CN100564666C - A kind of mushroom fruiting body cellulose - Google Patents
A kind of mushroom fruiting body cellulose Download PDFInfo
- Publication number
- CN100564666C CN100564666C CNB2007100414914A CN200710041491A CN100564666C CN 100564666 C CN100564666 C CN 100564666C CN B2007100414914 A CNB2007100414914 A CN B2007100414914A CN 200710041491 A CN200710041491 A CN 200710041491A CN 100564666 C CN100564666 C CN 100564666C
- Authority
- CN
- China
- Prior art keywords
- hour
- cellulose
- mushroom
- static
- fruiting body
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The present invention relates to a kind of mushroom fruiting body cellulose, it is characterized in that, repeatedly handle through soda acid and pure water from mushroom fruiting body and to remove the various materials beyond the cellulose and obtain simple mushroom fruiting body cellulose, advantage of the present invention be difficult for mouldy, cellulose is a β type glucose configuration, and cellulose self quite stable is difficult for reacting with other material generally speaking, safer, its caloric value is zero.The present invention adapts to suitability for industrialized production, and method is easy, can obtain high efficiency, low cost, broad-spectrum cellulose products under the prerequisite of quality assurance.Especially a kind of mushroom fruiting body cellulose that the present invention relates to can and stimulate production of antibodies to reach the physiological function that improves the human immunological competence by macrophage, provides a kind of novel raw material for developing relevant health products and medicine.
Description
Technical field
The present invention relates to a kind of mushroom fruiting body cellulose, relate in particular to a kind of mushroom fruiting body cellulose, belong to the cellulose technology field with the health products development of raw materials.
Background technology
Cellulose resource mainly obtains from plants such as cereal, beans, vegetables, fruit at present, and does not extract from the fructification mushroom of Mycophyta.
Summary of the invention
The purpose of this invention is to provide a kind of a kind of mushroom fruiting body cellulose that from the fructification mushroom of Mycophyta, extracts.
For realizing above purpose, technical scheme of the present invention provides a kind of extracting method of mushroom fruiting body cellulose, extracts from the mushroom powder, the steps include:
The first step. take by weighing behind crushing screening＜100 purpose mushrooms pulverize material and add 1 for 1 part: 10-50 times of 0.5-3 molar sodium hydroxide, soaks after 1-3 hour, stirred 2-5 hour with dissolution kettle, stop stirring, static layering is isolated with centrifuge and to be the dark-brown mother liquor; Mushroom materials slag input washing still carries out the running water washing, and pH separates to neutral back, delivers to centrifuge and will expect that slag drains;
Second step. add 1 again: 10-50 part 0.5-3 mole hydrochloride stirred 2-5 hour, stopped to stir, and static layering is isolated and is the light green mother liquor; Property among the mushroom residue is washed, separate the back, and the material slag drains;
The 3rd step. add 1 again: 10-50 part 0.5-3 molar sodium hydroxide stirred 2-5 hour, stopped to stir, and static layering is isolated band light brown mother liquor;
The 4th step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till pH for neutral, change the pure water washing once, the static layering filter residue drains;
The 5th step. with carrying out vacuum freeze drying after the freeze drier pre-freeze; Obtain dried cellulose, sieve once more mushroom fruiting body cellulose.
A kind of extracting method of mushroom fruiting body cellulose is characterized in that, repeatedly handles through soda acid and pure water from mushroom fruiting body and removes the various materials beyond the cellulose and obtain simple mushroom fruiting body cellulose, and its method is:
The first step. get 1 part of mushroom dry plate, put into hot melt and separate still, add≤80 ℃, 10-30 water doubly, soak 30-60 with minute after separate, drain with centrifuge, add 1: 10-50 times of 0.5-3 mole hydrochloride soaking and stirring 2-5 hour stops stirring, static layering is isolated light green color mother liquor with centrifuge;
Second goes on foot. and be washed till through tap water and change 1 after pH is neutrality: 10-50 times of 0.5-3 molar sodium hydroxide stirs and stopped in 2-5 hour stirring, and stirs after static 4-12 hour to stop in 1-4 hour stirring again, and static 2-5 hour, discards the dark-brown mother liquor after the static layering; Change running water and be washed till pH, separate mushroom pieces and drain for neutral;
The 3rd step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stopped to stir, and static layering is isolated faint yellow mother liquor; Change running water and be washed till pH, separate mushroom pieces and drain for neutral;
The 4th step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till pH for neutral, change the pure water washing once, the static layering filter residue drains;
The 5th step. take out and deliver to oven for drying, oven dry gets mushroom fruiting body cellulose after pulverizer is crushed to the 60-80 order.
