CN100584787C - Method for producing glass lamp-shade surface coating - Google Patents
Method for producing glass lamp-shade surface coating Download PDFInfo
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- CN100584787C CN100584787C CN200610079623A CN200610079623A CN100584787C CN 100584787 C CN100584787 C CN 100584787C CN 200610079623 A CN200610079623 A CN 200610079623A CN 200610079623 A CN200610079623 A CN 200610079623A CN 100584787 C CN100584787 C CN 100584787C
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- cellulose acetate
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- surface coating
- binding agent
- glass lamp
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Abstract
A kind of method for producing glass lamp-shade surface coating, it is characterized in that being formed by following ingredients and weight fraction preparation thereof: 40-60 part is as the acetate butyl and/or the amyl acetate-n of solvent, 25-45 part is as halogen calcium phosphate fluoressent powder, the Sodium Silicofluoride of pigment and filler, 30-40 part is as the acrylic resin and/or the nitro-cotton binding agent of binding agent, and 3-5 part joins behind even agent, cellulose acetate butyrate, cellulose acetate propionate, the cellulose acetate in three kinds of Mierocrystalline celluloses at least a as the silane of auxiliary agent; By the mixed back of above-mentioned weight part ball milling in ball fiber crops machine, fully dissolve, mix thoroughly, with 200-300 order silk screen filter, barreled is standby.This coating is exclusively used in the internal surface of muffle, makes to produce the soft light of oyster white.Has the advantage few in the raw material, that production cost is lower compared to existing technology to the disadvantageous composition of HUMAN HEALTH.
Description
Technical field
The present invention relates to a kind of production method of muffle internal surface coating.
Background technology
CN021536341 disclose Mr.'s Li Chenggui " the frosted coating and the coating process of decorating lamp bulb " apply for a patent technical information, with the multipolymer of the melamine of 30-45%, sulphonamide, formaldehyde or the former material body master composition (barium sulfate, lime carbonate, talcum powder or mica powder) identical, be blended into resin (Resins, epoxy, Synolac, amine resin or acryl resin), the solvent (alcohols, ketone or aromatic essence) of 20-30%, the glazing colour of 1-3% and the auxiliary agent of 0.5-1.5% of 30-45% with its character with transparency.Multipolymer that is adopted in this patent application technology and colorant all require the transparency good, and raw materials cost is higher; On the other hand, the existence of multiple toxic ingredient such as formaldehyde, Resins, epoxy in the raw material, healthy unfavorable to the operative employee.
Summary of the invention
The present invention is directed to the above-mentioned deficiency of prior art, provide a kind of cost toxic ingredient relatively low, in the raw material few relatively, soft, the milky method for producing glass lamp-shade surface coating of light.
The present invention can realize by following measure: formed by following ingredients and weight fraction preparation thereof: 40-60 part is as the acetate butyl and/or acetic acid penta fat of solvent, 25-45 part is as calcium halophosphate activated by antimony andmanganese phosphor powder, the Sodium Silicofluoride of pigment and filler, 30-40 part is as the acrylic resin and/or the nitro-cotton binding agent of binding agent, and 3-5 part joins behind even agent, cellulose acetate butyrate, cellulose acetate propionate, the cellulose acetate in three kinds of Mierocrystalline celluloses at least a as the silane of auxiliary agent; By the mixed back of above-mentioned weight part ball milling in ball fiber crops machine, fully dissolve, mix thoroughly, with 200-300 order silk screen filter, barreled is standby.
The present invention can also come perfect by following measure: 25-45 part is occupied wherein 15-25 part as the calcium halophosphate activated by antimony andmanganese phosphor powder in pigment and the filler.3-5 part joins even agent as the silane of auxiliary agent and occupies wherein 1.5-2 part.
Embodiment
The present invention distinguishes from the fluorescent material (the about 10 μ m of particle diameter) that uses, and belongs to halogen calcium phosphate fluoressent powder coating; Select organic soluble polymer to make binding agent, the nitro-cotton that suitable employing can be dissolved in acetic acid fourth (penta) fat is made binding agent, has the advantage that solvent is volatile, the coating disadvantage is few.But nitrocotton fiber is inflammable and explosive, has potential safety hazard, and therefore more available acrylic resin substitutes and makes the unicity binding agent.Silane gathers even agent, and (another name: glycidyl ether propyl chloride propyl trimethoxy silicane) as a kind of auxiliary agent, it is a kind of silicoorganic compound with special chemical structure, and the molecular formula of using in coating commonly used is Rsix
3Wherein R is unhydrolyzable reactive organic functional base, X is hydrolyzable alkoxyl group, it can pass through chemical reaction or physical action, forming the molecule bridge between original inert high molecular polymer (coating) mutually and glass adheres to each other both securely, be a kind of auxiliary agent of good enhancing sticking power, and have the coating of increasing period of storage, improve pigment and filler usage quantity and moistening dispersiveness, thus the advantage that reduces production costs; As the halogen calcium phosphate fluoressent powder of oyster white pigment and filler, Sodium Silicofluoride (also can consider to add titanium dioxide, further to reduce cost), have effects such as reinforcing, soft light, anti-mildew; Mainly make anti-shrinkage cavity, flow agent usefulness as cellulose acetate butyrate, cellulose acetate propionate, the cellulose acetate of auxiliary agent, make coatingsurface evenly smooth, have uvioresistant, weathering resistance, insulation function concurrently.
