CN101053352A - Buccal tablet and its preparation method - Google Patents

Buccal tablet and its preparation method Download PDF

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Publication number
CN101053352A
CN101053352A CN 200710068855 CN200710068855A CN101053352A CN 101053352 A CN101053352 A CN 101053352A CN 200710068855 CN200710068855 CN 200710068855 CN 200710068855 A CN200710068855 A CN 200710068855A CN 101053352 A CN101053352 A CN 101053352A
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extract
buccal tablet
preparation
dextrin
vitamin
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CN101053352B (en
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王岳飞
钱利生
宿迷菊
耿艳艳
杨贤强
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Zhejiang University ZJU
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Abstract

The present invention relates to a buccal tablet and its preparation method, in order to reduce the incidence probability of sore throat, composed of green tea extracts, saphium lychnophorum extracts, honeysuckle extracts, peppermint oil, vitamin c, sugar, dextrin and citric acid, its preparation method is that preparing green tea extracts, saphium lychnophorum extracts, honeysuckle extracts respectively, adding sugar, dextrin vitamin C and citric acid, with 60 percent (volume ratio) edible alcohol as wetting agent, stirring uniform, granulating, adding peppermint oil 20 to 100 and mixing after drying at 50 to 60 DGE C, compacting and moulding. It is scientific composing prescription, can not only be antiphlogistic and analgesia, but also enhance human body immunity, simple, fast and convenient, can preserve biological activity of various extracts maximum.

Description

A kind of buccal tablet and preparation method thereof
Technical field
The present invention relates to a kind of buccal tablet, especially relate to a kind of buccal tablet Chinese medicine and green tea composition, that have the pharynx-clearing throat-benefiting function that contains.
Background technology
Abscess of throat (sore throat) is oropharynx and a kind of clinical symptoms of laryngopharynx portion pathology, all suffer from acute or chronic pharyngitis, laryngitis, tonsillitis, circumtonsillar abscess, herpangina, ulceromembranous pharyngitis, throat abscess etc., all can cause the bottleneck throat congestion and swelling pain, swallow discomfort, claim again " larynx numbness ".Doctor trained in Western medicine generally believes it is by bacterial disease, the general local application that pays attention to combines the method for getting with antibiotic in treatment, as with 2% canopy acid solution, 3% salt solution and 1: 5000 furacilin solution be rinse repeatedly, perhaps use 2% jodine glycerin, 5% protargol liquid way in pharynx wall, or be contained in the oral cavity etc. with tabellae iodi gurgitis, Domiphen, peppermint etc., the function of certain relief of symptoms is arranged.China's traditional medicine is thought, abscess of throat is the heresy by affection of exogenous wind-heat mostly, or because of lung stomach stagnated fire upper punch, or by due to fire excess from yin deficiency, generally take to make up a prescription to the ill, take preparation, or take Chinese patent drug according to disease, but abscess of throat is a common frdquently encountered disease disease, seeking the dialectical preparation that makes up a prescription of doctor is a comparatively complicated process, patient treatment efficient is low, and doctor trained in Western medicine is too frequently measured and can be caused certain infringement to human body greatly eventually because use antibiotic, and incidence of disease height; Existing medical expert has appealed that the doctor changes treatment idea and the methods of treatment of traditional pharyngolaryngitis as the inflammation that swells and ache etc., not once finding that inflammation uses antibiotic, to reduce the side effect that antibiotic brings.
Summary of the invention
Purpose of the present invention mainly is that solution existing in prior technology therapeutic efficiency is not high, and uses antibiotic to the prejudicial technical problem of human body; Another object of the present invention is under the prerequisite of setting up the active treatment medical model, a kind of effectively anti-inflammatory analgesic is provided, be aided with buccal tablet that improves the body immunity effect and preparation method thereof simultaneously, make the treatment of this class common frdquently encountered disease disease of abscess of throat more simple and effective, reduce incidence probability.
