CN101129313B - Liquid shampoo for nourishing hair and preventing break and phalacrosis - Google Patents

Liquid shampoo for nourishing hair and preventing break and phalacrosis Download PDF

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Publication number
CN101129313B
CN101129313B CN200710049875A CN200710049875A CN101129313B CN 101129313 B CN101129313 B CN 101129313B CN 200710049875 A CN200710049875 A CN 200710049875A CN 200710049875 A CN200710049875 A CN 200710049875A CN 101129313 B CN101129313 B CN 101129313B
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parts
shampoo
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hair
avulsion
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CN101129313A (en
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姜家东
万岳鹏
蒋青
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Guangzhou Houdy Group Co., Ltd.
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GUANGZHOU HOUDY COSMETICESCO CO Ltd
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Abstract

Disclosed is a hair washing liquid for nourishing hair, wherein the constituents include (by weight percent) medicinal herbs extract 10-30%, keratin 2-10%, surface active agent 13-20. 5%, smoothing conditioner 4. 2-7. 5%, acid-alkali conditioning agent 0. 3-1. 5%, deionized water 32-65%. The medicinal herbs comprises the constituents of (by weight ratio) tuber of multiflower knotweed 15-30 parts,Chinese angelica root 15-30 parts, astragalus root 15-30 parts, arborvitae tops 10-30 parts, sesame seed 10-30 parts, ligustrum japonicum 10-30 parts, ginseng 10-30 parts and wild pepper 15-30 parts.

Description

The shampoo of nourishing hair and anti-breaking anti-avulsion
Technical field
The invention belongs to the shampoo field, particularly a kind of shampoo that hair is had trophic function and anti-breaking anti-avulsion function.
Background technology
The lifting of the quality of the life that is accompanied by economic development and comes, everybody wishes to have health, beautiful hair.Yet alopecia occurs at each age group, and according to interrelated data, the sickness rate of all types of alopecias is about about 4%.Modal in the alopecia is seborrheic alopecia, and its main cause is the head exdermoptosis, and sebum secretion is vigorous, and is excessive in a large number, and the follicular orifice hyperkeratosis forms thromboembolism, influences the nutrition of hair follicle, makes hair follicle atrophy breaking-up gradually, and hair is tapered and becomes fragile to coming off.Because hair lengths increases, and its hair scale sheet cell partly comes off, hair compliance variation is easy to distortion in addition, causes hairs break very easily takes place in combing and washing process to come off.
For nourishing hair, anti-loss, people explore the prescription of shampoo, have worked out multiple hair is had trophic function and can prevent the shampoo of alopecia, broken hair, but the prescription difference of various shampoos, and effect is difference to some extent also.Application number is that the Chinese patent application of 01106997.X discloses a kind of anti-avulsion, hair growth promoting, black hair, hair care, dandruff-controlling shampoo, and its prescription is: Fructus Gleditsia 40-60 gram; Radix Polygoni Multiflori 20-25 gram; Radix Angelicae Sinensis 20-45 gram; Radix Rehmanniae 15-35 gram; Radix Rehmanniae Preparata 15-35 gram; Semen sojae atricolor 40-65 gram; Fructus Cnidii 10-25 gram; Radix Astragali 10-25 gram; Radix Aucklandiae 10-25 gram; Olibanum 10-25 gram; Myrrha 10-25 gram; Rhizoma Chuanxiong 10-30 gram; Poria 5-15 gram; Radix Glycyrrhizae 3-10 gram.Application number is that 200410088762.8 Chinese patent application discloses a kind of natural hair tonic and trichomadesis proof hair lotion, the mass percent of its component and each component is: Folium Japanse Galangal powder 5-6%, light flour 6-8%, Oleum Sesami 0.4-0.5%, Alpinia japonica (Thunb.) Miq. oil 0.1-0.2%, IES 5-8%, Sal 1-2%, triumphant loose 0.1-0.3%, essence 0.5-1.5%, Cera Flava 8-10%, medicated wine 65-70%.
Summary of the invention
The object of the present invention is to provide the shampoo of a kind of nourishing hair and anti-breaking anti-avulsion, to satisfy the demand that people have health, beautiful hair.