The present invention is described in further detail below in conjunction with embodiment, earlier with eight embodiment raw material and weight part proportioning thereof be listed as into following table (videing infra):
Embodiment 1 (consulting weight part proportioning numeral in the following table):
35 weight parts (hereinafter to be referred as part) acetate butyl, 25 parts of acetic acid penta fat, 25 parts of halogen calcium phosphate fluoressent powders, 10 parts of Sodium Silicofluorides, 10 parts of titanium dioxides, 30 parts of acrylic resins, 10 parts of nitro-cotton binding agents, 2 parts of silane joined pour ball mill (jar) into after even agent, 1 part of cellulose acetate butyrate, 1 part of cellulose acetate propionate, 1 part of cellulose acetate are mixed and carry out ball milling 3-4h, the about 105r/min of drum's speed of rotation notices that the density of adjusting the powder slurry is about 1.34g/cm
3(winter is slightly high, and summer is more lower slightly), viscosity controller is at 14-18s.If viscosity height, density are little, then slightly add acetic acid fourth (penta) fat; If viscosity height, density are little, then slightly add fluorescence dry powder; If viscosity is low, density is big, then slightly adds binding agent; If viscosity is low, density is little, then solvent is too much, should regulate.Use 200-300 order silk screen filter at last, and continuously stirring, barreled is standby.
Embodiment 2-8 makes this coating by the parts by weight of each corresponding in last table proportioning raw materials with embodiment 1 same procedure.Among above-mentioned eight embodiment, preferred with embodiment 3,5,7.
It is few to the disadvantageous composition of health in the raw material, living that the present invention has compared to existing technology Produce lower-cost advantage.
Claims (2)
1, a kind of method for producing glass lamp-shade surface coating, it is characterized in that by following ingredients and weight part thereof formulated: 40-60 part is as the N-BUTYL ACETATE and/or the amyl acetate-n of solvent, 25-45 part is as calcium halophosphate activated by antimony andmanganese phosphor powder, the Sodium Silicofluoride of pigment and filler, 30-40 part is as the acrylic resin and/or the nitro-cotton binding agent of binding agent, and 3-5 part joins behind even agent, cellulose acetate butyrate, cellulose acetate propionate, the cellulose acetate in three kinds of Mierocrystalline celluloses at least a as the silane of auxiliary agent; By the mixed back of above-mentioned weight part ball milling in ball mill, fully dissolve, mix thoroughly, with 200-300 order silk screen filter, barreled is standby.
2, method for producing glass lamp-shade surface coating as claimed in claim 1 is characterized in that the calcium halophosphate activated by antimony andmanganese phosphor powder occupies 15-25 part wherein in said 45 parts of pigment and the filler.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN200610079623A CN100584787C (en) | 2006-04-28 | 2006-04-28 | Method for producing glass lamp-shade surface coating |
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CN200610079623A CN100584787C (en) | 2006-04-28 | 2006-04-28 | Method for producing glass lamp-shade surface coating |
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CN1850686A CN1850686A (en) | 2006-10-25 |
CN100584787C true CN100584787C (en) | 2010-01-27 |
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CN200610079623A Expired - Fee Related CN100584787C (en) | 2006-04-28 | 2006-04-28 | Method for producing glass lamp-shade surface coating |
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Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102464935B (en) * | 2010-11-19 | 2014-03-12 | 比亚迪股份有限公司 | Glass lampshade surface coating, preparation method thereof and glass lampshade |
CN102627900A (en) * | 2012-03-20 | 2012-08-08 | 江苏同辉照明科技有限公司 | Preparation method of anti-ultraviolet paint |
CN103602195B (en) * | 2013-11-19 | 2016-07-06 | 青岛祥嘉知识产权服务有限公司 | A kind of multifunctional water-proof paint of improvement |
CN103773200A (en) * | 2014-01-20 | 2014-05-07 | 南通钰成光电科技有限公司 | Anti-friction coating for glass lampshade, and preparation method thereof |
CN103925495B (en) * | 2014-04-14 | 2016-01-20 | 浙江三晶照明有限公司 | Coating in a kind of LED straight lamp and this LED straight lamp |
CN106833171A (en) * | 2016-12-16 | 2017-06-13 | 安徽极光照明工程有限公司 | A kind of production method of Lawn lamp cover surface coating |
CN108300070B (en) * | 2017-12-29 | 2020-05-22 | 宁波凯耀电器制造有限公司 | High-luminous-efficiency LED lamp coating powder and using method thereof |
CN108676433A (en) * | 2018-04-09 | 2018-10-19 | 南通德瑞森复合材料有限公司 | A kind of production method of paint specially adapted for glass fibre reinforced plastic |
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