CN101063279A - Mushroom fruiting body cellulose - Google Patents

Abstract

The invention relates to a mushroom seed cellulose, characterized in that treating the mushroom seed via acid, alkali and pure water for several times to remove the materials beside the cellulose to obtain pure mushroom seed cellulose. And the invention has the advantages that it is not easy to go mouldy, the cellulose is beta glucose type, which is stable without reaction with other materials, to obtains safety and zero heating amount. The invention is applied for batch production, with simple method, confirmed quality, high efficiency, low cost and wide application. And the mushroom seed cellulose can improve the people immunity via macrophage and exciting antibody, to be used as the material of health-care product and drug.

Description

A kind of mushroom fruiting body cellulose

Technical field

The present invention relates to a kind of mushroom fruiting body cellulose, relate in particular to a kind of mushroom fruiting body cellulose, belong to the cellulose technology field with the health products development of raw materials.

Background technology

Cellulose resource mainly obtains from plants such as cereal, beans, vegetables, fruit at present, and does not extract from the fructification mushroom of Mycophyta.

Summary of the invention

The purpose of this invention is to provide a kind of a kind of mushroom fruiting body cellulose that from the fructification mushroom of Mycophyta, extracts.

For realizing above purpose, technical scheme of the present invention provides a kind of mushroom fruiting body cellulose, it is characterized in that, repeatedly handles through soda acid and pure water from mushroom fruiting body or powder and removes the various materials beyond the cellulose and obtain simple mycelia cellulose.

A kind of extracting method of mushroom fruiting body cellulose is extracted from the mushroom powder, the steps include:

The first step. take by weighing behind crushing screening＜100 purpose mushrooms pulverize material and add 1 for 1 part: 10-50 times of 0.5-3 molar sodium hydroxide, soaks after 1-3 hour, stirred 2-5 hour with dissolution kettle, stop stirring, static layering is isolated with centrifuge and to be the dark-brown mother liquor; Mushroom materials slag input washing still carries out the running water washing, and PH separates to neutral back, delivers to centrifuge and will expect that slag drains;

Second step. add 1 again: 10-50 part 0.5-3 mole hydrochloride stirred 2-5 hour, stopped to stir, and static layering is isolated and is the light green mother liquor; Property among the mushroom residue is washed, separate the back, and the material slag drains;

The 3rd step. add 1 again: 10-50 part 0.5-3 molar sodium hydroxide stirred 2-5 hour, stopped to stir, and static layering is isolated band light brown mother liquor;

The 4th step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till PH for neutral, change the pure water washing once, the static layering filter residue drains;

The 5th step. with carrying out vacuum freeze drying after the freeze drier pre-freeze; Obtain dried cellulose, sieve once more the mushroom cellulose.

A kind of extracting method of mushroom fruiting body cellulose is characterized in that, repeatedly handles through soda acid and pure water from mushroom fruiting body and removes the various materials beyond the cellulose and obtain simple mushroom cellulose, and its method is:

The first step. get 1 part of mushroom dry plate, put into hot melt and separate still, add≤80 ℃, 10-30 water doubly, soak 30-60 with minute after separate, drain with centrifuge, add 1: 10-50 times of 0.5-3 mole hydrochloride soaking and stirring 2-5 hour stops stirring, static layering is isolated light green color mother liquor with centrifuge;

Second goes on foot. and be washed till through tap water and change 1 after PH is neutrality: 10-50 times of 0.5-3 molar sodium hydroxide stirs and stopped in 2-5 hour stirring, and stirs after static 4-12 hour to stop in 1-4 hour stirring again, and static 2-5 hour, discards the dark-brown mother liquor after the static layering; Change running water and be washed till PH, separate mushroom pieces and drain for neutral;

The 3rd step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stopped to stir, and static layering is isolated faint yellow mother liquor; Change running water and be washed till PH, separate mushroom pieces and drain for neutral;

The 4th step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till PH for neutral, change the pure water washing once, the static layering filter residue drains;

The 5th step. take out and deliver to oven for drying, oven dry gets the mushroom cellulose after pulverizer is crushed to the 60-80 order.

