CN109041630A - A kind of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution and preparation method thereof - Google Patents
A kind of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution and preparation method thereof Download PDFInfo
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- CN109041630A CN109041630A CN201810670097.5A CN201810670097A CN109041630A CN 109041630 A CN109041630 A CN 109041630A CN 201810670097 A CN201810670097 A CN 201810670097A CN 109041630 A CN109041630 A CN 109041630A
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- bitter buckwheat
- juice
- roxburghii tratt
- rosa roxburghii
- oral solution
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- 238000012986 modification Methods 0.000 description 1
- 150000002772 monosaccharides Chemical class 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 235000020995 raw meat Nutrition 0.000 description 1
- 235000021254 resistant starch Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000036186 satiety Effects 0.000 description 1
- 235000019627 satiety Nutrition 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 231100000701 toxic element Toxicity 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01C—PLANTING; SOWING; FERTILISING
- A01C1/00—Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G22/00—Cultivation of specific crops or plants not otherwise provided for
- A01G22/20—Cereals
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/46—Preservation of non-alcoholic beverages by heating
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
The invention discloses a kind of hypoglycemic Rosa roxburghii Tratt bitter buckwheat bud oral solutions and preparation method thereof.Rosa roxburghii Tratt bitter buckwheat bud oral solution is product made of being compounded by a certain percentage using Rosa roxburghii Tratt, bitter buckwheat bud as primary raw material.Production method is cultivated bitter buckwheat seed vernalization into bitter buckwheat sprout, is then harvested, is cleaned, squeezing the juice, extraction obtains bitter buckwheat bud juice.By the Rosa roxburghi Juice after clarifying treatment of taking away the puckery taste with after bitter buckwheat bud juice mixed processing, degassing sterilizes, is filling, cooling, after the assay was approved up to Rosa roxburghii Tratt bitter buckwheat bud oral solution.Rosa roxburghii Tratt bitter buckwheat bud oral solution natural nuisance-free provided by the invention, comfortable taste have preferable effect of lowering blood sugar, are a kind of drinks with peculiar flavour.
Description
Technical field
The invention belongs to oral solution preparation technical field, it is related to a kind of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution and its preparation side
Method.
Background technique
It Rosa roxburghii Tratt also known as send the spring to return, rosa roxburghii, is a kind of perennial fallen leaves bush of rosaceae Rosa, is distributed mainly on
The ground such as China Guizhou Bijie, six Pan Shui.National successively You20Duo Ge provinces and cities establish the artificial of large area from Guizhou Introduction And Trial
Cultivation base.Rosa roxburghii nutrition is abundant, except containing carbohydrate, protein, vitamin, inorganic salts and a variety of amino acid needed by human etc.
Outside main nutrient composition, flavones, organic acid and ascorbic acid also rich in, polysaccharide, superoxide dismutase, polyphenol, three
The bioactive substances such as terpene, sterol, medical value and hypoglycemic effect with higher.Traditional medicine mainly by its fruit,
Root is used as medicine, for helping digestion, antidiarrheal, relieving summer-heat and having indigestion abdominal distension, dysentery, enteritis, hypertension, angiorrhoxis bleeding, hypovitaminosis C
The treatment of the diseases such as disease.In addition, Rosa roxburghii Tratt, which also has, adjusts body's immunity, removing toxic substances, calmness, anti-aging, anti-atherogenic
The functions such as hardening, antitumor.
Buckwheat sprout is called rutin bitter buckwheat seedling, is the seedling generated using Germination of Buckwheat Seed, contains in cauline leaf abundant
Rutin.Rutin has expansion and strengthens the function of blood vessel, has good preventive effect, China people to hypertension and cardiovascular disease
Between early have edible buckwheat young stem and leaf traditional habit." a kind of fish raw meat No. CN201710222445.8 in Chinese patent application part
Careless ragopyrum tataricum beverage and preparation method thereof " it provides using cordate houttuynia and bitter buckwheat as cordate houttuynia ragopyrum tataricum beverage made of primary raw material.
