CN101049106A - Oil preparation for trapping and killing cockroach by natural pyrethrum element and preparation method - Google Patents
Oil preparation for trapping and killing cockroach by natural pyrethrum element and preparation method Download PDFInfo
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- CN101049106A CN101049106A CN 200710089944 CN200710089944A CN101049106A CN 101049106 A CN101049106 A CN 101049106A CN 200710089944 CN200710089944 CN 200710089944 CN 200710089944 A CN200710089944 A CN 200710089944A CN 101049106 A CN101049106 A CN 101049106A
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- cockroach
- finish
- natural pyrethrum
- oil
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Abstract
A natural pyrethrin oil as an attractant for killing roach, termite and ant is proportionally prepared from natural pyrethrin, vegetative or chemical synergist, penetrant, stabilizer and solvent. Its preparing process is also disclosed.
Description
Technical field
The present invention relates to insecticide, specifically cockroach by natural pyrethrum element trapping finish and preparation method.
Technical background
It is with a long history that natural pyrethrum is used for the control of sanitary insect pest, how based on control mosquito, flea, louse, and how occurs with the formulation of bait, canned aerosol, pulvis.And the chemical organic solvent of the many employings of aerosol solvent, contaminated environment, packing cost is high.Yet there are no the report that is used for cockroach prevention and cure with natural pyrethrum and vegetable oil preparation cockroach trapping finish.
Summary of the invention
The purpose of this invention is to provide a kind of easy degraded, environmentally friendly, to the cockroach by natural pyrethrum element of human body safety trapping finish and preparation method.
Technical scheme of the present invention is: prepare with following raw material:
Used natural pyrethrum is the pyrethrin refined oil, preparing per 100 gram cockroach trapping finish pyrethrum cellulose contents is (0.1-10) %, and synergist is the synthetic synergist of plant resource synergist or chemical industry, and the plant resource synergist is sesamin and citrene, sesamin (Asarinin, [sesamin] C
20H
18O
6) addition be pyrethrin content 1-5 doubly, the citrene addition be pyrethrin content 1-10 doubly, the synthetic synergist of chemical industry has piperonyl butoxide (PBO, 3,4-methylene-dioxy-6-n-pro-pyl benzyl normal-butyl tirethylene glycol ether, C
19H
30O
5) and synergy phosphorus (SV, O, O-diethyl-O-phenyl thiophosphate, C
10H
15O
3PS), addition is pyrethrin content 1-10 times; Bleeding agent is the solubility azone, and addition is 2% of a total amount; Stabilizing agent is plant resource stabilizing agent or the agent of chemical industry synthesizing stable, the plant resource stabilizing agent is a rosemary,, and addition is 2% of a pyrethrum cellulose content, and solvent is a vegetable oil, sesame oil, palm oil, rapeseed oil, anise-oil (belong to amomum tsaoko leaf and extract hair oil) are arranged, select one of them to add capacity as required.Selected solvent is a cockroach happiness edible oil material, can strengthen the control efficiency to cockroach,
The preparation method:
1. take by weighing the pyrethrin essential oil according to quantity and place beaker;
2. piperonyl butoxide is poured in the beaker, fully mixing and stirring;
3. again antioxidant BHT is poured in the beaker, fully mixing and stirring;
4. again azone is poured in the beaker, fully mixing and stirring;
5. add anise-oil again and stir, get final product to such an extent that cockroach by natural pyrethrum element is trapped and killed finish.
Above institute all prepares in steps at normal temperatures.Above step is followed in preparation equally in preparing tank, under continuous stirring condition, adds each batching one by one every 10 minutes.
The present invention fills a prescription and adopts natural pyrethrum, cockroach happiness food vegetable oil to make solvent, natural synergic agent, stabilizing agent, to the warm blooded animal low toxicity, easily degraded in natural environment, not only can improve drug effect but also avoided of the pollution of chemical organic solvent, guarantee safety largely human body to living environment.Prove through repetition test: cockroach by natural pyrethrum element trapping finish is sprayed to the cockroach place of often haunting with spray pattern to have and tags, trap and kill cockroach, and the while finish also has good control efficiency to many kinds of ants such as termite, silky ants; This spray droplet range of scatter is wide, and the trapping scope is wide, and the cockroach effect of going out can reach more than 80%.
Using method:
Cockroach by natural pyrethrum element trapping finish uses common plastics bottle, Aluminum Bottle splendid attire, adds the Manual pressure nozzle, under Manual pressure with reagent spray to the place that cockroach often haunts, tag, trap and kill cockroach.And canned aerosol is to lean on the effect of propellant to reach spraying deinsectization effect.When finding to have cockroach movable, cockroach by natural pyrethrum element is trapped and killed finish be sprayed to the place that cockroach may often haunt, as below corner, the table end, the sofa etc., if conditions permit is kept quite after spraying, dull thread, then effect is better.
