CN100424238C - Bunge prickly ash viscose fiber and preparation method and application thereof - Google Patents
Bunge prickly ash viscose fiber and preparation method and application thereof Download PDFInfo
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- CN100424238C CN100424238C CNB2006100363439A CN200610036343A CN100424238C CN 100424238 C CN100424238 C CN 100424238C CN B2006100363439 A CNB2006100363439 A CN B2006100363439A CN 200610036343 A CN200610036343 A CN 200610036343A CN 100424238 C CN100424238 C CN 100424238C
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Abstract
The present invention discloses pricklyash peel viscose fiber and a preparation method and application thereof. The fiber contains 1% to 8% of pricklyash peel extract measured by the total dry basis weight in the fiber, and the pricklyash peel extract is homogeneously dispersed in the fiber and on the skin layer of the fiber. The pricklyash peel viscose fiber of the present invention has the advantages of naturalness, degradability, softness, excellent dyeing property of the pricklyash peel viscose fiber, etc., and has the medicinal functions and health protection function. The pricklyash peel viscose fiber has the visible efficiency of resisting bacteria, removing mites and microbes, etc. Simultaneously, the pricklyash peel viscose fiber performs the auxiliary effects of preventing and curing eczema and titillation, delaying aging, etc. In addition, the pricklyash peel viscose fiber also has the effect of expelling mosquitoes.
Description
Technical field
The invention belongs to the textile industry field, relate to a kind of bunge prickly ash viscose fiber, also relate to the preparation method and its usage of bunge prickly ash viscose fiber.
Background technology
Viscose belongs to regenerated celulose fibre, and general molecular formula is (C
6H
10O
5) n, n is the degree of polymerization.It is to be raw material with native celluloses such as natural timber, reed, cotton linters, makes the soluble cellulose xanthate acid through operations such as alkalization, aging, yellows, is dissolved in sig water again to make viscose glue, makes through wet spinning.It is one of chemical fibre that drops into the earliest in the world suitability for industrialized production.Viscose divides two kinds on long filament and staple fibre.Viscose filament yarn claims artificial silk or viscose again; And viscose staple fibre has cotton type (claiming artificial cotton), wool type (title artificial wool) and medium-length fibre.Because the character of viscose approaches natural fabric, good hygroscopicity, moisture percentage meets the physiological requirement of human body skin most, have smooth nice and cool, ventilative, antistatic, dyeing characteristic such as gorgeous, dress is soft, comfortable, and spinnability is good, so, can carry out pure spinning, or with cotton, hair or various synthetic fiber blending, interweave, be used for all kinds of clothes and decorative textile product.And, after the fabric of viscose is discarded, can biodegradation, can not cause the influence of characteristic of concentration to environment.
Chinese prickly ash has very high medicinal and health care and is worth, and the medicinal function of Chinese prickly ash is all on the books on multiple successive dynasties medicine ancient books and modern drug encyclopedia.Chinese prickly ash .Pericarpium Zanthoxyli. (English) Bunge Pricklyash Peel is natural simply medicinal material.The pepper extract main component is materials such as linalool, citrene, nopinene, polyenoid acid amides.Chinese prickly ash is the traditional effective high value Chinese medicine of China, and it is hot in nature, and hot, the people's the spleen channel stomach of flavor can eliminating cold to remove dampness, the pain relieving desinsection, and can remove six colds of bowing.Cure mainly chronic enterogastritis, diseases such as stomach abdomen crymodynia and chornic arthritis, muscle rheumatalgia.It is reported, the extract of xanthoxylum or volatile oil antiviral, kill aspects such as germ, acarid, microorganism and have remarkable efficacy.The Chinese prickly ash crude extract has stronger desinsection, bactericidal action.External application can be treated eczema, be disturbed and itch, and delays senility, and has to report that Chinese prickly ash also has the effect of repellent mosquito.
Although viscose and Chinese prickly ash differ from one another,, still unmanned with viscose and Chinese prickly ash combination up to now, make a kind of product have the advantage of two kinds of materials simultaneously.The inventor after understanding, grasping the characteristic of viscose and Chinese prickly ash, research through great efforts, the health care with viscose textiles and Chinese prickly ash combines finally, this case produces thus.
Summary of the invention
The object of the present invention is to provide a kind of bunge prickly ash viscose fiber, make it except that the advantages such as dyeability of the pure natural with viscose, degradable, softness, excellence, also to give medicinal and health care function, improve material quality.
Another object of the present invention is to a kind of preparation method and application thereof of bunge prickly ash viscose fiber.