Technical scheme of the present invention: the prescription of the design shampoo of starting with from two aspects.The one, root of hair and scalp are adopted blood circulation promoting and blood stasis dispelling because of the malnutrition that the hair follicle obstruction causes, beneficial blood spermatogenesis presses down enhancing scalp nutrition such as fat sterilization, and hair growing is anti-loss, for this reason, has been equipped with medicinal plant extract in the prescription of shampoo; The 2nd, impaired at hair structure, utilize the reaction of hair keratin tissue, in conjunction with new albumen tissue, realize reparation to impaired hair quality, strengthen hair quality sword and intensity, prevent the broken hair alopecia, for this reason, in the prescription of shampoo, be equipped with keratin.
The shampoo of nourishing hair of the present invention and anti-breaking anti-avulsion, the mass percent of its contained component and each component is as follows:
Medicinal plant extract 10%~30%,
Keratin 2%~10%,
Surfactant 13%~20.5%,
Submissive conditioner 4.2%~7.5%,
Acid-base modifier 0.3%~1.5%,
Deionized water 32%~65%;
Described medicinal plant extract is that medicinal plants is pulverized, and under room temperature (indoor natural temperature), normal pressure is that extractant lixiviate or circulation are extracted the extracting solution that obtains and concentrated and form with ethanol, and the component that medicinal plants contains and the mass parts of each component are as follows:
15~30 parts of the Radixs Polygoni Multiflori, 15~30 parts of Radix Angelicae Sinensis, 15~30 parts of the Radixs Astragali, 10~30 parts of Cacumen Platycladis,
10~30 parts of Semen Sesami Nigrums, Fructus Ligustri Lucidi 10-30 part, 10~30 parts of Radix Ginsengs, 15~30 parts in Pericarpium Zanthoxyli.
In order better to promote the scalp blood circulation, suppress the head sebum secretion, strengthen scalp nutrition, can in the component of medicinal plants, increase a kind of in Rhizoma Zingiberis Recens, Flos Carthami, Semen Juglandis, the Flos Chrysanthemi at least, each component by mass, the content of Rhizoma Zingiberis Recens<15 part, the content of Flos Carthami<30 part, the content of Semen Juglandis<20 part, the content of Flos Chrysanthemi<25 part.
In order to make shampoo have antiseptic property and fragrant odour, salubrious, can in the shampoo component, increase essence and antiseptic, the mass percent of essence is 0.2%~1.0%, the mass percent of antiseptic is 0.05%~0.1%.
In the shampoo of the present invention, surfactant is at least a kind of in lauryl alcohol ammonium sulfate (70%), glycol stearate, the coconut oil alkylamide.
In the shampoo of the present invention, submissive conditioner is at least a kind of in emulsified silicone oil (50%), polyquaternary ammonium salt-10, the octadecanol.
In the shampoo of the present invention, the soda acid mediator agent is made up of citric acid and sodium citrate, and the mass ratio of citric acid and sodium citrate is 1: 2~1: 3.
The preparation method of shampoo of the present invention: each component of shampoo that measures is put into the container of belt stirrer, under agitation be heated to 60~80 ℃, after each component is all dissolved, be cooled to room temperature and be shampoo of the present invention in normal pressure.If comprise essence in the component, then all dissolve postcooling to 40~50 and ℃ add essence and stir in each component, be cooled to room temperature then.
The present invention has following beneficial effect:
1, contain medicinal plant extract in the shampoo of the present invention, experiment shows, can moisten scalp, and expansion scalp blood capillary promotes the scalp blood circulation, suppresses the head sebum secretion, activates melanocyte, strengthens scalp nutrition, and hair growing is anti-loss.
2, contain keratin in the shampoo of the present invention, the keratin on itself and hair fiber surface reacts to each other, and is attached to the hair fiber surface, makes the hair scale sheet cellularity on hair fiber surface complete, the hair fiber smooth surface; Owing to macromole keratin on the hair fiber surface combination, help to keep the moisture of hair fiber simultaneously with moist; In addition, the cystine in the keratin can combine with keratin in the hair fiber by disulfide bond, increases the intensity of hair, thereby significantly reduces the broken hair in washing and combing hair process and the alopecia that causes, and makes hair submissive moist.
