CN101028062A - Functional sweetener, its production and use - Google Patents
Functional sweetener, its production and use Download PDFInfo
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- CN101028062A CN101028062A CNA2007100958453A CN200710095845A CN101028062A CN 101028062 A CN101028062 A CN 101028062A CN A2007100958453 A CNA2007100958453 A CN A2007100958453A CN 200710095845 A CN200710095845 A CN 200710095845A CN 101028062 A CN101028062 A CN 101028062A
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Abstract
A functional sweetening agent with low (or no) content of saccharide and low caloricity and used in food, beverage, sweets, dairy products and health-care food for the patients of diabetes, obesity and decayed tooth is composed of trichlorosucrose and the natural auxiliary extracted from cone, rice, plant and water-soluble plant fibers in mass ratio of (0.5-10): (99.5-90). Its preparing process is also disclosed.
Description
Technical field
The present invention relates to food, beverage and functional health product technical field.Be specifically related to a kind of sugar-free, do not have heat, anticariogenic functional sweetener and its production and application.
Background technology
Sucralose (Sucralose, molecular formula C
12H
19O
8Cl
3Molecular weight is 397.64) be to be a kind of non-nutritive intense sweetener that raw material makes through chloro with sucrose, its chemistry is by name 4,1 ', 6 '-three chloro-4,1 ', 6 '-three deoxidation gala type sucrose are a kind of white powder products, very easily water-soluble (solubility 28.2 grams, 20 ℃), aqueous solution clear, its sugariness is 400-800 a times of sucrose.Sucralose has following advantage: (1) chemistry of aqueous solution good stability, sweet taste is constant under the high temperature, and with food in main components such as protein pectin chemically reactive not, sugariness is more stable in baking technology; (2) have no side effect, be absorbed hardly in human body, calorie value is zero, is diabetes patient's sweet taste substitute; (3) sweet taste is pure, and the same with sucrose do not have offending bitter aftertaste and other strange taste, and it is not utilized by the carious tooth germ, so can not cause carious tooth.
Yet,, very inconvenient in industrial direct use because the sugariness of Sucralose is high, operation control is very difficult, even very easily cause microcomponent is arranged in the air, and mouth and nose can feel for a long time that all sweet taste is excessive, holdup time is very long, causes that people's sense of taste is in the state of " sweet " all the time.If after the hand contact, all can cause and where run into, sweet everywhere, contact these article later on again, all can feel the sensation of " sweet ", for a long time be stuck with the pollution of " sweet ".So industrial direct use, to the assurance of consumption, the control of sugariness is all very inconvenient.
Thereby needing a kind of novel sweetener, it can keep the original sugar-free of Sucralose, not have the advantage of heat, no carious tooth, can solve industrial to reach inconvenient and " sweet " pollution problems of use in the daily life again.
Summary of the invention
The objective of the invention is to overcome above-mentioned " sweet " pollution, industrial use very difficult control consumption and sugariness, and use extremely inconvenient problem in the actual daily life, and provide that a kind of consumption is convenient, operation is controlled, taste with usage is similar to sucrose, sweet taste is pure, sugariness moderate controlled, do not have (low) sugar, nothing (low) heat, an anticariogenic functional sweetener.
According to above-mentioned purpose of the present invention, the invention provides following technical proposals:
A kind of functional sweetener, it comprises Sucralose and natural products auxiliary material.
In one embodiment of the invention, described Sucralose and natural products auxiliary material are equally distributed in sweetener.
In one embodiment of the invention, described functional sweetener is solid (an especially granule), liquid, or gelinite.
In one embodiment of the invention, the mass ratio of the Sucralose of described sweetener and natural products auxiliary material is 0.25: 99.75 to 28.2: 71.8, preferred 0.5: 99.5 to 15: 85, more preferably 0.8: 99.2 to 10.0: 90.0, further preferred 1.0: 99.0 to 5.0: 95.0.
In one embodiment of the invention, described natural products auxiliary material is selected from hydrolysate, fermentate and/or the extract of grain; In water-soluble natural plant extracts and the water-solubility vegetable fibres one or more.Described grain comprises rice, corn, oat, potato, buckwheat, soybean, soya bean etc.Described water-solubility vegetable fibres comprises edible water-soluble fibres such as green tea water-soluble fibre, corn water-soluble fibre, fruit water-soluble fibre, vegetables water water-soluble fibre, soybean water-soluble fiber, rice water-soluble fibre, konjaku water solutable fiber; Described fruit water-soluble fibre comprises apple water-soluble fibre, banana oil soluble fiber, strawberry water-soluble fibre, watermelon water-soluble fibre, pawpaw water-soluble fibre, mango water-soluble fibre, hawthorn water-soluble fibre etc.