No. CN201710838636.7 " honey tartary buckwheat tea and preparation method thereof " provides using honey and bitter buckwheat as one kind of primary raw material
Honey method for preparing duck wheat tea.But up to the present the only bitter buckwheat seed of the raw material in these patented technology products does not have
Bitter buckwheat seed is developed and compounds the patent application for carrying out the production of oral solution technology with Rosa roxburghi Juice for buckwheat peas.
Patent of invention content
It is abundant that the main purpose of the present invention is to provide a kind of nutritive values, and blood sugar decreasing effect is significant, the thorn of brisk taste
Pears bitter buckwheat seedling oral solution improves daily life, has preferable prevention and relaxation effect to hyperglycemia.
The technical solution that the invention patent solves above-mentioned technical problem is as follows:
A kind of preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution, comprising the following steps:
(1) choose seeds: reject it is damaged, damage by worms, go mouldy, shrivelled seed and impurity, choose fresh, full, germination percentage is high, at
Ripe degree height, storage time are no more than 2 years bitter buckwheat seeds；
(2) vernalization is sterilized: by the bitter buckwheat seed KMnO of step (1)4It is rinsed well after solution sterilization；It is 5- in water content
Cause 40-50h vernalization in 10% sandstone matrix；
(3) sow: the seed after taking appropriate vernalization is seeded in sandstone germination disk, evenly laid out sterile nothing in sandstone disk
Soil property sandstone, seed are sowed in sand bed at 1-1.5cm；
(4) sprout culture: after planting each moisturizing is primary sooner or later, keeps sand culture wet, ensures that seed smoothly sprouts；After planting
48h rises, and respectively sprays a mineral nutrition liquid sooner or later；
(5) harvest: bitter buckwheat bud cotyledon is shown laid flat in green after nursery 8-12d, and hypocotyl is in aubergine, and nearly root is white,
It can be harvested without samping off, without rotten neck, free from extraneous odour, and when bud length reaches 10-15cm or more；
(6) it squeezes the juice: selecting the tartary buckwheat malt of 10cm or so, remove kind of shell and rotten tartary buckwheat malt, clean up, be put into
Blanching 3-10min in 80-100 DEG C of water；Tartary buckwheat malt is crushed with juicing seperator and is squeezed the juice by the water for adding 50-100 times, juicing
After be put into beaker, extract 1-2h at 55-60 DEG C, be centrifuged 5-20min under 4000-8000r/min revolving speed, filter bitter
Buckwheat bud juice；
(7) Rosa roxburghii Tratt is squeezed the juice: being selected yellow and orange-yellow Single Roxburgh Rose Fruit, is removed the Rosa roxburghii Tratt and sandstone for rotting, damaging by worms, washed with clear water
Remove the soil and dust debris on Rosa roxburghii Tratt；After being broken into the fruit block of 0.3-0.5cm with stainless steel crusher, it is sent into stainless steel juicing
Machine presses extracting juice, and the tannin in 1 ‰ tannic acid hydrolysis Single Roxburgh Rose Fruit is added, carries out processing of taking away the puckery taste；The sorbic acid of 1g/kg is added
Potassium, 0.03g/kgEDTA carry out anti-corrosion color protection, after standing three days；Gelatin and diatomite clarification are added, thorn is filtered to obtain after three days
Pear juice；
(8) bitter buckwheat bud juice is deployed with Rosa roxburghi Juice: Rosa roxburghi Juice obtained in above-mentioned steps, bitter buckwheat bud juice are mixed to obtain mixing fruit
Compound stabilizer, sucrose and citric acid are dissolved in after dissolving in warm water and being added in blended fruit juice to uniform state, mixed by juice
Juice；
(9) degassing sterilization: step (8) mixed juice is deaerated, filling while hot after then being sterilized using autoclaving,
40 DEG C are subsequently cooled to hereinafter, up to the Rosa roxburghii Tratt bitter buckwheat seedling oral solution.
Preferably, step (2) KMnO4Solution concentration is 0.10%-0.20%, and sterilizing time is 10~15min.