Above-mentioned technical problem of the present invention is mainly solved by following technical proposals: buccal tablet is made by functional component, filler, binding agent, acidity regulator, wherein functional component is green-tea extract, Scaphium scaphigerum extract, Honegsukle flower P.E, peppermint oil and vitamin C, wherein honeysuckle is the close honeysuckle flower that adopts Xinmi City, Henan to produce, filler is a white granulated sugar, binding agent is a dextrin, acidity regulator is a citric acid, and concrete proportion of composing is counted by weight:
Green tea 500～1000 (the extract dry product is 75～150)
The sterculia seed 600～1200 (the extract dry product is 60～100)
Honeysuckle 200～600 (the extract dry product is 20～60)
Peppermint oil 20～100 Catergens 5～150 white granulated sugars 100～500
Dextrin 100～400 citric acids 20～70
The preparation method of buccal tablet is:
A: get green tea and put the water retting 0.5～1.5 hour that adds 10～15 times in the extractor, heating is boiled and was kept 1 hour, obtains decocting liquid one time, filters through 100～200 mesh sieve cloth; Be heated to and boil 1～1.5 hour frying in shallow oil water that slag adds 3～5 times, get the secondary decocting liquid, filter through 100～200 mesh sieve cloth, twice decocting liquid merging left standstill, get the upper strata stillness of night and send in the concentration tank, under atmospheric pressure state, be concentrated into relative density 1.15～1.25, require 85～90Kpa, temperature dry under 65 ℃～80 ℃ conditions in vacuum concentrate, pulverize, through 80 orders sieve green-tea extract;
B: get the clean sterculia seed and place the water retting 0.5～1 hour that adds 5～10 times in the extractor, heating is boiled and was kept 2 hours, obtains decocting liquid one time, filters through 80～200 mesh sieve cloth; Be heated to and boil 1～1.5 hour frying in shallow oil water that slag adds 3～5 times, get the secondary decocting liquid, filter through 100～200 mesh sieve cloth, twice decocting liquid merging left standstill, get the upper strata stillness of night and send in the concentration tank, under atmospheric pressure state, be concentrated into relative density 1.15～1.25, require 85～90Kpa, temperature dry under 65 ℃～80 ℃ conditions in vacuum concentrate, pulverize, through 80 orders sieve Scaphium scaphigerum extract;
C: Honegsukle flower P.E is identical with the Scaphium scaphigerum extract method;
D: white granulated sugar is crushed to 80～120 orders, in addition dextrin, vitamin C, citric acid is crushed to 60～100 orders respectively;
E: get green-tea extract, Scaphium scaphigerum extract, Honegsukle flower P.E, white granulated sugar, dextrin, vitamin C, citric acid by prescription, the edible alcohol that adds 60% (volume %) is as wetting agent, stir, granulate, after 50 ℃～60 ℃ dryings, add peppermint oil 20～100 mixings, compression moulding.
As preferably, green tea adopts selenium-rich green tea.
Below to prescription of the present invention according to elaborating:
Green tea: be the bud of Theaceae plant tea tree, leaf, tender stem, contain Tea Polyphenols in the tealeaves, catechin (EGCG), vitamin C and vitamin E, the phenols thing that spreads out, aromatic substance, amino acids material etc., also contain and enrich inorganic anticancer element, mainly contain selenium, molybdenum, manganese, germanium etc., can play nutrition health-care functions to human body, trace element in the tealeaves, material such as vitamin and Tea Polyphenols can suppress bacterium, removes free radical, suppress lipid peroxidation, also has the raising immunologic function, antitumor, reducing blood lipid, prevent effects such as atherosclerotic, result of the test shows, the tealeaves antistaphylohemolysin, streptococcus, Pseudomonas aeruginosa, proteus, shigella dysenteriae, Escherichia coli, effect obviously, in addition, the catechin of green tea has directly short proliferation function to lymphocyte, can obviously strengthen the NK cytoactive simultaneously, and green-tea extract can obviously suppress the mouse ear skin that TPA induces and produce red and swollen inflammatory reaction.In addition, more obvious as preferred selenium-rich green tea for the more common green tea of effect that improves body immunity.
The sterculia seed: be the mature seed of the Sterculiaceae plant sterculia seed, contain galacturonic acid, arabinose, galactolipin acetate, galactolipin, sterculin (sterculin), tragacanth sticking plain (bassorin) etc.Cold in nature, it is sweet, light to distinguish the flavor of.Energy clearing lung-heat heat, throat, gut purge defaecation.The traditional Chinese medical science is used for dry cough without phlegm, pharyngalgia hoarsen, chronic pharyngitis, constipation with heat retention more.Prove that through modern scientific research the sterculia seed has tangible anti-inflammatory, bactericidal action, can also increase mouse thymus weight and spleen weight, specific immune function is had facilitation.