The present invention has changed traditional cellulose and has derived from fibre of plant, but obtains proportion from 200g/cm through soda acid and PROCESS FOR TREATMENT from the mycelia fructification of the spore of reaching maturity
3～900g/cm
3The mushroom cellulose, from the cellulose that edible funguses such as mushroom extract, be β type glucose configuration.Cellulose self quite stable, safer, its heating is zero, and polysaccharide component especially wherein has by macrophage and stimulates production of antibodies to reach the physiological function that improves the human immunological competence, provides a kind of novel raw material for developing relevant health products and medicine.
This method adapts to suitability for industrialized production, and method is easy, can obtain high efficiency, low cost under the prerequisite of quality assurance, broad-spectrum cellulose products.
Advantage of the present invention is:
1. be difficult for mouldyly, cellulose is a β type glucose configuration;
2. cellulose self quite stable is difficult for reacting with other material generally speaking, and is safer;
3. but be not the β type glucose of health digestion though be made of glucose, its caloric value is zero.
The specific embodiment
The invention will be further described below in conjunction with embodiment.
Embodiment 1:
Take by weighing through behind the crushing screening＜after 100 purpose mushrooms are pulverized material 50g and added 2.5 molar sodium hydroxides and soak 2 hours, stirred 4 hours, stop stirring, static layering is isolated and is the dark-brown mother liquor; The mushroom materials slag is washed pH from the beginning and is separated to neutral back, and the material slag is drained; Add 2.5 mole hydrochlorides again and stirred 4 hours, stop to stir, static layering is isolated and is the aquamarine blue mother liquor; Property among the mushroom residue is washed, separate the back, and the material slag is drained; Add 2.5 molar sodium hydroxides again and stirred 4 hours, stop to stir, static layering is isolated band light brown mother liquor; Add 2.5 molar sodium hydroxides again and stirred 4 hours, stop to stir static layering; Isolate and be with faint yellow mother liquor; The material slag is drained, and washes pH from the beginning to neutral; Change the pure water washing, 5L washs once, separates aqueous cellulosic 350ml, carries out vacuum freeze drying after the pre-freeze; The dried cellulose that obtains sieves to such an extent that the mushroom fruiting body cellulose volume is 75ml weight 18.5g once more.