Preferably, sand bed thickness 3-5cm in step (2) the sandstone disk, the sandstone, which are common river sands, removes soil through eluriating
Matter part is dried at 120 DEG C, sterilizes gained after 2h after sieving under 150 DEG C of high temperature and ultraviolet lamp.
Preferably, condition of culture described in step (4): humidity 60-80%, 23-28 DEG C of temperature control, intensity of illumination 10000Lx,
The illumination period is preceding 5d dark, rear 5d illumination, daily light irradiation time 10-12h.
Preferably, mineral nutrition liquid described in step (4) includes the raw material of following parts by weight: Ca (NO3)2·4H2O
472mg/L；KNO3202mg/L；NH4NO380mg/L；KH2PO4136mg/L；K2SO4174mg/L；MgSO4120mg/L,
The preparation method comprises the following steps: by Ca (NO3)2·4H2O and KNO3It is hybridly prepared into nutrition A liquid, by MgSO4And NH4H2PO4It is hybridly prepared into
For nutrition B liquid.Inorganic salt quality is accurately weighed, is respectively placed in beaker and is dissolved in water, is mixed after being completely dissolved, by gained each group
A, B solution is settled to 500mL respectively, is stored in spare in brown reagent bottle.
Preferably, Rosa roxburghi Juice described in step (8): bitter buckwheat bud juice: compound stabilizer: sucrose: the mass ratio of citric acid are as follows:
35:16:10:9:0.1, wherein the compound stabilizer is made of in mass ratio for 15:3:7 CMC, xanthan gum, pectin.
Preferably, degassing conditions described in step (9): vacuum degree 90-100KPa, batch temperature are 20-25 DEG C, are taken off
Gas 15-30min.
Preferably, high pressure sterilization method described in step (9) is the 10-20min that sterilizes at 100-120 DEG C.
It is a further object of the present invention to provide a kind of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solutions, are main with Rosa roxburghii Tratt, bitter buckwheat bud
Raw material compounds manufactured product by a certain percentage.
The medical mechanism of the hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution of the present invention:
Rosa roxburghii Tratt is that vitamin C and citrin content are highest in existing fruit, by the Kiwi berry Victoria C content of good reputation
Also only have the 11% of Rosa roxburghii Tratt.In addition, the citrin content of Rosa roxburghii Tratt is also significantly larger than other fruits and vegetables, exceed other fruit and vegetable 10-
150 times are differed；The SOD that Rosa roxburghii Tratt is rich in is known as " biological gold ", has anti-cancer and cancer-preventing effect；Fruit of Grossularia burejensis Berger contains 18 kinds of ammonia
Base acid, including 8 kinds of necessary amino acid of human body；Rosa roxburghii Tratt VE content 2.40-3.61mg/100kg is used as antioxygen in vivo
Agent has the function of promoting longevity.It is certain animal experiments show that, supplement VE can inhibit the generation of animal tumor.In Rosa roxburghii Tratt
SOD, Polysaccharides from Rosa roxburghii and vitamin C, microelement isoreactivity ingredient synergistic effect can accelerate the excretion of lead, manganese, cadmium, arsenic, mercury etc.,
Its content in vivo is reduced, to play the detoxication to heavy metal.
Contain a large amount of resistant starch and dietary fiber in bitter buckwheat, makes tartary buckwheat product that there is high satiety, it is low glycemic
Index and low insulin index can improve glycometabolism, reduce the risk for suffering from coronary heart disease, obesity, diabetes, prevent and treat cholesterol mistake
High and obesity etc.；For the protein content of tartary buckwheat between 8%-19%, amino acid is balanced, and biological value is high.Bitter buckwheat albumen has
Anticancer, norcholesterol effect；About containing the lipid of 2.1%-3.0% in tartary buckwheat seed, triacylglyceride is in tartary buckwheat
The chief component of property lipid；In buckwheat powder other than calcium content is relatively low, Qi Tatie, zinc, manganese, copper, magnesium, potassium, 7 kinds of phosphorus
Minerals account for the 10%-80% for recommending Day feeding amount；Tartary buckwheat is rich in the opposite natural organic selenium lacked of other cereal, and selenium is in people
Body helps to mediate the toxic element in human body, adjusts body's immunity；Trivalent chromium also rich in, can enhance in bitter buckwheat
Insulin function is to improve glucose tolerance；Tartary buckwheat seed B family vitamin content is about 0.78mg/100g, is rich in vitamin
The citrin not having in B1, B2 and B6 and other cereal.