In order to reach above-mentioned purpose, solution of the present invention is:
Bunge prickly ash viscose fiber contain 1%～8% pepper extract with the total butt restatement of fiber in fiber, and pepper extract is dispersed in the inside and the top layer of fiber.
Above-mentioned pepper extract is that to choose any one kind of them with water, ethanol or chloroform be that the solvent extraction carrier obtains, and available things of Zanthoxylum bungeanum mainly comprises camphor tree alcohol, citrene, nopinene, polyenoid acid amides.
The preparation method of bunge prickly ash viscose fiber, with pepper extract after dissolving disperses, contain the consumption and the mixing of viscose blend of 1%～8% pepper extract in fiber butt gross weight, mixture filters, after the vacuum defoamation through fully stirring, through the long filament production line, the Chinese prickly ash viscose filament yarn that makes, perhaps through the staple fibre production line, the Chinese prickly ash viscose staple fibre that makes.
The preparation method of bunge prickly ash viscose fiber, with pepper extract after dissolving disperses, contain the consumption of 1%～8% pepper extract and spinning viscose glue by the direct blend of syringe device before spinning in fiber butt gross weight,, promptly obtain the Chinese prickly ash viscose filament yarn then through the long filament production line; Perhaps through the staple fibre production line, the Chinese prickly ash viscose staple fibre that makes.
Above-mentioned pepper extract dissolving prescription is: pepper extract 5wt%-20wt%, and solubilizer: 30wt%-40wt%, water: 40wt%-65wt%, wherein solubilizer is with ethanol: polyethylene glycol is that 1: 1 percentage by weight is made into.
The range of application of bunge prickly ash viscose fiber is: but Chinese prickly ash viscose filament yarn direct spinning, or interweave with cotton, chemical fibre doubling twisting, staple fibre can spin with short fiber blendings such as cotton, acrylic fibers, terylene, is used for underwear, T-shirt, nightwear, shirt, skirt, bedding etc.
The present invention is owing to be dispersed in pepper extract among the fiber, pepper extract in the inside of fiber and top layer and fiber become one securely.Pepper extract and viscose glue matrix compatibility, favorable dispersibility, wash resistant, fast light photograph, high temperature resistant, the dyeability of fiber and good spinnability.Make bunge prickly ash viscose fiber by said method, have broad-spectrum antiseptic, antibiotic dauer effect.Staphylococcus aureus, Escherichia coli, Candida albicans etc. there is significant anti-fungistatic effect.Health care and medical assistance effect are played in multiple contact dermatitis, skin disorder patient's treatment.
This bunge prickly ash viscose fiber, be to add the functional form fiber, except that the advantages such as dyeability of the pure natural with viscose, degradable, softness, excellence, also give medicinal and health care function, have multiple physiologically active, help to strengthen cell viability, can play conditioning skin, treat eczema, disturb and itch, delay senility, the effect of body beautification health has the effect of repellent mosquito simultaneously.
Experimental results show that: Chinese prickly ash viscose filament yarn quality of the present invention meets GB/T13758-92 Grade A standard; Chinese prickly ash viscose staple fibre quality meets GB/T14463-93 Grade A standard.
The specific embodiment
Bunge prickly ash viscose fiber has wide range of applications, and following example is not a limitation of the present invention.
Specific embodiment 1:
Preparing one ton of content is 4% Chinese prickly ash viscose filament yarn, at first prepares the pepper extract mother liquor.
The preparation prescription of Chinese prickly ash mother liquor:
Pepper extract: 5wt%-20wt%, solubilizer (ethanol: polyethylene glycol is 1: 1): 30wt%-40wt%, water: 40wt%-65wt%.
The preparation method who contains 10wt% pepper extract mother liquor: in the stainless steel still, add pepper extract 40Kg, add solubilizer 120Kg, add water 240Kg, stir, mixing, standby.
With above-mentioned mother liquor, with the blend continuously in the syringe before spinning of spinning viscose glue, the blend ratio is 1: 0.04 by the weight ratio that contains pepper extract in the weight of α-Cell in the total weight of fiber (alpha cellulose) and the mother liquor, enters simultaneously in the R535A spinning machine (perhaps R535, R535A semi-continuous spinning machine and continuous spinning machine) and carries out spinning.Spinning cake that falls behind the spinning moulding carries out desulfurization, washing, pickling, bleaching, washes, oils, dewaters, dries through compressing and washing (or drip washing) post processing again, becomes tube, promptly obtains desired above-mentioned Chinese prickly ash viscose filament yarn.
