CN101133008B - 从1,1,1,3,3,3-六氟丙烷非催化法生产1,1,3,3,3-五氟丙烯 - Google Patents

从1,1,1,3,3,3-六氟丙烷非催化法生产1,1,3,3,3-五氟丙烯 Download PDF

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Publication number
CN101133008B
CN101133008B CN2005800375571A CN200580037557A CN101133008B CN 101133008 B CN101133008 B CN 101133008B CN 2005800375571 A CN2005800375571 A CN 2005800375571A CN 200580037557 A CN200580037557 A CN 200580037557A CN 101133008 B CN101133008 B CN 101133008B
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China
Prior art keywords
pyrolysis
reactor
reaction zone
temperature
reaction
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Expired - Fee Related
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CN2005800375571A
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English (en)
Chinese (zh)
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CN101133008A (zh
Inventor
V·N·M·劳
A·C·西弗特
R·N·米勒
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EIDP Inc
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EI Du Pont de Nemours and Co
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C01B7/191—Hydrogen fluoride
    • C01B7/195—Separation; Purification
    • C01B7/196—Separation; Purification by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN2005800375571A 2004-10-29 2005-10-28 从1,1,1,3,3,3-六氟丙烷非催化法生产1,1,3,3,3-五氟丙烯 Expired - Fee Related CN101133008B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US62321004P 2004-10-29 2004-10-29
US60/623,210 2004-10-29
PCT/US2005/039169 WO2006050215A2 (en) 2004-10-29 2005-10-28 Non-catalytic manufacture of 1,1,3,3,3-pentafluoropropene from 1,1,1,3,3,3-hexafluoropropane

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN201010143775A Division CN101792365A (zh) 2004-10-29 2005-10-28 共沸或共沸类组合物、分离氟化氢的方法和分离1,1,3,3,3-五氟丙烯的方法

Publications (2)

Publication Number Publication Date
CN101133008A CN101133008A (zh) 2008-02-27
CN101133008B true CN101133008B (zh) 2011-11-23

Family

ID=36319717

Family Applications (2)

Application Number Title Priority Date Filing Date
CN2005800375571A Expired - Fee Related CN101133008B (zh) 2004-10-29 2005-10-28 从1,1,1,3,3,3-六氟丙烷非催化法生产1,1,3,3,3-五氟丙烯
CN201010143775A Pending CN101792365A (zh) 2004-10-29 2005-10-28 共沸或共沸类组合物、分离氟化氢的方法和分离1,1,3,3,3-五氟丙烯的方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN201010143775A Pending CN101792365A (zh) 2004-10-29 2005-10-28 共沸或共沸类组合物、分离氟化氢的方法和分离1,1,3,3,3-五氟丙烯的方法

Country Status (5)