Honeysuckle: be the caprifoliaceae plant dry flower of honeysuckle, the cold virtue clearly of Yin Qigan has clearing heat and detoxicating, effects such as detumescence makes eye bright, expelling wind and cold pathogens, also has in the appetizing again, the effect that detoxifcation is relieved inflammation or internal heat, the traditional Chinese medical science is used for controlling warm disease heating, temperature bloody flux, large carbuncle, pyogenic infections etc. more.Doctor trained in Western medicine studies have shown that have resisting pathogenic microbes, anti-inflammatory is analgesic, improve effects such as immunologic function.1200 meters of the five fingers mountain range, point mountain, Xinmi City, Henan, close honeysuckle flower original producton location described in the present invention ， Hai order.Honeysuckle includes wooden slippers straw colour element, inositol, biologicals such as tannic acid, go back protogene in a large number because of containing, so to staphylococcus, hemolytic streptococcus, typhoid bacillus, in conjunction with bacillus, pneumococcus, the toxin of secretions such as Escherichia coli has inhibitory action, macrophage phagocytic function is significantly improved, low macrophage antigen function is restored, pharmacological testing proof Honegsukle flower P.E can obviously reduce the swollen weight of rat granuloma, increase the phenol red excretion amount of mouse tracheae, and the ciliary movement of rabbit tracheae had obvious facilitation, at anti-inflammatory, the aspect of reducing phlegm effect is obvious.
Peppermint oil, English name PeppermintOil, for the bright cauline leaf of dicotyledon medicine Labiatae research plant peppermint or tame peppermint through distillable aromatic oil.For colourless oily liquids to faint yellow or green-yellow, pungent and refrigerant, strong scurrying property is arranged.Contain menthol (alcohols), thin what ester of acetic acid, carvone, jasmone, menthones, carvacrol, citrene, phellandrene etc., pungent in flavor and cool in property, return lung, Liver Channel, have the effect of wind and heat dispersing, can suppress the mucous membrane inflammation, eliminate implication, relieveing pain and refreshing.The evidence mint extract reacts to the rat carrageenan foot swelling, to the mouse acetic acid twisting all inhibitory action in various degree.Menthol has analgesia and antiinflammation.To staphylococcus aureus, beta hemolytic streptococcus, pneumococcus, corynebacterium diphtheriae, inhibitory action is arranged, dinitrofluorobenzene induced mice delayed allergy is not had obvious influence, think that these product have obviously antibacterial, anti-granulation hyperplasia, resolve phlegm effect.
Vitamin C: have height reducing substances and have oxidation resistant physiological action, be safeguard that body health promotes to grow with regulate the necessary organic compound of physiological function, strengthening immunologic function, promoting mineral matter element to absorb and promote playing an important role aspect the wound healing.Adding the vitamin purpose among the present invention is to improve body immunity, helps the function of moistening and cleaning throat of product better to bring into play.
Dextrin: English name Dextrin is to be raw material with starch, is being subjected to carrying out low in hydrolysis under heating, acid or the diastatic action, macromolecular starch at first transforms into micromolecular intermediate material, at this moment middle small-molecule substance, its dextrose equivalent (DE)＜20%, people just are called dextrin to it.Dextrin is the amorphous powder of white or off-white color, odorless, it is little sweet to distinguish the flavor of, and mainly as the filler of tablet, has good brew in pharmaceuticals industry, instant effective, taste just, thickening and emulsify well.Can well change properties of product, improve the quality of products.In the present invention, dextrin one is to use as bond, adhesive, can improve ratio of briquetting, in the shortening cycle, increases work efficiency; The 2nd, as stabilizing agent, dextrin toughness height, stability is also high.