3, through check, shampoo of the present invention meets sanitary index, and concrete data see the following form:
Figure G2007100498750D00031
The specific embodiment
Embodiment 1
1, the preparation of medicinal plant extract
(1) batching
The component of medicinal plants and the mass parts of each component are: 15 parts of the Radixs Polygoni Multiflori, 15 parts of Radix Angelicae Sinensis, 15 parts of the Radixs Astragali, 10 parts of Cacumen Platycladis, 10 parts of Semen Sesami Nigrums, 10 parts of Fructus Ligustri Lucidi, 10 parts of Radix Ginsengs, 15 parts in Pericarpium Zanthoxyli.
(2) circulation is extracted
To put into Soxhlet extractor after the medicinal plants pulverizing, under room temperature (20 ℃), normal pressure be that the extractant circulation is extracted with ethanol, the extracting solution that obtained adopts distillation to concentrate, and distills the spissated time to volatilize fully with ethanol and exceed, and distills spissated product and is medicinal plant extract.
2, the preparation of shampoo
(1) batching
The component of shampoo and the mass percent of each component are as follows:
The medicinal extract 15.5% of step 1 preparation, procom keratin 2%, surfactant: lauryl alcohol ammonium sulfate (70%) 12%, glycol stearate 0.5%, coconut oil alkylamide 0.5%, submissive conditioner: emulsified silicone oil (50%) 4%, polyquaternary ammonium salt-100.2%, acid-base modifier: citric acid 0.1%, sodium citrate 0.2%, deionized water 65%.
(2) dissolving and fill
Each component of shampoo that measures is put into the container of belt stirrer, under agitation be heated to 80 ℃, after each component is all dissolved, be cooled to room temperature and be filled into bottle in normal pressure.
Embodiment 2
1, the preparation of medicinal plant extract
(1) batching
The component of medicinal plants and the mass parts of each component are: 30 parts of the Radixs Polygoni Multiflori, 30 parts of Radix Angelicae Sinensis, 30 parts of the Radixs Astragali, 30 parts of Cacumen Platycladis, 30 parts of Semen Sesami Nigrums, 30 parts of Fructus Ligustri Lucidi, 30 parts of Radix Ginsengs, 30 parts in Pericarpium Zanthoxyli.
(2) circulation is extracted
To put into Soxhlet extractor after the medicinal plants pulverizing, under room temperature (24 ℃), normal pressure be that the extractant circulation is extracted with ethanol, the extracting solution that obtained adopts distillation to concentrate, and distills the spissated time to volatilize fully with ethanol and exceed, and distills spissated product and is medicinal plant extract.
2, the preparation of shampoo
(1) batching
The component of shampoo and the mass percent of each component are as follows:
The medicinal extract 10% of step 1 preparation, procom keratin 6.5%, surfactant: lauryl alcohol ammonium sulfate (70%) 16%, glycol stearate 2.0%, coconut oil alkylamide 2.5%, submissive conditioner: emulsified silicone oil (50%) 5.0%, octadecanol 1.5%, polyquaternary ammonium salt-10 1.0%, acid-base modifier: citric acid 0.4%, sodium citrate 1.1%, deionized water 54%.
(2) dissolving and fill
Each component of shampoo that measures is put into the container of belt stirrer, under agitation be heated to 70 ℃, after each component is all dissolved, be cooled to room temperature and be filled into bottle in normal pressure.
Embodiment 3
1, the preparation of medicinal plant extract
(1) batching
The component of medicinal plants and the mass parts of each component are: 20 parts of the Radixs Polygoni Multiflori, 24 parts of Radix Angelicae Sinensis, 18 parts of the Radixs Astragali, 15 parts of Cacumen Platycladis, 15 parts of Semen Sesami Nigrums, 20 parts of Fructus Ligustri Lucidi, 12 parts of Radix Ginsengs, 20 parts in Pericarpium Zanthoxyli.