Specific embodiment 2:
For preparing one ton of content is 4% Chinese prickly ash viscose staple fibre, at first prepares the pepper extract mother liquor.
The preparation prescription of Chinese prickly ash mother liquor:
Pepper extract: 5wt%-20wt%, solubilizer (ethanol: polyethylene glycol is 1: 1): 30wt%-40wt%, water: 40wt%-65wt%.
The preparation method who contains 10wt% pepper extract mother liquor: in the stainless steel still, add pepper extract 40Kg, add solubilizer 120Kg, add water 240Kg, stir, mixing, standby.
With above-mentioned mother liquor, with mixing of viscose in the dissolving machine blend, the blend ratio is 1: 0.04 by the weight ratio that contains pepper extract in the weight of α-Cell in the total weight of fiber (alpha cellulose) and the mother liquor, blend is through stirring, filtration, vacuum defoamation, maturation enters the viscose staple fibre spinning machine and carries out spinning.Tow behind the spinning moulding passes through staple fibre post processing carrying out desulfurization, washing, pickling, bleaching again, washes, oils, cuts off, dries, and packing promptly obtains desired above-mentioned Chinese prickly ash viscose staple fibre.
Specific embodiment 3:
Preparing one ton of content is 1% Chinese prickly ash viscose filament yarn, at first prepares the pepper extract mother liquor.
The preparation prescription of Chinese prickly ash mother liquor:
Pepper extract: 5wt%-20wt%, solubilizer (ethanol: polyethylene glycol is 1: 1): 30wt%-40wt%, water: 40wt%-65wt%.
The preparation method who contains 10wt% pepper extract mother liquor: in the stainless steel still, add pepper extract 10Kg, add solubilizer 30Kg, add water 60Kg, stir, mixing, standby.
With above-mentioned mother liquor, with the blend continuously in the syringe before spinning of spinning viscose glue, the blend ratio is 1: 0.01 by the weight ratio that contains pepper extract in the weight of α-Cell in the total weight of fiber (alpha cellulose) and the mother liquor, enters simultaneously in the R535A spinning machine (perhaps R535, R535A semi-continuous spinning machine and continuous spinning machine) and carries out spinning.Spinning cake that falls behind the spinning moulding carries out desulfurization, washing, pickling, bleaching, washes, oils, dewaters, dries through compressing and washing (or drip washing) post processing again, becomes tube, promptly obtains desired above-mentioned Chinese prickly ash viscose filament yarn.
Specific embodiment 4:
For preparing one ton of content is 1% Chinese prickly ash viscose staple fibre, at first prepares the pepper extract mother liquor.
The preparation prescription of Chinese prickly ash mother liquor:
Pepper extract: 5wt%-20wt%, solubilizer (ethanol: polyethylene glycol is 1: 1): 30wt%-40wt%, water: 40wt%-65wt%.
The preparation method who contains 10wt% pepper extract mother liquor: in the stainless steel still, add pepper extract 10Kg, add solubilizer 30Kg, add water 60Kg, stir, mixing, standby.
With above-mentioned mother liquor, with mixing of viscose in the dissolving machine blend, the blend ratio is 1: 0.01 by the weight ratio that contains pepper extract in the weight of α-Cell in the total weight of fiber (alpha cellulose) and the mother liquor, blend is through stirring, filtration, vacuum defoamation, maturation enters the viscose staple fibre spinning machine and carries out spinning.Tow behind the spinning moulding passes through staple fibre post processing carrying out desulfurization, washing, pickling, bleaching again, washes, oils, cuts off, dries, and packing promptly obtains desired above-mentioned Chinese prickly ash viscose staple fibre.
Experimental results show that: bunge prickly ash viscose fiber: 4% Chinese prickly ash content, acarid scattering ratio are not less than 70%, 1% Chinese prickly ash content, and the acarid scattering ratio is not less than 63%, have performance in significant mildew-resistant, the temperature simultaneously.
In a word, fiber of the present invention is soft, and close skin exquisiteness can play the antibacterial conditioning skins such as mite, microorganism that drive, and treats eczema, disturbs and itch, and delays senility the effect of body beautification health.This invention combines the health care of Chinese prickly ash with taking textiles, have vast potential for future development.
Claims (10)
1. bunge prickly ash viscose fiber is characterized in that: contain 1%～8% pepper extract with the total butt restatement of fiber in fiber.
2. bunge prickly ash viscose fiber as claimed in claim 1 is characterized in that: pepper extract is scattered in the inside and the top layer of fiber.