The inventor thinks that bottleneck throat directly communicates with nature, all there is bacterium to exist under the normal condition, because of physics, chemical irritation or immunity degradation, bottleneck throat germ reproduction and causing a disease, bottleneck throat hyperemia, oedema, lymph foilicie hyperplasia appear, disease sees that pharynx is ached, itches, done, foreign body sensation etc., it is common frdquently encountered disease disease, therefore, should be to put prevention first, anti-inflammatory is loose bitterly on the one hand, on the one hand by improving body immunity, twice combinations are with the purpose that reaches the training source that consolidates, preventing and treating diseases, improves health conditions.For the affection of exogenous wind-heat type, the wind heat-clearing thereby product of the present invention can loose, secretion replenishing and throat moistening swelling and pain relieving; For lung stomach excess pattern of fever, product of the present invention clearly purging the lung of pathogenic fire heat with stomach fire, fire falls with yin-nourishing, decrease in interior for lung-kidney deficiency, lung kidney essense gas consumption, the throat illness of flaring up of deficient fire throat type, but the present invention's heat-clearing is moistened throat with yin-nourishing thereby go up, fall fiery anti-inflammatory, eliminate abscess of throat.
Therefore, the present invention has the prescription science, but both anti-inflammatory analgesics can improve body immunity again, strengthens resistance against diseases, and its method is simple and efficient, can keep characteristics such as each extract biologically active to greatest extent.
The specific embodiment
Below by embodiment, technical scheme of the present invention is described in further detail.
Embodiment: a: get 1000 portions of green tea and put the water retting 0.5 hour that adds 10 times in the extractor, heating is boiled and was kept 1 hour, obtains decocting liquid one time, filters through 100 mesh sieve cloth; Be heated to and boil 1 hour frying in shallow oil water that slag adds 3 times, get the secondary decocting liquid, filter through 120 mesh sieve cloth, twice decocting liquid merging left standstill, get the upper strata stillness of night and send in the concentration tank, under atmospheric pressure state, be concentrated into relative density 1.25, require 87Kpa, temperature dry under 65 ℃ of conditions in vacuum concentrate, pulverize, through 80 orders sieve green-tea extract;
B: get the clean sterculia seed and place the water retting 0.5 hour that adds 5 times in the extractor for 1000 parts, heating is boiled and was kept 2 hours, obtains decocting liquid one time, filters through 80 mesh sieve cloth; Be heated to and boil 1.5 hours frying in shallow oil water that slag adds 5 times, get the secondary decocting liquid, filter through 120 mesh sieve cloth, twice decocting liquid merging left standstill, get the upper strata stillness of night and send in the concentration tank, under atmospheric pressure state, be concentrated into relative density 1.25, require 87Kpa, temperature dry under 65 ℃ of conditions in vacuum concentrate, pulverize, through 80 orders sieve Scaphium scaphigerum extract;
C: Honegsukle flower P.E is identical with Scaphium scaphigerum extract consumption and method in this example;
D: white granulated sugar is crushed to 80 orders, in addition dextrin, vitamin C, citric acid is crushed to 60 orders respectively;
E: get green-tea extract, Scaphium scaphigerum extract, Honegsukle flower P.E, white granulated sugar, dextrin, vitamin C, citric acid by prescription, the edible alcohol that adds 60% (volume %) is as wetting agent, stir, granulate, after 60 ℃ of dryings, add peppermint oil 20 mixings, by every 0.5g compression moulding.
Product of the present invention is carried out animal experiment, set up basic, normal, high three dosage groups, 5,10,15 times of using the human body RD respectively, animal used as test is a cleaning level SD rat, and per os is given clothes 30 days continuously, and the 31st day once more to clothes, after causing inflammation, it is as follows to record data:
Buccal tablet is to the influence of animal toes thickness
Dosage Size of animal (only) Animal toes thickness (mm)
Before causing inflammation Cause scorching back 1 hour Cause scorching back 3 hours Cause scorching back 6 hours
0.00g/kg 10 4.18±0.42 6.26±0.38 7.22±0.23 6.89±0.28
0.25g/kg 10 4.13±0.27 6.1 5±0.26 7.03±0.45 6.93±0.36
0.50g/kg 10 4.14±0.28 5.76±0.27 6.54±0.29 6.44±0.25
1.50g/kg 10 4.17±0.26 5.56±0.30 6.29±0.26 6.18±0.28
Experimental result shows: buccal tablet of the present invention can obviously alleviate animal and cause 1,3, the 6 hour toes swelling degree in scorching back.