Bitter buckwheat gained bean sprout after germination has full of nutrition, and amino acid ratio is reasonable, and protein digestibility utilization rate is high,
Contents of monosaccharides is high, and unsaturated fatty acid, vitamin and mineral are abundant, and anti-nutritional factors is low, no allergy mechanism, rich in a large amount of raw
The characteristics of object Flavonoid substances, and there is stronger anti-oxidant, lower hyperlipidemia, hypertension, hyperglycemia, reduce capillary permeability and capilary is maintained to follow
The functional activities such as ring are a kind of good nutritional health food resources.
Compared with prior art, the beneficial effect of the invention patent is:
Rosa roxburghii Tratt bitter buckwheat seedling oral solution provided by the invention is a kind of natural nuisance-free drink with obvious effect of lowering blood sugar,
Using Rosa roxburghi Juice and bitter buckwheat juice as main raw material(s) in the present invention, addition compound stabilizer, sucrose and citric acid act synergistically, preparation
Oral solution brisk taste, unique in taste, natural nuisance-free has significant hypoglycemic effect, can do daily drinks and drink, can also
The medicinal conditioning hyperglycemia of diet is done, is a kind of drink full of nutrition.
Specific embodiment
The principle of the invention patent and feature are described below, patent that the given examples are served only to explain the present invention, and
The non-range for being used to limit the invention patent.
Embodiment 1
A kind of preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution, comprising the following steps:
(1) choose seeds: reject it is damaged, damage by worms, go mouldy, shrivelled seed and impurity, choose fresh, full, germination percentage is high, at
Ripe degree height, storage time are no more than 2 years bitter buckwheat seeds；
(2) it sterilizes vernalization: with concentration being 0.10%KMnO by the bitter buckwheat seed of step (1)4Solution sterilizes 15min backlash
Wash clean；It is to cause 50h vernalization in 5% sandstone matrix in water content；
(3) sow: the seed after taking appropriate vernalization is seeded in sandstone germination disk, and evenly laid out sand bed is thick in sandstone disk
The sterile no soil property sandstone of 3cm, seed are sowed in sand bed at 1cm；
(4) sprout culture: after planting each moisturizing is primary sooner or later, keeps sand culture wet, ensures that seed smoothly sprouts；After planting
48h rises, and respectively sprays a mineral nutrition liquid sooner or later；Setting condition of culture: humidity 60%, 23 DEG C of temperature control, intensity of illumination
10000Lx, illumination period are preceding 5d dark, rear 5d illumination, daily light irradiation time 12h；Wherein, mineral nutrition liquid includes as follows
The raw material of parts by weight: Ca (NO3)2·4H2O 472mg/L； KNO3202mg/L；NH4NO380mg/L；KH2PO4136mg/L；
K2SO4174mg/L；MgSO4120mg/L；
(5) harvest: bitter buckwheat bud cotyledon is shown laid flat in green after nursery 8d, and hypocotyl is in aubergine, and nearly root is white, without sudden
Disease, without rotten neck, free from extraneous odour, and when bud is long reach 10cm or more when can harvest；
(6) it squeezes the juice: selecting the tartary buckwheat malt of 10cm or so, remove kind of shell and rotten tartary buckwheat malt, clean up, be put into
Blanching 10min in 80 DEG C of water；Tartary buckwheat malt is crushed with juicing seperator and is squeezed the juice, is put into beaker after juicing by the water for adding 50 times
In, 2h is extracted at 55 DEG C, is centrifuged 20min under 4000r/min revolving speed, filters to obtain bitter buckwheat bud juice；
(7) Rosa roxburghii Tratt is squeezed the juice: being selected yellow and orange-yellow Single Roxburgh Rose Fruit, is removed the Rosa roxburghii Tratt and sandstone for rotting, damaging by worms, washed with clear water
Remove the soil and dust debris on Rosa roxburghii Tratt；After being broken into the fruit block of 0.3cm with stainless steel crusher, it is sent into stainless steel juice extractor pressure