In one embodiment of the invention, the hydrolysate of described rice, fermentate and/or extract comprise paddy rice polyphenol, water-soluble rice protein etc.
In one embodiment of the invention, the hydrolysate of described corn, fermentate and/or extract comprise for example maltodextrin, Dextrose Monohydrate, microcrystalline cellulose, beta-schardinger dextrin-etc.
In one embodiment of the invention, the composition of described water-solubility vegetable fibres can be selected from one or more in pectin, natural plant gum, resin, polydextrose, arabogalactan, araban, galactan, galactan aldehydic acid, araboxylan, wood sugar glucose, glycoprotein, cellulose, lignin and the derivative thereof.
In one embodiment of the invention, described sweetener contains equally distributed natural food colour, the mass ratio of the gross mass of described natural food colour and Sucralose and natural products auxiliary material is 0.001: 99.999 to 0.05: 99.95, preferred 0.002: 99.998 to 0.02: 99.98, more preferably 0.005: 99.995 to 0.01: 99.99.Described natural food colour can be selected from one or more in chlorophyll, carrotene, lycopene, lutein, kaoliang color, chrysanthemum flavine, carthamin and the analog etc.Described even distribution is meant that natural food colour is equally distributed in sweetener.
In one embodiment of the invention, described sweetener contains equally distributed natural flavouring, the mass ratio of the gross mass of described natural flavouring and Sucralose and natural products auxiliary material is 0.001: 99.999 to 0.05: 99.95, preferred 0.002: 99.998 to 0.02: 99.98, more preferably 0.005: 99.995 to 0.01: 99.99.Described natural flavouring can be selected from one or more in lemon, banana, apple, strawberry, vanilla, cloves, tsaoko, orange peel, Bai Zang, peppermint, nutmeg, basyleave, semen armeniacae amarae, Herba Lycopi's perfume (or spice), storax and the analog etc.
In one embodiment of the invention, the sugariness scope of described functional sweetener is 0.5-170 a times of sucrose sweetness, and preferred 1.5-60 times, more preferably 3-10 doubly.
In one embodiment of the invention, the bulk density of described sweetener is 0.1g/mL-0.75g/mL, preferred 0.15g/mL-0.55g/mL.
According to purpose of the present invention, also provide the method for the described sweetener of following preparation:
A kind of preparation method of sweetener according to the present invention, adopt dry granulation technology: the natural products auxiliary material and the Sucralose of described mass ratio are pulverized through Highefficientpulverizer, mix after crossing about 100 mesh sieves, place the dry granulation machine, adjust pressure and engine speed, select suitable screen cloth to make the compacting granulating, promptly through the whole grain of 20-100 order shaking screen;
In one embodiment of the invention, in the step of described natural products auxiliary material of the mixing of above-mentioned dry granulation technology and Sucralose, also add described natural food colour and/or natural flavouring.
This method can adopt cycle type dry press or drum-type dry press to finish, and can directly suppress, and need not moistening, dry run.Gained even particle size, bulk density be big, be difficult for scattering or attached in the environment, having reduced the aerial residence time of Sucralose.
A kind of preparation method of functional sweetener comprises the following steps: according to the present invention
(1) dissolving of Sucralose: in temperature is 5 ℃-45 ℃, preferred 10 ℃-35 ℃, more preferably under 15 ℃-30 ℃, Sucralose is dissolved in the water as wetting agent, and to make its concentration range be that 0.25 quality % (w/w) is to saturated concentration (for example being 28.2 quality % under 25 ℃), preferred 0.5 quality %-20 quality %, more preferably 1 quality %-10 quality %; And
(2) granulate, described method of granulating can be selected from wet granulation, fluidized granulation and spray-drying process.
In one embodiment, described granulation step adopts wet granulation technology:
The natural products auxiliary material is pulverized through Highefficientpulverizer, after crossing about 100 mesh sieves, place wet mixing pelletizer, add wetting agent (aqueous solution of sucrose trichloride) and stir the system softwood, make Sucralose evenly attached on the natural products auxiliary material, granulate 55-75 ℃ of heated-air drying through the 20-40 mesh sieve, with the whole grain of 20 orders-100 order shaking screen, promptly get the granule of the uniform functional sweetener of the present invention that distributes;
In one embodiment of the invention, in above-mentioned wet-mixing granulating process, before adding aqueous solution of sucrose trichloride, also be included in and add described natural food colour and/or natural flavouring in the described natural products auxiliary material, and the step that mixes.