3. bunge prickly ash viscose fiber as claimed in claim 1 is characterized in that: pepper extract is to extract carrier with water, ethanol or chloroform to obtain, and available things of Zanthoxylum bungeanum mainly comprises camphor tree alcohol, citrene, nopinene, polyenoid acid amides.
4. the preparation method of bunge prickly ash viscose fiber, it is characterized in that: with pepper extract after dissolving disperses, contain the consumption and the mixing of viscose blend of 1%～8% pepper extract in fiber butt gross weight, mixture is through fully stirring, filter, after the vacuum defoamation, through the long filament production line, the Chinese prickly ash viscose filament yarn that makes.
5. the preparation method of bunge prickly ash viscose fiber, it is characterized in that: with pepper extract after dissolving disperses, contain the consumption and the mixing of viscose blend of 1%～8% pepper extract in fiber butt gross weight, mixture is through fully stirring, filter, after the vacuum defoamation, through the staple fibre production line, the Chinese prickly ash viscose staple fibre that makes.
6. the preparation method of bunge prickly ash viscose fiber, it is characterized in that: pepper extract is contained the consumption of 1%～8% pepper extract and spinning viscose glue by the direct blend of syringe device before spinning in fiber butt gross weight after dissolving disperses, through the long filament production line, promptly obtain the Chinese prickly ash viscose filament yarn then.
7. the preparation method of bunge prickly ash viscose fiber, it is characterized in that: pepper extract is contained the consumption of 1%～8% pepper extract and spinning viscose glue by the direct blend of syringe device before spinning in fiber butt gross weight after dissolving disperses, then through the staple fibre production line, the Chinese prickly ash viscose staple fibre that makes.
8. as the preparation method of bunge prickly ash viscose fiber as described in the claim 4 to 7 any, it is characterized in that: pepper extract dissolving prescription is: pepper extract 5wt%-20wt%, solubilizer 30wt%-40wt%, water 40wt%-65wt%, wherein solubilizer is with ethanol: polyethylene glycol is that 1: 1 percentage by weight is made into.
9. the Chinese prickly ash viscose filament yarn is used for direct spinning, or interweaves with cotton, chemical fibre doubling twisting.
10. the Chinese prickly ash viscose staple fibre is used for spinning with short fiber blending.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100363439A CN100424238C (en) | 2006-06-29 | 2006-06-29 | Bunge prickly ash viscose fiber and preparation method and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100363439A CN100424238C (en) | 2006-06-29 | 2006-06-29 | Bunge prickly ash viscose fiber and preparation method and application thereof |
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| CN1876904A CN1876904A (en) | 2006-12-13 |
| CN100424238C true CN100424238C (en) | 2008-10-08 |
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| CNB2006100363439A Expired - Fee Related CN100424238C (en) | 2006-06-29 | 2006-06-29 | Bunge prickly ash viscose fiber and preparation method and application thereof |
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| CN112941651A (en) * | 2019-12-10 | 2021-06-11 | 上海美纤智能科技有限公司 | Mite-repelling textile |
| CN114059234B (en) * | 2021-11-26 | 2023-05-26 | 成都大学 | Fruit and vegetable preservative film and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1594679A (en) * | 2004-07-08 | 2005-03-16 | 武汉科技学院 | Fiber modified by Chinese traditional medicine and manufacturing method thereof |
| CN1786300A (en) * | 2005-12-12 | 2006-06-14 | 张志伟 | Functional viscose fiber containing Chinese medicinal component and its preparation method |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1594679A (en) * | 2004-07-08 | 2005-03-16 | 武汉科技学院 | Fiber modified by Chinese traditional medicine and manufacturing method thereof |
| CN1786300A (en) * | 2005-12-12 | 2006-06-14 | 张志伟 | Functional viscose fiber containing Chinese medicinal component and its preparation method |
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| PB01 | Publication | ||
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Xiamen Hualun Printing & Dyeing Co., Ltd. Assignor: Fujian Zhonghe Co., Ltd. Contract fulfillment period: 2009.8.1 to 2014.7.31 Contract record no.: 2009351000063 Denomination of invention: Bunge prickly ash viscose fiber and preparation method and application thereof Granted publication date: 20081008 License type: Exclusive license Record date: 2009.9.8 |
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| LIC | Patent licence contract for exploitation submitted for record |
Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2009.8.1 TO 2014.7.31; CHANGE OF CONTRACT Name of requester: XIAMEN HUALUN PRINTING AND DYEING CO., LTD. Effective date: 20090908 |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20081008 Termination date: 20180629 |