(2) circulation is extracted
To put into Soxhlet extractor after the medicinal plants pulverizing, under room temperature (25 ℃), normal pressure be that the extractant circulation is extracted with ethanol, the extracting solution that obtained adopts distillation to concentrate, and distills the spissated time to volatilize fully with ethanol and exceed, and distills spissated product and is medicinal plant extract.
2, the preparation of shampoo
(1) batching
The component of shampoo and the mass percent of each component are as follows:
The medicinal extract 20% of step 1 preparation, procom keratin 8.2%, surfactant: lauryl alcohol ammonium sulfate (70%) 14.5%, glycol stearate 2.0%, submissive conditioner: emulsified silicone oil (50%) 5.5%, octadecanol 0.8%, acid-base modifier: citric acid 0.3%, sodium citrate 0.7%, deionized water 48%.
(2) dissolving and fill
Each component of shampoo that measures is put into the container of belt stirrer, under agitation be heated to 70 ℃, after each component is all dissolved, be cooled to room temperature and be filled into bottle in normal pressure.
Embodiment 4
1, the preparation of medicinal plant extract
(1) batching
The component of medicinal plants and the mass parts of each component are: 15 parts of the Radixs Polygoni Multiflori, 20 parts of Radix Angelicae Sinensis, 20 parts of the Radixs Astragali, 18 parts of Cacumen Platycladis, 20 parts of Semen Sesami Nigrums, 16 parts of Fructus Ligustri Lucidi, 14 parts of Radix Ginsengs, 15 parts in Pericarpium Zanthoxyli, 6 parts in Rhizoma Zingiberis Recens, 10 parts on Flos Carthami.
(2) lixiviate
Put into after medicinal plants pulverized and alcoholic acid container is housed under room temperature (28 ℃), normal pressure, soaks, alcoholic acid amount is flooded medicinal plants and is got final product, soak time is 1.0 hours, soak and finish to obtain after filtration extracting solution, filtering residue is repeated aforementioned operation twice, merge each time extracting solution obtained and adopt distillation concentrated, distilling the spissated time volatilizees fully with ethanol and exceeds, and distills spissated product and is medicinal plant extract.
2, the preparation of shampoo
(1) batching
The component of shampoo and the mass percent of each component are as follows:
The medicinal extract 30% of step 1 preparation, procom keratin 6%, surfactant: lauryl alcohol ammonium sulfate (70%) 15%, coconut oil alkylamide 2.0%, submissive conditioner: emulsified silicone oil (50%) 6.5%, acid-base modifier: citric acid 0.2%, sodium citrate 0.6%, deionized water 38.82%, essence 0.8%, antiseptic 0.08%.
(2) dissolving and fill
Each component of the shampoo except that essence that measures is put into the container of belt stirrer, under agitation be heated to 60 ℃, after each component is all dissolved, be cooled to 45 ℃ and add essence and stir, be cooled to room temperature then and be filled into bottle in normal pressure.
Embodiment 5
1, the preparation of medicinal plant extract
(1) batching
The component of medicinal plants and the mass parts of each component are: 24 parts of the Radixs Polygoni Multiflori, 16 parts of Radix Angelicae Sinensis, 22 parts of the Radixs Astragali, 14 parts of Cacumen Platycladis, 22 parts of Semen Sesami Nigrums, 18 parts of Fructus Ligustri Lucidi, 18 parts of Radix Ginsengs, 24 parts in Pericarpium Zanthoxyli, 10 parts in Rhizoma Zingiberis Recens, 16 parts on Flos Carthami, 12 parts of Semen Juglandis, 8 parts of Flos Chrysanthemis.
(2) lixiviate
Put into after medicinal plants pulverized and alcoholic acid container is housed under room temperature (28 ℃), normal pressure, soaks, alcoholic acid amount is flooded medicinal plants and is got final product, soak time is 0.5 hour, soak and finish to obtain after filtration extracting solution, filtering residue is repeated aforementioned operation twice, merge each time extracting solution obtained and adopt distillation concentrated, distilling the spissated time volatilizees fully with ethanol and exceeds, and distills spissated product and is medicinal plant extract.