Extracting juice is added the tannin in 1 ‰ tannic acid hydrolysis Single Roxburgh Rose Fruit, carries out processing of taking away the puckery taste；The potassium sorbate of addition 1g/kg,
0.03g/kgEDTA carries out anti-corrosion color protection, after standing three days；Gelatin and diatomite clarification are added, filters to obtain Rosa roxburghii Tratt after three days
Juice；
(8) bitter buckwheat bud juice is deployed with Rosa roxburghi Juice: Rosa roxburghi Juice obtained in above-mentioned steps, bitter buckwheat bud juice are mixed to obtain mixing fruit
Compound stabilizer, sucrose and citric acid are dissolved in after dissolving in warm water and being added in blended fruit juice to uniform state, mixed by juice
Juice；Wherein Rosa roxburghi Juice: bitter buckwheat bud juice: compound stabilizer: sucrose: the mass ratio of citric acid are as follows: 35:16:10:9:0.1, wherein institute
Compound stabilizer is stated to be made of in mass ratio for 15:3:7 CMC, xanthan gum, pectin；
(9) degassing sterilization: by step (8) mixed juice vacuum degree be 90KPa, batch temperature be 20 DEG C at deaerate
30min, then using autoclaving sterilize, at 100 DEG C sterilize 20min after it is filling while hot, be subsequently cooled to 40 DEG C hereinafter,
Up to the Rosa roxburghii Tratt bitter buckwheat seedling oral solution.
Embodiment 2
A kind of preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution, comprising the following steps:
(1) choose seeds: reject it is damaged, damage by worms, go mouldy, shrivelled seed and impurity, choose fresh, full, germination percentage is high, at
Ripe degree height, storage time are no more than 2 years bitter buckwheat seeds；
(2) it sterilizes vernalization: with concentration being 0.15%KMnO by the bitter buckwheat seed of step (1)4Solution sterilizes 12min backlash
Wash clean；It is to cause 48h vernalization in 5.7% sandstone matrix in water content；
(3) sow: the seed after taking appropriate vernalization is seeded in sandstone germination disk, and evenly laid out sand bed is thick in sandstone disk
The sterile no soil property sandstone of 3-5cm, seed are sowed in sand bed at 1.5cm；
(4) sprout culture: after planting each moisturizing is primary sooner or later, keeps sand culture wet, ensures that seed smoothly sprouts；After planting
48h rises, and respectively sprays a mineral nutrition liquid sooner or later；Setting condition of culture: humidity 80%, 25 DEG C of temperature control, intensity of illumination
10000Lx, illumination period are preceding 5d dark, rear 5d illumination, daily light irradiation time 12h；Wherein, mineral nutrition liquid includes as follows
The raw material of parts by weight: Ca (NO3)2·4H2O 472mg/L； KNO3202mg/L；NH4NO380mg/L；KH2PO4136mg/L；
K2SO4174mg/L；MgSO4120mg/L；
(5) harvest: bitter buckwheat bud cotyledon is shown laid flat in green after nursery 10d, and hypocotyl is in aubergine, and nearly root is white, nothing
Samping off can be harvested without rotten neck, free from extraneous odour, and when bud length reaches 15cm or more；
(6) it squeezes the juice: selecting the tartary buckwheat malt of 10cm or so, remove kind of shell and rotten tartary buckwheat malt, clean up, be put into
Blanching 5min in 90 DEG C of water；Tartary buckwheat malt is crushed with juicing seperator and is squeezed the juice, is put into beaker after juicing by the water for adding 50 times
In, 1h is extracted at 60 DEG C, is centrifuged 10min under 4500r/min revolving speed, filters to obtain bitter buckwheat bud juice；
(7) Rosa roxburghii Tratt is squeezed the juice: being selected yellow and orange-yellow Single Roxburgh Rose Fruit, is removed the Rosa roxburghii Tratt and sandstone for rotting, damaging by worms, washed with clear water
Remove the soil and dust debris on Rosa roxburghii Tratt；After being broken into the fruit block of 0.5cm with stainless steel crusher, it is sent into stainless steel juice extractor pressure
Extracting juice is added the tannin in 1 ‰ tannic acid hydrolysis Single Roxburgh Rose Fruit, carries out processing of taking away the puckery taste；The potassium sorbate of addition 1g/kg,