The result is as follows for its toxicity test:
The result: the record death toll, obtain lethality, with probability value analysis software, try to achieve the confidence interval of LC50 and 95%.
Using spss software and carry out regression analysis, obtain equation of linear regression Y=3.2574X-8.7733, is 493.5351ug/ml to the half lethal concentration LC50 of cockroach.95% confidence interval is 260.6638-909.6895ug/ml.
Table one cockroach by natural pyrethrum element trapping finish kills the cockroach test data sheet
| Concentration (concentration logarithm) | Average weight (g) | The 24h death toll | The 48h death toll | The 48h average mortality | ||
| 50 times of concentration one dilutions | 1000ug/ml (3.00) | I | 0.2735 | 8 | 9 | |
| II | 0.2355 | 10 | 10 | 93.3％ | ||
| III | 0.2541 | 9 | 9 | |||
| 75 times of concentration two dilutions | 667ug/ml (2.82) | I | 0.2799 | 5 | 6 | |
| II | 0.2448 | 6 | 7 | 63.3％ | ||
| III | 0.2548 | 6 | 6 | |||
| 100 times of concentration three dilutions | 500ug/ml (2.70) | I | 0.2686 | 3 | 4 | |
| II | 0.2391 | 3 | 4 | 36.7％ | ||
| III | 0.2451 | 3 | 3 | |||
| 300 times of concentration four dilutions | 170ug/ml (2.20) | I | 0.2459 | 2 | 2 | |
| II | 0.2870 | 0 | 1 | 13.3％ | ||
| III | 0.2634 | 1 | 1 | |||
| 500 times of concentration five dilutions | 100ug/ml (2.00) | I | 0.2713 | 0 | 0 | |
| II | 0.2396 | 0 | 0 | 0 | ||
| III | 0.2561 | 0 | 0 | |||
| The clear water contrast | I | 0.2434 | 0 | 0 | ||
| II | 0.2576 | 0 | 0 | 0 | ||
| III | 0.2548 | 0 | 0 |
Embodiment
Embodiment 1:
Preparation 100 grams 1% cockroach by natural pyrethrum element trapping finish.
1. take by weighing 2 gram pyrethrin essential oils (pyrethrin content is 50%) and place beaker;
2. take by weighing 5 gram piperonyl butoxides and pour in the beaker, stir;
3. take by weighing 0.02 gram rosemary, and pour in the beaker, stir;
4. take by weighing 2 gram solubility azones and pour in the beaker, stir;
5. take by weighing 90.98 gram anise-oils again and pour in the beaker, stir, get final product to such an extent that 1% cockroach by natural pyrethrum element is trapped and killed finish.
Above institute all prepares in steps at normal temperatures.Above step is followed in preparation equally in preparing tank, under continuous stirring condition, adds each batching one by one every 10 minutes.
Embodiment 2:
Preparation 100 grams 0.1% cockroach by natural pyrethrum element trapping finish.
1. take by weighing 0.2 gram pyrethrin essential oil (pyrethrin content is 50%) and place beaker;
2. take by weighing 0.5 gram sesamin and pour in the beaker, stir;
3. take by weighing 0.002 rosemary, gram and pour in the beaker, stir;
4. take by weighing 2 gram solubility azones and pour in the beaker, stir;
5. take by weighing 97.298 gram rapeseed oils again and pour in the beaker and stir, get final product 0.1% cockroach by natural pyrethrum element trapping finish.
Embodiment 3:
Preparation 100 grams 10% cockroach by natural pyrethrum element trapping finish.
1. take by weighing 20 gram pyrethrin essential oils (pyrethrin content is 50%) and place beaker;
2. take by weighing 50 gram citrenes and pour in the beaker, stir;
3. take by weighing 0.2 gram rosemary, and pour in the beaker, stir;
4. take by weighing 2 gram solubility azones and pour in the beaker, stir;
5. take by weighing 27.8 gram palm oils again and pour in the beaker, stir, get final product to such an extent that 10% cockroach by natural pyrethrum element is trapped and killed finish.
Above institute all prepares in steps at normal temperatures.Above step is followed in preparation equally in preparing tank, under continuous stirring condition, adds each batching one by one every 10 minutes.
Claims (6)
1. a cockroach by natural pyrethrum element is trapped and killed finish, it is characterized in that making with following materials of weight proportions: the content of natural pyrethrum is the 0.1%-10% of total amount, the 1-10 that the synthetic synergist of plant resource synergist or chemical industry is a pyrethrin doubly, bleeding agent is the 1-2% of pyrethrum cellulose content, stabilizing agent is the 1-2% of pyrethrum cellulose content, and solvent supplies 100%.
2. cockroach by natural pyrethrum element trapping finish according to claim 1 is characterized in that the plant resource synergist is sesamin and citrene, synthetic synergist piperonyl butoxide of chemical industry or synergy phosphorus.
3. cockroach by natural pyrethrum element trapping finish according to claim 1 is characterized in that the plant resource stabilizing agent is a rosemary.