Product of the present invention is carried out human feeding trial, adopt the double blind control method, with 103 routine experimenters, clinical symptoms, pharyngeal sign are divided into test-meal group 51 examples and control group 52 examples at random, take buccal tablet and placebo respectively, every day 3 times, each 2.After 15 days, observed and recorded result, improvement rate X 2Check, calculate the back and obtain following data:
Pharyngeal clinical symptoms is improved situation
Symptom Control group improvement rate Test-meal group improvement rate
Pharyngalgia 27.27 69.57
Pharynx is itched 25.00 72.73
Dry throat 37.50 72.00
Dry cough 33.33 71.43
Foreign body sensation 38.46 58.33
Many speeches increase the weight of 40.00 60.00
Pharyngeal sign is improved situation
Symptom Control group improvement rate Test-meal group improvement rate
Myxedema 15.00 54.55
Mucous hyperemia 26.00 65.31
Lymphocytosis 26.67 64.52
Secretion adheres to 25.00 57.14
The result shows, buccal tablet to pharyngalgia, pharynx itch, dry throat, dry cough, foreign body sensation, many speeches increase the weight of etc., and pharyngeal clinical symptoms has clear improvement, pharyngeal signs such as lymph foilicie hyperplasia, secretion after pharyngeal mucosa oedema, mucous hyperemia, the pharynx adhere to are had clear improvement.
At last, should be pointed out that above embodiment only is the more representational example of the present invention.Obviously, technical scheme of the present invention is not limited to the foregoing description, and many distortion can also be arranged.All distortion that those of ordinary skill in the art can directly derive or associate from content disclosed by the invention all should be thought protection scope of the present invention.

Claims (3)

1. buccal tablet and preparation method thereof, described buccal tablet is made by functional component, filler, binding agent, acidity regulator, it is characterized in that described functional component is green-tea extract, Scaphium scaphigerum extract, Honegsukle flower P.E, peppermint oil and vitamin C, wherein said honeysuckle is the close honeysuckle flower that adopts Xinmi City, Henan to produce, described filler is a white granulated sugar, described binding agent is a dextrin, described acidity regulator is a citric acid, and described buccal tablet is counted by weight by following component and formed:
Green tea 500～1000 (the extract dry product is 75～150)
The sterculia seed 600～1200 (the extract dry product is 60～100)
Honeysuckle 200～600 (the extract dry product is 20～60)
Peppermint oil 20～100 vitamin Cs 25～150 white granulated sugars 100～500
Dextrin 100～400 citric acids 20～70.
2. a kind of buccal tablet according to claim 1 and preparation method thereof is characterized in that the preparation method of described buccal tablet comprises following steps:
A: get green tea and put the water retting 0.5～1.5 hour that adds 10～15 times in the extractor, heating is boiled and was kept 1 hour, obtains decocting liquid one time, filters through 100～200 mesh sieve cloth; Be heated to and boil 1～1.5 hour frying in shallow oil water that slag adds 3～5 times, get the secondary decocting liquid, filter through 100～200 mesh sieve cloth, twice decocting liquid merging left standstill, get the upper strata stillness of night and send in the concentration tank, under atmospheric pressure state, be concentrated into relative density 1.15～1.25, require 85～90Kpa, temperature dry under 65 ℃～80 ℃ conditions in vacuum concentrate, pulverize, through 80 orders sieve green-tea extract;
B: get the clean sterculia seed and place the water retting 0.5～1 hour that adds 5～10 times in the extractor, heating is boiled and was kept 2 hours, obtains decocting liquid one time, filters through 80～200 mesh sieve cloth; Be heated to and boil 1～1.5 hour frying in shallow oil water that slag adds 3～5 times, get the secondary decocting liquid, filter through 100～200 mesh sieve cloth, twice decocting liquid merging left standstill, get the upper strata stillness of night and send in the concentration tank, under atmospheric pressure state, be concentrated into relative density 1.15～1.25, require 85～90Kpa, temperature dry under 65 ℃～80 ℃ conditions in vacuum concentrate, pulverize, through 80 orders sieve Scaphium scaphigerum extract;
C: Honegsukle flower P.E is identical with the Scaphium scaphigerum extract method;
D: white granulated sugar is crushed to 80～120 orders, in addition dextrin, vitamin C, citric acid is crushed to 60～100 orders respectively;
E: get green-tea extract, Scaphium scaphigerum extract, Honegsukle flower P.E, white granulated sugar, dextrin, vitamin C, citric acid by prescription, the edible alcohol that adds 60% (volume %) stirs as wetting agent, granulate, after 50 ℃～60 ℃ dryings, add the peppermint oil mixing, compression moulding.