0.03g/kg EDTA carries out anti-corrosion color protection, after standing three days；Gelatin and diatomite clarification are added, filters to obtain Rosa roxburghii Tratt after three days
Juice；
(8) bitter buckwheat bud juice is deployed with Rosa roxburghi Juice: Rosa roxburghi Juice obtained in above-mentioned steps, bitter buckwheat bud juice are mixed to obtain mixing fruit
Compound stabilizer, sucrose and citric acid are dissolved in after dissolving in warm water and being added in blended fruit juice to uniform state, mixed by juice
Juice；Wherein Rosa roxburghi Juice: bitter buckwheat bud juice: compound stabilizer: sucrose: the mass ratio of citric acid are as follows: 35:16:10:9:0.1, wherein institute
Compound stabilizer is stated to be made of in mass ratio for 15:3:7 CMC, xanthan gum, pectin；
(9) degassing sterilization: by step (8) mixed juice vacuum degree be 92KPa, batch temperature be 20 DEG C at deaerate
15-30min, then using autoclaving sterilize, at 100 DEG C sterilize 20min after it is filling while hot, be subsequently cooled to 40 DEG C with
Under to get the Rosa roxburghii Tratt bitter buckwheat seedling oral solution.
Embodiment 3
A kind of preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution, comprising the following steps:
(1) choose seeds: reject it is damaged, damage by worms, go mouldy, shrivelled seed and impurity, choose fresh, full, germination percentage is high, at
Ripe degree height, storage time are no more than 2 years bitter buckwheat seeds；
(2) it sterilizes vernalization: with concentration being 0.20%KMnO by the bitter buckwheat seed of step (1)4Solution sterilizes 15min backlash
Wash clean；It is to cause 40h vernalization in 10% sandstone matrix in water content；
(3) sow: the seed after taking appropriate vernalization is seeded in sandstone germination disk, and evenly laid out sand bed is thick in sandstone disk
The sterile no soil property sandstone of 5cm, seed are sowed in sand bed at 1.5cm；
(4) sprout culture: after planting each moisturizing is primary sooner or later, keeps sand culture wet, ensures that seed smoothly sprouts；After planting
48h rises, and respectively sprays a mineral nutrition liquid sooner or later；Setting condition of culture: humidity 80%, 28 DEG C of temperature control, intensity of illumination
10000Lx, illumination period are preceding 5d dark, rear 5d illumination, daily light irradiation time 10h；Wherein, mineral nutrition liquid includes as follows
The raw material of parts by weight: Ca (NO3)2·4H2O 472mg/L； KNO3202mg/L；NH4NO380mg/L；KH2PO4136mg/L；
K2SO4174mg/L；MgSO4120mg/L；
(5) harvest: bitter buckwheat bud cotyledon is shown laid flat in green after nursery 12d, and hypocotyl is in aubergine, and nearly root is white, nothing
Samping off can be harvested without rotten neck, free from extraneous odour, and when bud length reaches 15cm or more；
(6) it squeezes the juice: selecting the tartary buckwheat malt of 10cm or so, remove kind of shell and rotten tartary buckwheat malt, clean up, be put into
Blanching 3min in 100 DEG C of water；Tartary buckwheat malt is crushed with juicing seperator and is squeezed the juice, is put into beaker after juicing by the water for adding 100 times
In, 1h is extracted at 60 DEG C, is centrifuged 5min under 8000r/min revolving speed, filters to obtain bitter buckwheat bud juice；
(7) Rosa roxburghii Tratt is squeezed the juice: being selected yellow and orange-yellow Single Roxburgh Rose Fruit, is removed the Rosa roxburghii Tratt and sandstone for rotting, damaging by worms, washed with clear water
Remove the soil and dust debris on Rosa roxburghii Tratt；After being broken into the fruit block of 0.3-0.5cm with stainless steel crusher, it is sent into stainless steel juicing
Machine presses extracting juice, and the tannin in 1 ‰ tannic acid hydrolysis Single Roxburgh Rose Fruit is added, carries out processing of taking away the puckery taste；The sorbic acid of 1g/kg is added