Country Link
US (1) US20060094911A1 (https=)
EP (1) EP1805124A2 (https=)
JP (1) JP2008518938A (https=)
CN (2) CN101133008B (https=)
WO (1) WO2006050215A2 (https=)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7388117B2 (en) * 2005-11-01 2008-06-17 E.I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,2,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
US7476771B2 (en) * 2005-11-01 2009-01-13 E.I. Du Pont De Nemours + Company Azeotrope compositions comprising 2,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
MY151990A (en) 2005-11-01 2014-07-31 Du Pont Solvent compositions comprising unsaturated fluorinated hydrocarbons
MY160614A (en) * 2006-02-28 2017-03-15 Du Pont Azeotropic compositions comprising fluorinated compounds for cleaning applications
US8377327B2 (en) * 2006-06-27 2013-02-19 E I Du Pont De Nemours And Company Tetrafluoropropene production processes
US7833434B2 (en) * 2006-06-27 2010-11-16 E. I. Du Pont De Nemours And Company Tetrafluoropropene production processes
US7803975B2 (en) * 2006-07-13 2010-09-28 E.I. Du Pont De Nemours And Company Process for separating a fluoroolefin from HF by liquid-liquid extraction
GB0614927D0 (en) * 2006-07-27 2006-09-06 Ineos Fluor Holdings Ltd Separation process
JP5439177B2 (ja) * 2006-08-24 2014-03-12 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 共沸蒸留によってフッ化水素からフルオロオレフィンを分離する方法
CN101535223A (zh) * 2006-09-05 2009-09-16 纳幕尔杜邦公司 用于制备氟烃的纯化工艺和方法
US8007677B2 (en) 2006-09-08 2011-08-30 E.I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,1,1,2,3-pentafluoropropene and hydrogen fluoride and uses thereof
JP5416587B2 (ja) 2006-10-03 2014-02-12 メキシケム、アマンコ、ホールディング、ソシエダッド、アノニマ、デ、カピタル、バリアブレ プロセス
US7981312B2 (en) * 2006-10-31 2011-07-19 E. I. Du Pont De Nemours And Company Processes for producing and compositions comprising 2,3,3,3-tetrafluoropropene and/or 1,2,3,3-tetrafluoropropene
CN103483140B (zh) * 2006-10-31 2015-09-09 纳幕尔杜邦公司 氟丙烷、卤代丙烯以及2-氯-3,3,3-三氟-1-丙烯与hf的共沸组合物和1,1,1,2,2-五氟丙烷与hf的共沸组合物的制备方法
TW200844075A (en) * 2006-10-31 2008-11-16 Du Pont Processes for the production of fluoropropanes and halopropenes
GB0625214D0 (en) * 2006-12-19 2007-01-24 Ineos Fluor Holdings Ltd Process
US8101672B2 (en) * 2007-12-13 2012-01-24 Honeywell International Inc. Azeotrope-like compositions of 1,1,2,3,3-pentafluoropropene
ES2483995T3 (es) * 2008-02-21 2014-08-08 E. I. Du Pont De Nemours And Company Procesos para la separación de 1,3,3,3-tetrafluoropropeno del fluoruro de hidrógeno por medio de destilación azeotrópica
US8203022B2 (en) * 2008-10-27 2012-06-19 E I Du Pont De Nemours And Company Conversion of 2-chloro-1,1,1,2-tetrafluoropropane to 2,3,3,3-tetrafluoropropene
RU2011121361A (ru) * 2008-10-27 2012-12-10 Е.И.Дюпон Де Немур Энд Компани Превращение гидрофторхлорпропанов в фторпропены
US8697922B2 (en) 2008-10-27 2014-04-15 E I Du Pont De Nemours And Company Conversion of 2-chloro-1,1,1,2-tetrafluoropropane to 2,3,3,3-tetrafluoropropene
US20110215273A1 (en) * 2008-11-13 2011-09-08 Solvay Fluor Gmbh Hydrofluoroolefins, manufacture of hydrofluoroolefins and methods of using hydrofluoroolefins
CN110845295A (zh) * 2014-08-14 2020-02-28 科慕埃弗西有限公司 通过脱氟化氢来制备E-1，3，3，3-四氟丙烯(HFC-1234ze)的方法
EP3392229A4 (en) * 2015-12-16 2019-08-07 AGC Inc. PROCESS FOR PREPARING HYDROFLUOROLEFIN
WO2019051390A1 (en) * 2017-09-11 2019-03-14 The Chemours Company, Fc, Llc AZEOTROPIC COMPOSITIONS COMPRISING HYDROGEN FLUORIDE AND FLUOROCARBONS
WO2021049605A1 (ja) * 2019-09-12 2021-03-18 関東電化工業株式会社 ＝ｃｆ２もしくは＝ｃｈｆの構造を持つフルオロオレフィンの精製方法、並びに高純度フルオロオレフィン及びその製造方法
TW202430495A (zh) 2022-10-03 2024-08-01 日商關東電化工業股份有限公司 氟烯烴之製造方法
CN116003210A (zh) * 2022-11-30 2023-04-25 三明市海斯福化工有限责任公司 一种偏氟乙烯单体的制备方法及偏氟乙烯单体

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3397248A (en) * 1964-05-15 1968-08-13 Du Pont Process for the preparation of hexafluoropropene
DE1965977A1 (de) * 1968-12-28 1971-01-28 Bitterfeld Chemie Vorrichtung zur Durchfuehrung von thermischen Reaktionen
JPH0967281A (ja) * 1995-09-01 1997-03-11 Daikin Ind Ltd １，１，１，３，３−ペンタフルオロプロペンの製造方法及び１，１，１，３，３−ペンタフルオロプロパンの製造方法
US5945573A (en) * 1997-01-31 1999-08-31 E. I. Du Pont De Nemours And Company Process for the manufacture of 1,1,1,3,3-pentafluoropropane
US6369284B1 (en) * 1997-01-31 2002-04-09 E. I. Du Pont De Nemours And Company Catalytic manufacture of pentafluoropropenes
US6376727B1 (en) * 1997-06-16 2002-04-23 E. I. Du Pont De Nemours And Company Processes for the manufacture of 1,1,1,3,3-pentafluoropropene, 2-chloro-pentafluoropropene and compositions comprising saturated derivatives thereof
US6031141A (en) * 1997-08-25 2000-02-29 E. I. Du Pont De Nemours And Company Fluoroolefin manufacturing process
US6583328B1 (en) * 1999-04-05 2003-06-24 Pcbu Services, Inc. Method for the preparation of 1,1,1,3,3-pentafluoropropene and 1,1,1,3,3-pentafluoropropane
US6703533B1 (en) * 1999-08-20 2004-03-09 E. I. Du Pont De Nemours And Company Preparation of selected fluoroolefins
US20020032356A1 (en) * 2000-07-14 2002-03-14 Gelblum Peter Gideon Synthesis of perfluoroolefins

Also Published As

Publication number Publication date
US20060094911A1 (en) 2006-05-04
WO2006050215A3 (en) 2007-05-18
EP1805124A2 (en) 2007-07-11
WO2006050215A2 (en) 2006-05-11
JP2008518938A (ja) 2008-06-05
CN101792365A (zh) 2010-08-04
CN101133008A (zh) 2008-02-27

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Granted publication date: 20111123

Termination date: 20131028