3. a kind of buccal tablet according to claim 1 and 2 and preparation method thereof, the green tea that it is characterized in that described preparation buccal tablet is selenium-rich green tea.
CN2007100688558A 2007-05-22 2007-05-22 Buccal tablet and its preparation method Active CN101053352B (en)

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Cited By (12)

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CN102308939A (en) * 2011-07-21 2012-01-11 宁国市亿邦生物科技有限公司 Litsea coreana sugar-free buccal tablet
CN101690531B (en) * 2009-10-13 2013-02-27 夏海龙 Fire-clearing cold-dispelling tea
CN103315292A (en) * 2013-05-20 2013-09-25 安徽天方茶业（集团）有限公司 Selenium-rich tea buccal tablets and preparation method thereof
CN103431098A (en) * 2013-09-11 2013-12-11 江苏丘陵地区镇江农业科学研究所 Method for preparing okra tea lozenges
CN103907717A (en) * 2014-03-31 2014-07-09 吴淑芬 Method for preparing green tea dew
CN105028864A (en) * 2015-06-30 2015-11-11 朱丹 Dark tea extract buccal tablets and preparation method thereof
CN106177190A (en) * 2016-08-15 2016-12-07 新疆环拓生物科技有限公司 A kind of guttural tablets and preparation method thereof
CN106804816A (en) * 2017-01-16 2017-06-09 广州大浦金医药科技有限公司 Tea buccal tablet and preparation method thereof
CN107125616A (en) * 2017-04-26 2017-09-05 合肥绿益食品有限公司 Beef ham is hyperchromic and color protecting method
CN107897422A (en) * 2017-12-06 2018-04-13 浙江东来药业有限责任公司 A kind of enzyme tea buccal tablet for protecting oral hygiene and preparation method thereof
CN108684915A (en) * 2018-04-03 2018-10-23 温州科技职业学院 A kind of yellow tea sugar-free low energy is without matrix chewing gum and preparation method thereof
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CN101690531B (en) * 2009-10-13 2013-02-27 夏海龙 Fire-clearing cold-dispelling tea
CN102308939A (en) * 2011-07-21 2012-01-11 宁国市亿邦生物科技有限公司 Litsea coreana sugar-free buccal tablet
CN103315292A (en) * 2013-05-20 2013-09-25 安徽天方茶业（集团）有限公司 Selenium-rich tea buccal tablets and preparation method thereof
CN103431098A (en) * 2013-09-11 2013-12-11 江苏丘陵地区镇江农业科学研究所 Method for preparing okra tea lozenges
CN103907717A (en) * 2014-03-31 2014-07-09 吴淑芬 Method for preparing green tea dew
CN103907717B (en) * 2014-03-31 2015-10-14 桂林融通科技有限公司 A kind of preparation method of green tea dew
CN105028864A (en) * 2015-06-30 2015-11-11 朱丹 Dark tea extract buccal tablets and preparation method thereof
CN105028864B (en) * 2015-06-30 2018-10-30 朱丹 A kind of black tea extract buccal tablet and preparation method thereof
CN106177190A (en) * 2016-08-15 2016-12-07 新疆环拓生物科技有限公司 A kind of guttural tablets and preparation method thereof
CN106804816A (en) * 2017-01-16 2017-06-09 广州大浦金医药科技有限公司 Tea buccal tablet and preparation method thereof
CN107125616A (en) * 2017-04-26 2017-09-05 合肥绿益食品有限公司 Beef ham is hyperchromic and color protecting method
CN107897422A (en) * 2017-12-06 2018-04-13 浙江东来药业有限责任公司 A kind of enzyme tea buccal tablet for protecting oral hygiene and preparation method thereof
CN108684915A (en) * 2018-04-03 2018-10-23 温州科技职业学院 A kind of yellow tea sugar-free low energy is without matrix chewing gum and preparation method thereof
CN111616365A (en) * 2020-07-03 2020-09-04 广州市博卡利生物科技研究所 Preparation method of refreshing liquid acting on central nerves

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