Potassium, 0.03g/kgEDTA carry out anti-corrosion color protection, after standing three days；Gelatin and diatomite clarification are added, thorn is filtered to obtain after three days
Pear juice；
(8) bitter buckwheat bud juice is deployed with Rosa roxburghi Juice: Rosa roxburghi Juice obtained in above-mentioned steps, bitter buckwheat bud juice are mixed to obtain mixing fruit
Compound stabilizer, sucrose and citric acid are dissolved in after dissolving in warm water and being added in blended fruit juice to uniform state, mixed by juice
Juice；Wherein Rosa roxburghi Juice: bitter buckwheat bud juice: compound stabilizer: sucrose: the mass ratio of citric acid are as follows: 35:16:10:9:0.1, wherein institute
Compound stabilizer is stated to be made of in mass ratio for 15:3:7 CMC, xanthan gum, pectin；
(9) degassing sterilization: by step (8) mixed juice vacuum degree be 100KPa, batch temperature be 25 DEG C at deaerate
15min, then using autoclaving sterilize, at 100 DEG C sterilize 20min after it is filling while hot, be subsequently cooled to 40 DEG C hereinafter,
Up to the Rosa roxburghii Tratt bitter buckwheat seedling oral solution.
It is obvious to a person skilled in the art that the invention patent is not limited to the details of above-mentioned exemplary embodiment, and
And without departing substantially from the spirit or essential attributes of the invention patent, it can realize in other specific forms of the invention special
Benefit.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, the present invention is special
The range of benefit is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in
All changes in justice and range are included in the invention patent, and any label in claim should not be considered as involved by limitation
And claim.
The above description is only a preferred embodiment of the patent of the present invention, is not intended to limit the invention patent, all in the present invention
Within the spirit and principle of patent, any modification, equivalent replacement, improvement and so on should be included in the guarantor of the invention patent
Within the scope of shield.
Claims (10)
1. a kind of preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution, it is characterised in that: the following steps are included:
(1) it chooses seeds: rejecting breakage, damage by worms, go mouldy, shrivelled seed and impurity, selection is fresh, full, germination percentage is high, maturity
High, storage time is no more than 2 years bitter buckwheat seeds；
(2) vernalization is sterilized: by the bitter buckwheat seed KMnO of step (1)4It is rinsed well after solution sterilization；It is 5-10% in water content
Cause 40-50h vernalization in sandstone matrix；
(3) sow: the seed after taking appropriate vernalization is seeded in sandstone germination disk, evenly laid out sterile no soil property in sandstone disk
Sandstone, seed are sowed in sand bed at 1-1.5cm；
(4) sprout culture: after planting each moisturizing is primary sooner or later, keeps sand culture wet, ensures that seed smoothly sprouts；After planting 48h
It rises, respectively sprays a mineral nutrition liquid sooner or later；
(5) harvest: bitter buckwheat bud cotyledon is shown laid flat in green after nursery 8-12d, and hypocotyl is in aubergine, and nearly root is white, without sudden
Disease, without rotten neck, free from extraneous odour, and when bud is long reach 10-15cm or more when can harvest；
(6) it squeezes the juice: selecting the tartary buckwheat malt of 10cm or so, remove kind of shell and rotten tartary buckwheat malt, clean up, be put into 80-
Blanching 3-10min in 100 DEG C of water；Tartary buckwheat malt is crushed with juicing seperator and is squeezed the juice, put after juicing by the water for adding 50-100 times
Enter in beaker, extract 1-2h at 55-60 DEG C, be centrifuged 5-20min under 4000-8000r/min revolving speed, filters to obtain bitter buckwheat bud
Juice；
(7) Rosa roxburghii Tratt is squeezed the juice: being selected yellow and orange-yellow Single Roxburgh Rose Fruit, is removed the Rosa roxburghii Tratt and sandstone for rotting, damaging by worms, wash away thorn with clear water