A kind of preparation method of sweetener according to the present invention, adopt fluidized granulation technology:
Sucralose is dissolved in the water under 5 ℃ to 45 ℃, forms the aqueous solution of 0.5 quality % to saturated concentration; The raw material of natural products auxiliary material is pulverized through Highefficientpulverizer, crossed about 100 mesh sieves, place the fluidized granulation machine, EAT 80-100 ℃; Leaving air temp reaches 25-35 ℃, and fluidized granulation with the whole grain of 20 orders-100 order shaking screen, promptly gets the flakes granule of the uniform sweetener of the present invention that distributes;
In one embodiment of the invention, in above-mentioned fluidized granulation technology, before fluidized granulation, also be included in and add described natural food colour and/or natural flavouring in the described natural products auxiliary material, and the step that mixes.
This method is mixed, granulation, dry goes on foot and finishes.Particle forms under the state of boiling, surperficial rounding, good fluidity, uniformity height, and production process is difficult for polluting, and is difficult for scattering or attached in the environment, having reduced the aerial residence time of Sucralose.End product quality can better be guaranteed.
A kind of preparation method of sweetener according to the present invention, adopt spray-drying process technology:
Sucralose and natural products auxiliary material are dissolved in the water EAT 160-200 ℃ under 5 ℃ to 60 ℃; Leaving air temp 60-80 ℃, spraying granulation with the whole grain of 20 orders-100 order shaking screen, promptly gets the granule of the uniform sweetener of the present invention that distributes;
In one embodiment of the invention, in above-mentioned spray-drying process technology, before spraying granulation, also be included in and add described natural food colour and/or natural flavouring in the described natural products auxiliary material, and the step that mixes.
The particle that this method makes is loose porous, except that the advantage with fluidized granulation, is more suitable for the low product of Sucralose content.
According to purpose of the present invention, a kind of food additives also are provided, described food additives contain sweetener of the present invention.Described food additives also can contain other supplementary element.
Functional sweetener of the present invention can be with the form of pure sweetener, and the form of for example pure Sucralose and pure natural product auxiliary material provides, and also can provide with the form of adding pigment and/or spices more in addition, can also provide to contain forms such as other additive in addition.
Thereby, the invention provides that a kind of consumption is convenient, operation is controlled, sugariness moderate controlled, do not have (low) sugar, do not have (low) heat, anticariogenic multi-functional sweetener.The multi-functional sweetener of the present invention (relax can sugared Sucrapure ) can be widely used in the industrial products such as food additives, food, beverage, functional drink, candy, dairy products, health products, in the especially various food additives.The multi-functional sweetener mouthfeel of the present invention is good, is easy to preservation, and using method and sucrose are just the same, and taste is similar to sucrose, but does not have the side effect of the high sugar of sucrose, high heat, thus go for diabetes patient, adiposis patient, and the carious tooth patient's is edible.And, can use different natural products auxiliary materials as main carrier or use several different carriers according to the use of difference in functionality.
The preparation method of functional sweetener of the present invention has following characteristics: 1. each step preparation process yield is high; 2. the yield rate for preparing gained is up to more than 99%; 3. preparation condition is very easily controlled grasp; 4. employed equipment cost is lower in the preparation process; 5. production process does not have any environmental pollution.Therefore the inventive method especially is suitable for industrialized production.
Description of drawings
The present invention is described further below with reference to accompanying drawings, wherein:
Fig. 1 is the dry granulation process chart according to the preparation method of functional sweetener of the present invention;
Fig. 2 is the wet granulation technology flow chart according to the preparation method of functional sweetener of the present invention;
Fig. 3 is the fluidized bed granulation process chart according to the preparation method of functional sweetener of the present invention;
Fig. 4 is the spray-drying process process chart according to the preparation method of functional sweetener of the present invention.
The specific embodiment
In the embodiment illustrated, the model of Highefficientpulverizer is the 30B type, and the manufacturer is magnificent drying equipment Co., Ltd for Changzhou shakes; The model of wet mixing pelletizer is GHL-250, and the manufacturer is magnificent drying equipment Co., Ltd for Changzhou shakes; The model of dry granulation machine is GK-70, and the manufacturer is a Jiangsu rarity group; The model of fluidized granulation machine is LBF-90, and the manufacturer is good granulation drying equipment of a Changzhou Co., Ltd; The model of spray-drying pelleting machine is YPG-100, and the manufacturer is Changzhou Meng He pharmaceutical machine Co., Ltd.
