研究所(中国)有限公司 | Light and thin fabric and production method thereof |
CN103541138A (en) * | 2012-07-11 | 2014-01-29 | 东丽纤维研究所(中国)有限公司 | Ultra-soft textile and application thereof |
CN102936821A (en) * | 2012-09-29 | 2013-02-20 | 浙江港龙织造科技有限公司 | Photocatalyst fabric dyeing and finishing process |
CN102936790B (en) * | 2012-09-29 | 2014-03-12 | 浙江港龙织造科技有限公司 | Processing technology of multifunctional photocatalytic knitwear |
CN102936821B (en) * | 2012-09-29 | 2015-04-08 | 浙江港龙织造科技有限公司 | Photocatalyst fabric dyeing and finishing process |
CN102936790A (en) * | 2012-09-29 | 2013-02-20 | 浙江港龙织造科技有限公司 | Processing technology of multifunctional photocatalytic knitwear |
CN104233601A (en) * | 2013-06-14 | 2014-12-24 | 东丽纤维研究所(中国)有限公司 | Super-soft knitted fabric and processing method thereof |
CN104233601B (en) * | 2013-06-14 | 2017-06-30 | 东丽纤维研究所(中国)有限公司 | A kind of super soft knitted fabric and its processing method |
CN109385726A (en) * | 2017-08-07 | 2019-02-26 | 中国石化仪征化纤有限责任公司 | A kind of preparation method of the blended short fine elastic fabric of PBT/PET |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101177828A (en) | Polybutylene terephthalate fiber elastic fabric | |
Choudhury | Principles of textile finishing | |
CN104878508A (en) | Cotton and natural silk napped fabric and method for processing same | |
CN1834320A (en) | Color fillet chamois leather suede fabric and preparation thereof | |
CN102181990B (en) | Heavy cotton viscose blended dual-elasticity yarn drill fabric and finishing process thereof | |
CN103255570B (en) | Warp-knitting elastic suede textile | |
CN105063852A (en) | Fabric containing Tencel A200 and cotton and processing method thereof | |
CN103147204A (en) | Thin woven fabric | |
CN107151855B (en) | The method for weaving of the big jacquard blanket fabric of all-cotton yarn-dyed multilayer | |
CN101387031A (en) | Natural fiber mixed fabric with flash effect and production method thereof | |
CN109403096B (en) | Terylene warp-knitted stripe fabric and production method thereof | |
CN109082768B (en) | Terylene warp-knitted plain fabric and production method thereof | |
CN100594267C (en) | Xiyurong clothing leather base cloth manufacturing method | |
CN101487156A (en) | Four-side elastic thin fabric and production method thereof | |
CN103422231B (en) | A kind of elastic corduroy fabric and production method thereof and application | |
CN101387033B (en) | Soft high density zonal elastic fabrics with heterochrosis effect | |
CN107881621A (en) | One kind, which is relaxed, plays Crinkled face fabric | |
CN109112705B (en) | Terylene warp-knitted check fabric and production method thereof | |
CN104611873A (en) | Dyeing and finishing processing method for improving distortion of polyester cotton natural elastic twill fabric | |
CN107475852A (en) | A kind of hollow-out fabric and its production method | |
CN107287908A (en) | The weft yarn kiering colouring method of the big jacquard blanket fabric of all-cotton yarn-dyed multilayer | |
KR100826223B1 (en) | Velvet textile and the manufacture method | |
CN211227563U (en) | Bead ground diamond-shaped grid sweater terry fabric | |
CN104664639A (en) | Pure hemp knitted underwear material without scratchiness and processing method thereof | |
JP3172230U (en) | Stretch fabric |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C12 | Rejection of a patent application after its publication | ||
RJ01 | Rejection of invention patent application after publication |
Open date: 20080514 |