2, the preparation of shampoo
(1) batching
The component of shampoo and the mass percent of each component are as follows:
The medicinal extract 28% of step 1 preparation, procom keratin 10%, surfactant: lauryl alcohol ammonium sulfate (70%) 20%; Submissive conditioner: emulsified silicone oil (50%) 6.4%, polyquaternary ammonium salt-101.0%, acid-base modifier: citric acid 0.4%, sodium citrate 1.1%, deionized water 32%, essence 1.0%, antiseptic 0.1%.
(2) dissolving and fill
Each component of the shampoo except that essence that measures is put into the container of belt stirrer, under agitation be heated to 60 ℃, after each component is all dissolved, be cooled to 40 ℃ and add essence and stir, be cooled to room temperature then and be filled into bottle in normal pressure.
Embodiment 6
1, the effect of medicinal plant extract experiment
(1) preparation of medicinal plant extract
A, batching
The component of medicinal plants and the mass parts of each component are: 15 parts of the Radixs Polygoni Multiflori, 15 parts of Radix Angelicae Sinensis, 15 parts of the Radixs Astragali, 10 parts of Cacumen Platycladis, 10 parts of Semen Sesami Nigrums, 10 parts of Fructus Ligustri Lucidi, 10 parts of Radix Ginsengs, 15 parts in Pericarpium Zanthoxyli.
B, circulation are extracted
To put into Soxhlet extractor after the medicinal plants pulverizing, under room temperature (20 ℃), normal pressure be that the extractant circulation is extracted with ethanol, the extracting solution that obtained adopts distillation to concentrate, and distills the spissated time to volatilize fully with ethanol and exceed, and distills spissated product and is medicinal plant extract.
C, preparation experimental drug liquid
The medicinal plant extract of step B preparation is mixed with three kinds of medicinal liquids of mass concentration 5%, 10%, 30% respectively with deionized water.
(2) animal subject and experimental implementation
Animal subject is a nude mice, totally 20, is divided into 4 test group, every group of 5 nude mices.The 1st group is matched group, and the 2nd group, the 3rd group, the 4th group is experimental group.
Matched group: with deionized water 5 nude mice epidermises are rubbed wiping once a day, each 5 minutes, continue 20 days.
Test 1 group: with the plant extract medicinal liquid of mass concentration 5% 5 nude mice epidermises are rubbed wiping once a day, each 5 minutes, continue 20 days.
Test 2 groups: with the plant extract medicinal liquid of mass concentration 10% 5 nude mice epidermises are rubbed wiping once a day, each 5 minutes, continue 20 days.
Test 3 groups: with the plant extract medicinal liquid of mass concentration 30% 5 nude mice epidermises are rubbed wiping once a day, each 5 minutes, continue 20 days.
(3) experimental result
Experimental result sees the following form:
Group name Nude mice epidermis hair amplification degree
Matched group 0.0%
Test 1 group 4.6%
Test 2 groups 10.7%
Test 3 groups 26.8%
Experimental result shows that 10%, 30% pair of the mass concentration of medicinal plant extract promotes the nude mice hair growth that obvious effects is arranged.
2, the effect of shampoo experiment
Use the shampoo and the basic shampoo of embodiment 1 preparation to carry out the effect experiment.
The component of the shampoo of embodiment 1 preparation and the mass percent of each component are as follows:
The medicinal extract 15.5% of step 1 preparation, procom keratin 2%, surfactant: lauryl alcohol ammonium sulfate (70%) 12%, glycol stearate 0.5%, coconut oil alkylamide 0.5%, submissive conditioner: emulsified silicone oil (50%) 4%, polyquaternary ammonium salt-100.2%, acid-base modifier: citric acid 0.1%, sodium citrate 0.2%, deionized water 65%.
The basis shampoo is meant and does not contain medicinal plant extract and keratic shampoo that the component of basic shampoo and the mass percent of each component are as follows:
Surfactant: lauryl alcohol ammonium sulfate (70%) 12%, glycol stearate 0.5%, coconut oil alkylamide 0.5%, submissive conditioner: emulsified silicone oil (50%) 4%, polyquaternary ammonium salt-100.2%, acid-base modifier: citric acid 0.1%, sodium citrate 0.2%, deionized water 82.5%.