Sweetener of the present invention is generally solid, especially graininess; Certainly, it also can be liquid, colloid or other form.Natural products auxiliary material of the present invention is all from natural products, and for example therefore grain, fruit, vegetables etc. all are edible, promptly can be edible as the auxiliary material of food additives or food, and can be not harmful.In fact, described edible natural products auxiliary material can be the natural products in any source, as long as it is harmless, solvable, suitablely be prepared into even product with Sucralose.These auxiliary materials can be the forms of pure compound, also can be the forms of mixture.
Preferably, Sucralose and natural products auxiliary material are evenly distributed in the sweetener of the present invention.When additionally adding additives such as natural food colour and/or natural flavouring when sweetener of the present invention, these additives preferably also are to be evenly distributed in the sweetener of the present invention.This be evenly distributed with to be beneficial to make product quality keep stable, and realize as the function of the described sweetener of the object of the invention, for example make sweetener more be not easy to volatilize.This even distribution is the even distribution of basic molecular level preferably, and for example Sucralose and natural products auxiliary material molecule are evenly distributed in the sweetener, make sweetener become the phase (as solid phase, liquid phase or gel phase) of homogeneous.Certainly, Sucralose of the present invention and natural products auxiliary material also can be used as trickle uniform particles and are distributed in the sweetener of the present invention, as long as can realize the object of the invention.
Embodiment 1: through dry granulation technology
To pulverize through Highefficientpulverizer, and cross 99kg natural products auxiliary material behind 100 mesh sieves and 1kg Sucralose and 0.1kg natural food colour, the 0.1kg natural flavouring mixes; put dry granulation machine (the 16-24 eye mesh screen is housed); adjustment pressure is 5Mpa; the velocity of rotation of main frame is 600rpm; select suitable screen cloth to make the compacting granulating; through the whole grain of 20-100 order; promptly get the granule that dry granulation forms the sweetener of the present invention that is evenly distributed; its sugariness is 4.5 times of sucrose, and bulk density is 0.48g/ml.
Embodiment 2: through wet granulation technology
In the aseptic rustless steel container of drying, the 3kg Sucralose fully is dissolved in pure (but all food-grade water) water, its solution temperature is controlled at about 40 ℃; The concentration of aqueous solution of sucrose trichloride is controlled at about 20%, as wetting agent.
97kg natural products auxiliary material is pulverized through Highefficientpulverizer; after crossing 100 mesh sieves; put wet mixing pelletizer; after mixing with 0.1kg natural food colour and 0.1kg natural flavouring; add wetting agent (aqueous solution of sucrose trichloride) and stir the system softwood; evenly attached on the carriers such as natural products auxiliary material and natural flavouring, natural food colour; granulate through the 20-40 mesh sieve; 55-75 ℃ of heated-air drying; the whole grain of 20 orders-100 order shaking screen promptly gets the granule that wet granulation forms the sweetener of the present invention that is evenly distributed.The sugariness of the sweetener of gained is 9 times of sucrose, and bulk density is 0.35g/ml.
Embodiment 3: through fluidized granulation technology
In the aseptic rustless steel container of drying, Sucralose 0.75kg fully is dissolved in the pure water, its solution temperature is controlled at about 40 ℃; The concentration of aqueous solution of sucrose trichloride is controlled at about 0.5%.
The raw material of natural products auxiliary material 49.25kg is pulverized through Highefficientpulverizer, crossed 100 mesh sieves, place the fluidized granulation machine, mix EAT 80-100 ℃ with natural food colour and natural flavouring; Leaving air temp reaches 25-35 ℃, fluidized granulation, and the whole grain of 20 orders-100 order shaking screen promptly gets the flakes granule of the uniform sweetener of the present invention that distributes.The sugariness of the sweetener of gained is 6 times of sucrose, and bulk density is 0.3g/ml.
Embodiment 4: through fluidized granulation technology
Sucralose 2.5kg fully is dissolved in the pure water, and its solution temperature is controlled at about 40 ℃; The concentration of aqueous solution of sucrose trichloride is controlled at about 2.5%.