Example 2:
Get mushroom dry plate 50g and separate after 30 minutes through 〉=80 ℃ of hot-water soaks, remove to soak water, drain and add 2.5 mole hydrochloride soaking and stirring 4 hours, stop to stir, static layering is isolated the yellow green mother liquor; Be washed till through tap water and add 2.5 molar sodium hydroxides after pH is neutrality and stir and to stop in 4 hours stirring, stir again after static 12 hours and stopped in 2 hours stirring, static 2 hours, discard the dark-brown mother liquor after the static layering; Change running water and be washed till PH, separate mushroom pieces and drain for neutral; Add 2.5 molar sodium hydroxides again and stirred 2 hours, stop to stir, stirred 2 hours after static 2 hours again, stop to stir, static layering is isolated the khaki mother liquor; Change running water and be washed till pH, separate mushroom pieces and drain for neutral; Add 2.5 molar sodium hydroxides again and stirred 2 hours, stop to stir, stirred 2 hours after static 2 hours again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till pH for neutral, changes the pure water washing once, and the static layering filter residue drains; Oven for drying is delivered in taking-up; To get mushroom fruiting body cellulose volume 20ml weight be 14.2g after pulverizer is pulverized the 60-80 order in oven dry
Mushroom fruiting body cellulose and general cellulose performance comparison sheet
Claims (2)
1. the extracting method of a mushroom fruiting body cellulose is extracted from the mushroom powder, the steps include:
The first step. take by weighing behind crushing screening＜100 purpose mushrooms pulverize material and add 1 for 1 part: 10-50 times of 0.5-3 molar sodium hydroxide, soaks after 1-3 hour, stirred 2-5 hour with dissolution kettle, stop stirring, static layering is isolated with centrifuge and to be the dark-brown mother liquor; Mushroom materials slag input washing still carries out the running water washing, and pH separates to neutral back, delivers to centrifuge and will expect that slag drains;
Second step. add 1 again: 10-50 part 0.5-3 mole hydrochloride stirred 2-5 hour, stopped to stir, and static layering is isolated and is the light green mother liquor; Property among the mushroom residue is washed, separate the back, and the material slag drains;
The 3rd step. add 1 again: 10-50 part 0.5-3 molar sodium hydroxide stirred 2-5 hour, stopped to stir, and static layering is isolated band light brown mother liquor;
The 4th step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till pH for neutral, change the pure water washing once, the static layering filter residue drains;
The 5th step. with carrying out vacuum freeze drying after the freeze drier pre-freeze; Obtain dried cellulose, sieve once more mushroom fruiting body cellulose.
2. the extracting method of a mushroom fruiting body cellulose is characterized in that, repeatedly handles through soda acid and pure water from mushroom fruiting body and removes the various materials beyond the cellulose and obtain simple mushroom fruiting body cellulose, and its method is:
The first step. get 1 part of mushroom dry plate, put into hot melt and separate still, add≤80 ℃, 10-30 water doubly, soak 30-60 with minute after separate, drain with centrifuge, add 1: 10-50 times of 0.5-3 mole hydrochloride soaking and stirring 2-5 hour stops stirring, static layering is isolated light green color mother liquor with centrifuge;
Second goes on foot. and be washed till through tap water and change 1 after pH is neutrality: 10-50 times of 0.5-3 molar sodium hydroxide stirs and stopped in 2-5 hour stirring, and stirs after static 4-12 hour to stop in 1-4 hour stirring again, and static 2-5 hour, discards the dark-brown mother liquor after the static layering; Change running water and be washed till pH, separate mushroom pieces and drain for neutral;
The 3rd step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stopped to stir, and static layering is isolated faint yellow mother liquor; Change running water and be washed till pH, separate mushroom pieces and drain for neutral;
The 4th step. add 1 again: 10-50 times of 0.5-3 molar sodium hydroxide stirred 1-4 hour, stopped to stir, and stirred 1-4 hour after static 1-4 hour again, stop to stir, static layering is isolated faint yellow mother liquor, changes running water and is washed till pH for neutral, change the pure water washing once, the static layering filter residue drains;