(1) shampoo with 3 gram embodiment, 1 preparation is applied to the identical hair sample (Aisan's hair) of 3 grams respectively with the basic shampoo of 3 grams, then respectively with 40 ℃ of lasting current flushings 2 minutes, wet comb 10 times, the wet comb power that hair respectively restrainted in record, calculating mean value.Compare with the same hair of using basic shampoo, use the hair of shampoo of the present invention, its wet comb power reduces by 45%~60%.
(2) shampoos and the basic shampoos of 3 grams with 3 gram embodiment 1 preparations are applied to the identical topknot of 3 grams respectively, washed 2 minutes with 40 ℃ of lasting current respectively then, behind each topknot natural drying, place constant temperature, constant humidity laboratory (20 ℃, 60RH).Compare with the hair of using basic shampoo group, the hair soft degree of using shampoo of the present invention strengthens 50%~70%.
(3) shampoo with 3 gram embodiment, 1 preparation is applied to the identical topknot of 3 grams respectively with the basic shampoo of 3 grams, washed 2 minutes with 40 ℃ of lasting current respectively then, each topknot after the flushing is placed under the artificial ultraviolet light shine 30 minutes (being equivalent to 125 hours outdoor sunlight strengths).Repeat behind aforesaid operations 50 hairs of picked at random from each topknot again, measure every hair and prolong 20% energy requirement, calculate average energy.Compare with using basic shampoo group, the hair intensity of using shampoo of the present invention is significantly increased, and hair fiber tension force increases by 15%~30%.

Claims (5)

1. the shampoo of a nourishing hair and anti-breaking anti-avulsion is characterized in that component comprises medicinal plant extract, keratin, surfactant, submissive conditioner, acid-base modifier, deionized water, and the mass percent of each component is as follows:
Medicinal plant extract 10%~30%,
Keratin 2%~10%,
Surfactant 13%~20.5%,
Submissive conditioner 4.2%~7.5%,
Acid-base modifier 0.3%~1.5%,
Deionized water 32%~65%;
Described medicinal plant extract is that medicinal plants is pulverized, under the room temperature normal pressure be that the extractant circulation is extracted the extracting solution distillation that obtains and concentrated and form with ethanol, the spissated time volatilizees fully with ethanol and exceeds, and the component that medicinal plants contains and the mass parts of each component are as follows:
15~30 parts of the Radixs Polygoni Multiflori, 15~30 parts of Radix Angelicae Sinensis, 15~30 parts of the Radixs Astragali, 10~30 parts of Cacumen Platycladis,
10~30 parts of Semen Sesami Nigrums, 10~30 parts of Fructus Ligustri Lucidi, 10~30 parts of Radix Ginsengs, 15~30 parts in Pericarpium Zanthoxyli.
2. the shampoo of nourishing hair according to claim 1 and anti-breaking anti-avulsion is characterized in that also comprising essence and antiseptic, and the mass percent of essence is 0.2%~1.0%, and the mass percent of antiseptic is 0.05%~0.1%.
3. the shampoo of nourishing hair according to claim 1 and 2 and anti-breaking anti-avulsion is characterized in that surfactant is at least a kind of in lauryl alcohol ammonium sulfate, glycol stearate, the coconut oil alkylamide.
4. the shampoo of nourishing hair according to claim 3 and anti-breaking anti-avulsion is characterized in that submissive conditioner is at least a kind of in emulsified silicone oil, polyquaternary ammonium salt-10, the octadecanol.
5. the shampoo of nourishing hair according to claim 4 and anti-breaking anti-avulsion is characterized in that acid-base modifier is made up of citric acid and sodium citrate, and the mass ratio of citric acid and sodium citrate is 1: 2~1: 3.
CN200710049875A 2007-08-30 2007-08-30 Liquid shampoo for nourishing hair and preventing break and phalacrosis Active CN101129313B (en)

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