Get the water-solubility vegetable fibres 47.5kg that crosses the 80-120 eye mesh screen, put in the fluidized granulation machine, add natural food colour 0.1kg and natural food colour spices 0.1kg mixing 3-5 minute.Set phase voltage 400V, air-introduced machine electric current 18A, EAT 60-80 ℃.Reach 25-35 ℃ Deng leaving air temp, open the peristaltic pump driver, rotational speed regulation is changeed to about 15-35, and the atomizing of beginning sucralose solution is pressed into: preceding 10 kilograms of 0.3MPa, rotational speed regulation is adjusted rotating speed according to leaving air temp for preceding 10 kilograms.Air intake 60-80 ℃, air-out keeps 25-35 ℃, and air door opens 4/5.The back transfers to 65-85 ℃ to air intake for 10 kilograms, and air-out keeps 32-38 ℃.Air door is carried out (all opening).Atomizing pressure is big (0.8MPa) as far as possible.If differ from 5 kilograms when having sprayed, certain whitewashing leaving air temp that guarantees waits when having sprayed like this at 30 ℃ (accent low-rotate speeds), sprays a lower nozzle (in order to avoid pipe obstruction) with a small amount of purified water.EAT is adjusted to 50 ℃, just can closes heating.Because waste heat, leaving air temp can be buffered to 40-45 ℃.Naturally being cooled to then just can discharging below 30 ℃.If when having sprayed, leaving air temp has only 38-39 ℃, will close heating a little later like this, abdicates and closes heating when the wind-warm syndrome degree is raised to more than 40 ℃ again.The whole grain of 20 orders-100 order shaking screen promptly gets the flakes granule that fluidized granulation forms the sweetener of the present invention that is evenly distributed.The sugariness of the sweetener of gained is 18 times of sucrose, and bulk density is 0.28g/ml.
Embodiment 5: spray-dried granulation
In the aseptic rustless steel container of drying, 1.5kg Sucralose, natural products auxiliary material 98.5kg are dissolved in the pure water, its solution temperature is controlled at about 60 ℃.
EAT 160-200 ℃; Leaving air temp reaches 60-80 ℃, spraying granulation, and the whole grain of 20 orders-100 order shaking screen promptly gets the granule of the uniform sweetener of the present invention that distributes.The sugariness of the sweetener of gained is 6 times of sucrose, and bulk density is 0.2g/ml.
Sweetener of the present invention by fluid bed fluidized drying one-step palletizing, spray-drying process, wet granulation, dry granulation preparation sees the following form 1;
The example that adds the sweetener of the present invention of various natural flavourings (food grade natural perfume material) sees the following form 2;
The example that adds the sweetener of the present invention of various natural food colours sees the following form 3;
The example that adds the sweetener of the present invention of various natural flavourings and natural food colour sees the following form 4;
Percentage in above-mentioned table 1, table 2, table 3 and the table 4 is mass percent.
Table 1
Table 2
Annotate: described carrier is one or more the combination in the natural products auxiliary material, and the consumption of natural flavouring is 0.1-0.5%.
Table 3
Annotate: described carrier is one or more the combination in the natural products auxiliary material, and the consumption of natural food colour is 0.1-0.5%.
Table 4
Annotate: described carrier is one or more the combination in the natural products auxiliary material, and the consumption of natural flavouring is 0.1-0.5%, and the consumption of natural food colour is 0.1-0.5%.
Claims (10)
1. functional sweetener, described functional sweetener comprises Sucralose and natural products auxiliary material.
2. functional sweetener according to claim 1 is characterized in that, described Sucralose and natural products auxiliary material are equally distributed in sweetener, and the mass ratio of described Sucralose and natural products auxiliary material is 0.5: 99.5 to 28.2: 71.8.
3. functional sweetener according to claim 2, it is characterized in that described natural products auxiliary material is selected from hydrolysate, fermentate or the extract of corn, paddy rice hydrolysate, fermentate or extract, water-soluble natural plant extracts, and in the water solutable edible fiber one or more; Described water solutable edible fiber is selected from one or more in green tea water-soluble fibre, corn water-soluble fibre, fruit water-soluble fibre, vegetables water water-soluble fibre, soybean water-soluble fiber, rice water-soluble fibre and the konjaku water solutable fiber.
4. functional sweetener according to claim 3, it is characterized in that, described functional sweetener contains equally distributed natural food colour, and the mass ratio of the gross mass of described natural food colour and Sucralose and natural products auxiliary material is 0.005: 99.995 to 0.01: 99.99; Described natural food colour is selected from one or more in chlorophyll, carrotene, lycopene, lutein, kaoliang color, chrysanthemum flavine and the carthamin.