4. cockroach by natural pyrethrum element trapping finish according to claim 1 is characterized in that bleeding agent is the solubility azone.
5. cockroach by natural pyrethrum element trapping finish according to claim 1 is characterized in that solvent is a vegetable oil, i.e. sesame oil, palm oil, rapeseed oil, anise-oil.
6. the described cockroach by natural pyrethrum element of claim 1 is trapped and killed the main method of preparation of finish, it is characterized in that carrying out according to the following steps:
1) takes by weighing the pyrethrin essential oil according to quantity and place beaker;
2) synergist is poured in the beaker, stirred;
3) again stabilizing agent is poured in the beaker, stirred;
4) again bleeding agent is poured in the beaker, stirred;
5) it is even to add the plant resource stirring solvent again, get final product cockroach by natural pyrethrum element trapping finish;
Above institute all prepares in steps at normal temperatures, under continuous stirring condition, adds each batching one by one every 10 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200710089944 CN101049106A (en) | 2006-11-14 | 2007-03-22 | Oil preparation for trapping and killing cockroach by natural pyrethrum element and preparation method |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200610048813.3 | 2006-11-14 | ||
| CN200610048813 | 2006-11-14 | ||
| CN 200710089944 CN101049106A (en) | 2006-11-14 | 2007-03-22 | Oil preparation for trapping and killing cockroach by natural pyrethrum element and preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101049106A true CN101049106A (en) | 2007-10-10 |
Family
ID=38780880
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200710089944 Pending CN101049106A (en) | 2006-11-14 | 2007-03-22 | Oil preparation for trapping and killing cockroach by natural pyrethrum element and preparation method |
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|---|---|
| CN (1) | CN101049106A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101999349A (en) * | 2010-12-21 | 2011-04-06 | 广东省昆虫研究所 | D-limonene-containing mixed oil agent for killing solenopsis invicta buren and method for killing the solenopsis invicta buren |
| CN104247722A (en) * | 2014-05-30 | 2014-12-31 | 馥稷生物科技发展（上海）有限公司 | Insecticide mate and preparation method thereof |
| CN105123776A (en) * | 2015-09-18 | 2015-12-09 | 广东省昆虫研究所 | Insecticide with high-content pyrethrin |
| CN106818840A (en) * | 2017-01-05 | 2017-06-13 | 广州翼鲲环境科技有限公司 | A kind of cockroach bait and preparation method thereof |
| CN106942304A (en) * | 2017-04-11 | 2017-07-14 | 安徽省明美矿物化工有限公司 | A kind of concave convex rod ant killing agent and preparation method thereof |
| CN111226961A (en) * | 2020-03-27 | 2020-06-05 | 成都市房屋安全事务中心(成都市白蚁防治研究中心) | Environment-friendly termite killing preparation |
| CN113519507A (en) * | 2021-06-21 | 2021-10-22 | 广州阿佩斯康生物科技有限公司 | Plant oil for ultra-low-capacity spraying and insect killing of unmanned aerial vehicle |
-
2007
- 2007-03-22 CN CN 200710089944 patent/CN101049106A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101999349A (en) * | 2010-12-21 | 2011-04-06 | 广东省昆虫研究所 | D-limonene-containing mixed oil agent for killing solenopsis invicta buren and method for killing the solenopsis invicta buren |
| CN101999349B (en) * | 2010-12-21 | 2013-02-27 | 广东省昆虫研究所 | D-limonene-containing mixed oil agent for killing solenopsis invicta buren and method for killing the solenopsis invicta buren |
| CN104247722A (en) * | 2014-05-30 | 2014-12-31 | 馥稷生物科技发展（上海）有限公司 | Insecticide mate and preparation method thereof |
| CN105123776A (en) * | 2015-09-18 | 2015-12-09 | 广东省昆虫研究所 | Insecticide with high-content pyrethrin |
| WO2017045268A1 (en) * | 2015-09-18 | 2017-03-23 | 广东省生物资源应用研究所 | Insecticide with high content of pyrethrin |
| CN105123776B (en) * | 2015-09-18 | 2019-03-08 | 广东省生物资源应用研究所 | A kind of high-content pyrethrin insecticide |
| CN106818840A (en) * | 2017-01-05 | 2017-06-13 | 广州翼鲲环境科技有限公司 | A kind of cockroach bait and preparation method thereof |
| CN106942304A (en) * | 2017-04-11 | 2017-07-14 | 安徽省明美矿物化工有限公司 | A kind of concave convex rod ant killing agent and preparation method thereof |
| CN111226961A (en) * | 2020-03-27 | 2020-06-05 | 成都市房屋安全事务中心(成都市白蚁防治研究中心) | Environment-friendly termite killing preparation |
| CN113519507A (en) * | 2021-06-21 | 2021-10-22 | 广州阿佩斯康生物科技有限公司 | Plant oil for ultra-low-capacity spraying and insect killing of unmanned aerial vehicle |
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