The present invention has changed traditional cellulose and has derived from fibre of plant, but obtains proportion from 200g/cm through soda acid and PROCESS FOR TREATMENT from the mycelia fructification of the spore of reaching maturity ³～900g/cm ³The mushroom cellulose, from the cellulose that edible funguses such as mushroom extract, be β type glucose configuration.Cellulose self quite stable, safer, its heating is zero, and polysaccharide component especially wherein has by macrophage and stimulates production of antibodies to reach the physiological function that improves the human immunological competence, provides a kind of novel raw material for developing relevant health products and medicine.

This method adapts to suitability for industrialized production, and method is easy, can obtain high efficiency, low cost under the prerequisite of quality assurance, broad-spectrum cellulose products.

Advantage of the present invention is:

1. be difficult for mouldyly, cellulose is a β type glucose configuration;

2. cellulose self quite stable is difficult for reacting with other material generally speaking, and is safer;

3. but be not the β type glucose of health digestion though be made of glucose, its caloric value is zero.

The specific embodiment

The invention will be further described below in conjunction with embodiment.

Embodiment 1:

Take by weighing through behind the crushing screening＜after 100 purpose mushrooms are pulverized material 50g and added 2.5 molar sodium hydroxides and soak 2 hours, stirred 4 hours, stop stirring, static layering is isolated and is the dark-brown mother liquor; The mushroom materials slag is washed PH from the beginning and is separated to neutral back, and the material slag is drained; Add 2.5 mole hydrochlorides again and stirred 4 hours, stop to stir, static layering is isolated and is the aquamarine blue mother liquor; Property among the mushroom residue is washed, separate the back, and the material slag is drained; Add 2.5 molar sodium hydroxides again and stirred 4 hours, stop to stir, static layering is isolated band light brown mother liquor; Add 2.5 molar sodium hydroxides again and stirred 4 hours, stop to stir static layering; Isolate and be with faint yellow mother liquor; The material slag is drained, and washes PH from the beginning to neutral; Change the pure water washing, 5L washs once, separates aqueous cellulosic 350ml, carries out vacuum freeze drying after the pre-freeze; The dried cellulose that obtains sieves to such an extent that mushroom cellulose volume is 75ml weight 18.5g once more.

Example 2:

Get mushroom dry plate 50g and separate after 30 minutes through 〉=80 ℃ of hot-water soaks, remove to soak water, drain and add 2.5 mole hydrochloride soaking and stirring 4 hours, stop to stir, static layering is isolated the yellow green mother liquor; Be washed till through tap water and add 2.5 molar sodium hydroxides after PH is neutrality and stir and to stop in 4 hours stirring, stir again after static 12 hours and stopped in 2 hours stirring, static 2 hours, discard the dark-brown mother liquor after the static layering; Change running water and be washed till PH, separate mushroom pieces and drain for neutral; Add 2.5 molar sodium hydroxides again and stirred 2 hours, stop to stir, stirred 2 hours after static 2 hours again, stop to stir, static layering is isolated the khaki mother liquor; Change running water and be washed till PH, separate mushroom pieces and drain for neutral; Add 2.5 molar sodium hydroxides again and stirred 2 hours, stop to stir, stirred 2 hours after static 2 hours again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till PH for neutral, changes the pure water washing once, and the static layering filter residue drains; Oven for drying is delivered in taking-up; To get volume 20ml weight be 14.2g after pulverizer is pulverized the 60-80 order in oven dry

Mushroom fruiting body cellulose and general cellulose performance comparison sheet