Soil and dust debris on pears；After being broken into the fruit block of 0.3-0.5cm with stainless steel crusher, it is sent into stainless steel juice extractor pressure
Extracting juice is added the tannin in 1 ‰ tannic acid hydrolysis Single Roxburgh Rose Fruit, carries out processing of taking away the puckery taste；The potassium sorbate of addition 1g/kg,
0.03g/kgEDTA carries out anti-corrosion color protection, after standing three days；Gelatin and diatomite clarification are added, filters to obtain Rosa roxburghii Tratt after three days
Juice；
(8) bitter buckwheat bud juice is deployed with Rosa roxburghi Juice: Rosa roxburghi Juice obtained in above-mentioned steps, bitter buckwheat bud juice are mixed into obtain blended fruit juice,
Compound stabilizer, sucrose and citric acid are dissolved in after being dissolved in warm water and being added in blended fruit juice to uniform state, obtains mixed juice；
(9) degassing sterilization: step (8) mixed juice is deaerated, filling while hot after then being sterilized using autoclaving, then
40 DEG C are cooled to hereinafter, up to the Rosa roxburghii Tratt bitter buckwheat seedling oral solution.
2. the preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution as described in claim 1, it is characterised in that: step (2) institute
State KMnO4Solution concentration is 0.10%-0.20%, and sterilizing time is 10~15min.
3. the preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution as described in claim 1, it is characterised in that: step (2) institute
State sand bed thickness 3-5cm in sandstone disk, the sandstone are that common river sand through eluriating removes soil property part, dry, are sieved at 120 DEG C
Obtained by being sterilized under 150 DEG C of high temperature and ultraviolet lamp after 2h afterwards.
4. the preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution as described in claim 1, it is characterised in that: in step (4)
The condition of culture: humidity 60-80%, 23-28 DEG C of temperature control, intensity of illumination 10000Lx, the illumination period is preceding 5d dark, rear 5d
Illumination, daily light irradiation time 10-12h.
5. the preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution as described in claim 1, it is characterised in that: in step (4)
The mineral nutrition liquid includes the raw material of following parts by weight: Ca (NO3)2·4H2O 472mg/L；KNO3202mg/L；NH4NO3
80mg/L；KH2PO4136mg/L；K2SO4174mg/L；MgSO4 120mg/L。
6. the preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution as described in claim 1, it is characterised in that: in step (8)
The Rosa roxburghi Juice: bitter buckwheat bud juice: compound stabilizer: sucrose: the mass ratio of citric acid are as follows: 35:16:10:9:0.1.
7. the preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution as described in claim 1, it is characterised in that: in step (8)
The compound stabilizer is made of in mass ratio for 15:3:7 CMC, xanthan gum, pectin.
8. the preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution as described in claim 1, it is characterised in that: in step (9)
The degassing conditions: vacuum degree 90-100KPa, batch temperature are 20-25 DEG C, and deaerate 15-30min.
9. the preparation method of hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution as described in claim 1, it is characterised in that: in step (9)
The high pressure sterilization method is the 10-20min that sterilizes at 100-120 DEG C.
10. hypoglycemic Rosa roxburghii Tratt bitter buckwheat seedling oral solution prepared by a kind of claim 1, it is characterised in that: based on Rosa roxburghii Tratt, bitter buckwheat bud
Raw material is wanted to compound manufactured product by a certain percentage.
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| CN112006191A (en) * | 2020-07-27 | 2020-12-01 | 遵义师范学院 | Roxburgh rose fruit juice beverage and preparation method thereof |
| CN116235949A (en) * | 2023-04-10 | 2023-06-09 | 成都大学 | Tartary buckwheat sprout rice cake and preparation method thereof |
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