5. functional sweetener according to claim 4, it is characterized in that, described functional sweetener contains equally distributed natural flavouring, and the mass ratio of the gross mass of described natural flavouring and Sucralose and natural products auxiliary material is 0.005: 99.995 to 0.01: 99.99; Described natural flavouring is selected from one or more in lemon, banana, apple, strawberry, vanilla, cloves, tsaoko, orange peel, Bai Zang, peppermint, nutmeg, basyleave, semen armeniacae amarae, Herba Lycopi's perfume (or spice) and the storax.
6. method for preparing as functional sweetener as described in each of claim 1 to 3; described method comprises the steps: natural products auxiliary material and Sucralose are mixed; place the dry granulation machine; adjust pressure and engine speed; select suitable screen cloth to make the compacting granulating, with the whole grain of 20-100 order shaking screen.
7. method for preparing as functional sweetener as described in each of claim 1 to 3, described method comprises the steps: Sucralose is dissolved in the water under 5 ℃ to 45 ℃, forms the aqueous solution of 0.5 quality % to saturated concentration; After the natural products auxiliary material sieved, place wet mixing pelletizer, add aqueous solution of sucrose trichloride and stir the system softwood; make Sucralose evenly attached on the natural products auxiliary material; granulate through the 20-40 mesh sieve, 55-75 ℃ of heated-air drying is with the whole grain of 20 orders-100 order shaking screen.
8. method for preparing as functional sweetener as described in each of claim 1 to 3, described method comprises the steps: Sucralose is dissolved in the water under 5 ℃ to 45 ℃, forms the aqueous solution of 0.5 quality % to saturated concentration; The raw material of natural products auxiliary material is crossed 100 mesh sieves, place the fluidized granulation machine, EAT 80-100 ℃, leaving air temp 25-35 ℃; Carry out fluidized granulation, with the whole grain of 20 orders-100 order shaking screen.
9. method for preparing as functional sweetener as described in each of claim 1 to 3, described method comprises the steps: Sucralose, natural products auxiliary material are dissolved in the water under 5 ℃ to 60 ℃; Under EAT 160-200 ℃, leaving air temp 60-80 ℃, carry out spraying granulation, with the whole grain of 20 orders-100 order shaking screen.
10. the application of the described functional sweetener of each of claim 1 to 5 in preparation food additives, food, beverage, functional beverage and health products.
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| CNA2007100958453A CN101028062A (en) | 2007-04-10 | 2007-04-10 | Functional sweetener, its production and use |
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| CNA2007100958453A CN101028062A (en) | 2007-04-10 | 2007-04-10 | Functional sweetener, its production and use |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102113606A (en) * | 2010-12-31 | 2011-07-06 | 张胜勇 | Slimming candy and preparation method thereof |
| CN105713996A (en) * | 2014-12-02 | 2016-06-29 | 中粮集团有限公司 | Solid molasses powder and preparation method, use and storage method thereof |
| CN107198213A (en) * | 2017-06-21 | 2017-09-26 | 裴寿松 | Sweetener and preparation method thereof |
| CN110338255A (en) * | 2019-06-25 | 2019-10-18 | 中粮集团有限公司 | A kind of preparation method of flavor sugar |
| CN110483532A (en) * | 2019-09-05 | 2019-11-22 | 卓士鸿 | The method that bunge pricklyash leaf extracts chlorophyll and aromatic oil |
-
2007
- 2007-04-10 CN CNA2007100958453A patent/CN101028062A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102113606A (en) * | 2010-12-31 | 2011-07-06 | 张胜勇 | Slimming candy and preparation method thereof |
| CN105713996A (en) * | 2014-12-02 | 2016-06-29 | 中粮集团有限公司 | Solid molasses powder and preparation method, use and storage method thereof |
| CN105713996B (en) * | 2014-12-02 | 2019-10-15 | 中粮集团有限公司 | A kind of solid molasses powder and preparation method thereof, purposes and storage method |
| CN107198213A (en) * | 2017-06-21 | 2017-09-26 | 裴寿松 | Sweetener and preparation method thereof |
| CN110338255A (en) * | 2019-06-25 | 2019-10-18 | 中粮集团有限公司 | A kind of preparation method of flavor sugar |
| CN110338255B (en) * | 2019-06-25 | 2023-04-11 | 中粮集团有限公司 | Preparation method of flavored sugar |
| CN110483532A (en) * | 2019-09-05 | 2019-11-22 | 卓士鸿 | The method that bunge pricklyash leaf extracts chlorophyll and aromatic oil |
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