	General cellulose	The mushroom cellulose
			Peculiar function		A, the cellulose that extracts from mushroom fruiting body, the polysaccharide component that contains can produce the stimulation antibody of macrophage and reach human immunological competence's raising
	B, contain abundant trace element--germanium, have health care, promote longevity, anti-ageing, antitumor efficacy
		Total function		A, imbibition in stomach, be easy to produce satiety and suppress the feed obesity is had regulatory function preferably
B, can suppress T-CHOL and raise, reduce the synthetic of cholic acid and its esters and absorb, accelerate fatty deslagging prevention cardiovascular and cerebrovascular disease
			C, slow down small intestine to the absorption of glucose, suppress postprandial blood sugar and raise, effectively prevent diabetes
D, reduce and to induce breast cancer female hormone to be diffused into the probability in the tissue in the blood and reduce generation breast cancer
			E, form good environment, suppress that microbiologic population forms in the growth alteration enteron aisle of saprophytic bacteria the survival and reproduction of intestinal beneficial bacterium
Hydroxy kind side chain radical in f, its structure because of, can adsorb in the enteron aisle particularly carcinogen of harmful substance, reduce enteron aisle cancer and hemorrhoid
			G, can and discharge sodium, the potassium ratios that reduce in the blood, the effects of bringing high blood pressure down in a large number with sodium ion in the enteron aisle, potassium ion exchange

Claims (3)

1. a mushroom fruiting body cellulose is characterized in that, repeatedly handles through soda acid and pure water from mushroom fruiting body or powder and removes the various materials beyond the cellulose and obtain simple mycelia cellulose.

2. the extracting method of a mushroom fruiting body cellulose is extracted from the mushroom powder, the steps include:

The first step. take by weighing behind crushing screening＜100 purpose mushrooms pulverize material and add 1 for 1 part: 10-50 times of 0.5-3 molar sodium hydroxide, soaks after 1-3 hour, stirred 2-5 hour with dissolution kettle, stop stirring, static layering is isolated with centrifuge and to be the dark-brown mother liquor; Mushroom materials slag input washing still carries out the running water washing, and PH separates to neutral back, delivers to centrifuge and will expect that slag drains;

Second step. add 1 again: 10-50 part 0.5-3 mole hydrochloride stirred 2-5 hour, stopped to stir, and static layering is isolated and is the light green mother liquor; Property among the mushroom residue is washed, separate the back, and the material slag drains;

The 3rd step. add 1 again: 10-50 part 0.5-3 molar sodium hydroxide stirred 2-5 hour, stopped to stir, and static layering is isolated band light brown mother liquor;

The 4th step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till PH for neutral, change the pure water washing once, the static layering filter residue drains;

The 5th step. with carrying out vacuum freeze drying after the freeze drier pre-freeze; Obtain dried cellulose, sieve once more the mushroom cellulose.

3. the extracting method of a mushroom fruiting body cellulose is characterized in that, repeatedly handles through soda acid and pure water from mushroom fruiting body and removes the various materials beyond the cellulose and obtain simple mushroom cellulose, and its method is:

The first step. get 1 part of mushroom dry plate, put into hot melt and separate still, add≤80 ℃, 10-30 water doubly, soak 30-60 with minute after separate, drain with centrifuge, add 1: 10-50 times of 0.5-3 mole hydrochloride soaking and stirring 2-5 hour stops stirring, static layering is isolated light green color mother liquor with centrifuge;

Second goes on foot. and be washed till through tap water and change 1 after PH is neutrality: 10-50 times of 0.5-3 molar sodium hydroxide stirs and stopped in 2-5 hour stirring, and stirs after static 4-12 hour to stop in 1-4 hour stirring again, and static 2-5 hour, discards the dark-brown mother liquor after the static layering; Change running water and be washed till PH, separate mushroom pieces and drain for neutral;

The 3rd step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stopped to stir, and static layering is isolated faint yellow mother liquor; Change running water and be washed till PH, separate mushroom pieces and drain for neutral;

The 4th step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till PH for neutral, change the pure water washing once, the static layering filter residue drains;

The 5th step. take out and deliver to oven for drying, oven dry gets the mushroom cellulose after pulverizer is crushed to the 60-80 order.