The 5th step. take out and deliver to oven for drying, oven dry gets mushroom fruiting body cellulose after pulverizer is crushed to the 60-80 order.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100414914A CN100564666C (en) | 2007-05-31 | 2007-05-31 | A kind of mushroom fruiting body cellulose |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100414914A CN100564666C (en) | 2007-05-31 | 2007-05-31 | A kind of mushroom fruiting body cellulose |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101063279A CN101063279A (en) | 2007-10-31 |
| CN100564666C true CN100564666C (en) | 2009-12-02 |
Family
ID=38964537
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2007100414914A Expired - Fee Related CN100564666C (en) | 2007-05-31 | 2007-05-31 | A kind of mushroom fruiting body cellulose |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100564666C (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108142923A (en) * | 2018-03-14 | 2018-06-12 | 广东省微生物研究所（广东省微生物分析检测中心） | Purposes of the mushroom dietary fiber extract in the preparation for preparing treatment and/or prevention intestinal bacilli illness relevant disease |
| CN111587925A (en) * | 2020-06-02 | 2020-08-28 | 大连工业大学 | Preparation method of stable margarine prepared from degreased euphausia superba protein and composite cellulose |
-
2007
- 2007-05-31 CN CNB2007100414914A patent/CN100564666C/en not_active Expired - Fee Related
Non-Patent Citations (6)
| Title |
|---|
| 香菇多糖提取工艺和含量测定方法研究. 白玉静，佟丽华.黑龙江医药科学，第29卷第1期. 2006 |
| 香菇多糖提取工艺和含量测定方法研究. 白玉静，佟丽华.黑龙江医药科学，第29卷第1期. 2006 * |
| 香菇多糖提取技术的研究. 黄伟光.龙岩师专学报，第17卷第3期. 1999 |
| 香菇多糖提取技术的研究. 黄伟光.龙岩师专学报，第17卷第3期. 1999 * |
| 香菇子实体蛋白多糖Le-Ⅲ的分离、纯化及其性质研究. 杨娟，吴谋成，张声华.华中农业大学学报，第18卷第2期. 1999 |
| 香菇子实体蛋白多糖Le-Ⅲ的分离、纯化及其性质研究. 杨娟，吴谋成，张声华.华中农业大学学报，第18卷第2期. 1999 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101063279A (en) | 2007-10-31 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101775376B (en) | Compound bamboo shoot wall breaking enzyme and preparation method of bamboo shoot dietary fiber | |
| CN102450648B (en) | Extraction method for dietary fiber from citrus peel residues | |
| CN103859422B (en) | Production method of banana flower soluble dietary fiber | |
| CN101816413B (en) | Method for preparing insoluble tea-leaf dietary fiber | |
| CN101933613A (en) | Enzymolysis method for extracting insoluble dietary fiber from bamboo sprout | |
| CN106333193B (en) | Full-resource utilization method of sweet potato starch processing wastewater | |
| CN101933616A (en) | Method for preparing dietary fiber through solid-gas explosion | |
| CN101812111A (en) | Comprehensive deep processing method for oil tea fruits | |
| CN104366640B (en) | A kind of preparation method of Auricularia polycose beverage | |
| CN104757564A (en) | Method for preparing dietary fibers by means of peanut shells | |
| CN101828613B (en) | Process for producing Pu'er tea powder | |
| CN109527601A (en) | The preparation method of seaweed diet fiber | |
| CN101810271B (en) | Method for preparing highland barley green | |
| CN103319321A (en) | Extraction method of juglone and derivative in walnut green tangerine peel | |
| CN104957586A (en) | Multi-plant fiber salt and preparation method for same | |
| CN103284167B (en) | Preparation method of pholiota nameko insoluble dietary fiber | |
| CN101785831B (en) | Preparation method of rice bran dietary fiber | |
| CN103535743A (en) | Phyllostachys pracecox shoot dietary fiber and preparation method thereof | |
| CN100564666C (en) | A kind of mushroom fruiting body cellulose | |
| CN102630890B (en) | Method for preparing leechee or longan pulp powder | |
| CN103689611B (en) | A kind of extracting method of alfalfa dietary fiber | |
| CN102146143A (en) | Method for preparing pectin and cellulose from extracting residues of ginseng and American ginseng and application thereof | |
| CN101331923A (en) | Water melon meal fiber powder and preparation method and use thereof | |
| CN102020723B (en) | Method for continuously extracting low-ester pectin and microcrystalline cellulose from jerusalem artichoke stalks | |
| CN1037401C (en) | Iodine tea and producing method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 200240 Shanghai city Minhang District Jianchuan Road No. 951 Patentee after: Shanghai pharmaceutical Polytron Technologies Inc Address before: 200240 Shanghai city Minhang District Jianchuan Road No. 951 Patentee before: Shanghai Cirui Pharmaceutical Sci. & Tech. Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20091202 Termination date: 20200531 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |