CL2012003376A1 - Proceso para remover lignina de licor negro acidificando el licor negro, en donde el licor negro es oxidado antes de dicha acidificacion para minimizar elazufre reducido total (trs) en el licor negro, de manera que las hemicelulosas sean oxidadas para formar un agente de acidificacion, el cual complementa a dicho acidificante en la acidificacion; proceso para separar lignina de licor negro. - Google Patents
Proceso para remover lignina de licor negro acidificando el licor negro, en donde el licor negro es oxidado antes de dicha acidificacion para minimizar elazufre reducido total (trs) en el licor negro, de manera que las hemicelulosas sean oxidadas para formar un agente de acidificacion, el cual complementa a dicho acidificante en la acidificacion; proceso para separar lignina de licor negro.Info
- Publication number
- CL2012003376A1 CL2012003376A1 CL2012003376A CL2012003376A CL2012003376A1 CL 2012003376 A1 CL2012003376 A1 CL 2012003376A1 CL 2012003376 A CL2012003376 A CL 2012003376A CL 2012003376 A CL2012003376 A CL 2012003376A CL 2012003376 A1 CL2012003376 A1 CL 2012003376A1
- Authority
- CL
- Chile
- Prior art keywords
- black liquor
- acidification
- oxidized
- lignin
- acidifier
- Prior art date
Links
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0057—Oxidation of liquors, e.g. in order to reduce the losses of sulfur compounds, followed by evaporation or combustion if the liquor in question is a black liquor
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
- C07G1/00—Low-molecular-weight derivatives of lignin
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H8/00—Macromolecular compounds derived from lignocellulosic materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Paper (AREA)
- Compounds Of Unknown Constitution (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US35096910P | 2010-06-03 | 2010-06-03 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CL2012003376A1 true CL2012003376A1 (es) | 2013-01-25 |
Family
ID=45063558
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CL2012003376A CL2012003376A1 (es) | 2010-06-03 | 2012-11-30 | Proceso para remover lignina de licor negro acidificando el licor negro, en donde el licor negro es oxidado antes de dicha acidificacion para minimizar elazufre reducido total (trs) en el licor negro, de manera que las hemicelulosas sean oxidadas para formar un agente de acidificacion, el cual complementa a dicho acidificante en la acidificacion; proceso para separar lignina de licor negro. |
Country Status (11)
| Country | Link |
|---|---|
| US (3) | US8771464B2 (https=) |
| EP (1) | EP2576662B1 (https=) |
| JP (1) | JP5898677B2 (https=) |
| CN (1) | CN103154097B (https=) |
| BR (1) | BR112012030594A2 (https=) |
| CA (1) | CA2799798C (https=) |
| CL (1) | CL2012003376A1 (https=) |
| ES (1) | ES2854725T3 (https=) |
| PL (1) | PL2576662T3 (https=) |
| PT (1) | PT2576662T (https=) |
| WO (1) | WO2011150508A1 (https=) |
Families Citing this family (74)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2763447C (en) * | 2009-06-10 | 2017-10-31 | Metso Power Ab | Method for precipitating lignin from black liquor by utilizing waste gases |
| US9879119B2 (en) | 2009-09-25 | 2018-01-30 | Michael A. Lake | Lignin product and process for making same |
| WO2011037967A2 (en) * | 2009-09-25 | 2011-03-31 | Lake Michael A | Process for recovering lignin |
| AT510812A1 (de) * | 2010-10-29 | 2012-06-15 | Annikki Gmbh | Verfahren zur gewinnung von lignin |
| US9790641B2 (en) * | 2011-05-24 | 2017-10-17 | Liquid Lignin Company, Llc | Process for treating lignin |
| ES2658916T3 (es) * | 2011-06-22 | 2018-03-12 | Valmet Aktiebolag | Método de separación de lignina del licor negro que comprende múltiples etapas de acidificación |
| CA2858651C (en) | 2011-12-09 | 2021-01-26 | Upm-Kymmene Corporation | A method for making a lignin component, a lignin component and its use and a product |
| US9163169B2 (en) | 2012-03-13 | 2015-10-20 | Georgia-Pacific Chemicals Llc | Adhesive compositions having a reduced cure time and methods for making and using same |
| EP2825698B1 (en) | 2012-03-16 | 2016-10-05 | Valmet Aktiebolag | Method for lignin separation from black liquor |
| EP2878614A1 (en) | 2012-05-03 | 2015-06-03 | Virdia Ltd. | Methods for treating lignocellulosic materials |
| US8809426B2 (en) | 2012-05-11 | 2014-08-19 | Cyclewood Solutions, Inc. | Chemical modification of lignin and lignin derivatives |
| FI127010B (en) * | 2012-08-24 | 2017-09-29 | Upm Kymmene Corp | A method for recovering low molecular weight lignin from a filtrate |
| US9586338B2 (en) | 2012-10-01 | 2017-03-07 | Georgia-Pacific Chemicals Llc | Methods for making lignocellulose containing composite products |
| US9458298B2 (en) | 2012-10-01 | 2016-10-04 | Georgia-Pacific Chemicals Llc | Methods for making lignocellulose containing composite products |
| WO2014070861A1 (en) * | 2012-10-30 | 2014-05-08 | Thies Mark | Ph-induced fractionation processes for recovery of lignin |
| US9777032B2 (en) * | 2012-10-30 | 2017-10-03 | Cyclewood Solutions, Inc. | Injection of a chemical reagent into a process stream that contains lignin |
| EP2948590B1 (en) * | 2013-01-24 | 2019-05-08 | Valmet AB | Method for producing high purity lignin |
| FI20135105L (fi) * | 2013-02-04 | 2014-08-05 | Andritz Oy | Menetelmä kemikaalien ja sivutuotteiden talteenottamiseksi korkean sulfiditeetin keittolipeistä |
| NZ711575A (en) | 2013-03-14 | 2017-02-24 | Georgia Pacific Chemicals Llc | Binder compositions and methods for making and using same |
| US9587077B2 (en) | 2013-03-14 | 2017-03-07 | Georgia-Pacific Chemicals Llc | Methods for making composite products containing lignocellulose substrates |
| KR20160007537A (ko) | 2013-05-03 | 2016-01-20 | 버디아, 인크. | 열안정성 리그닌 분획물의 제조 방법 |
| JP6666242B2 (ja) | 2013-05-03 | 2020-03-13 | ヴァーディア, インコーポレイテッド | リグノセルロース系材料処理の方法 |
| SE540451C2 (en) * | 2013-05-29 | 2018-09-18 | Suncarbon Ab | A method for the treatment of spent pulping liquor for the production of a stream of depolymerized lignin |
| CN105829406B (zh) * | 2013-12-12 | 2020-06-30 | 索理思科技公司 | 木质素纳米颗粒分散体及制备和使用其的方法 |
| WO2015095841A1 (en) | 2013-12-20 | 2015-06-25 | Georgia-Pacific Chemicals Llc | Release aids with adjustable cloud points for creping processes |
| CA2944619C (en) | 2014-04-02 | 2021-10-12 | Georgia-Pacific Chemicals Llc | Methods for making lignocellulose composite products |
| WO2015153520A1 (en) | 2014-04-02 | 2015-10-08 | Georgia-Pacific Chemicals Llc | Methods for making lignocellulose composite products with oxidative binders and encapsulated catalyst |
| CA2944623A1 (en) | 2014-04-02 | 2015-10-08 | Georgia-Pacific Chemicals Llc | Methods for making lignocellulose composite products with oxidative binders and complexed metal catalyst |
| FI127601B (en) * | 2014-04-03 | 2018-10-15 | Andritz Oy | Method for handling spent wash solution of a lignin-recovery process |
| FI126369B (en) * | 2014-06-06 | 2016-10-31 | Andritz Oy | A method for using lignin extracted from black liquor as fuel for a lime kiln |
| CN109851814B (zh) * | 2014-07-09 | 2022-03-11 | 威尔迪亚有限责任公司 | 用于从黑液中分离和精制木质素的方法及其组合物 |
| SE539887C2 (en) * | 2014-10-03 | 2018-01-02 | Stora Enso Oyj | A method to purify lignin from Sulfur by using an electric field |
| KR101521238B1 (ko) * | 2014-11-04 | 2015-05-18 | (재)울산테크노파크 | 흑액으로부터 고순도 리그닌을 추출하는 방법 |
| US20160186067A1 (en) * | 2014-12-30 | 2016-06-30 | Shell Oil Company | Methods and systems for processing cellulosic biomass |
| US10858554B2 (en) | 2015-04-15 | 2020-12-08 | Fpinnovations | High residual content (HRC) kraft/soda lignin as an ingredient in wood adhesives |
| FI129778B (en) | 2015-06-26 | 2022-08-31 | Teknologian Tutkimuskeskus Vtt Oy | Procedure for activation and precipitation of lignin |
| EP3320140B1 (en) | 2015-07-07 | 2021-12-15 | Solenis Technologies, L.P. | Methods for inhibiting the deposition of organic contaminants in pulp and papermaking systems |
| FI128962B (en) * | 2015-11-06 | 2021-04-15 | Teknologian Tutkimuskeskus Vtt Oy | Alkali-O2 oxidized lignin as a dispersant |
| KR20240113617A (ko) * | 2016-03-31 | 2024-07-22 | 웨스트 프레이저 밀즈 리미티드 | 목재 펄프를 포함하는 셀룰로오스 합성물 |
| CN109477308A (zh) | 2016-05-03 | 2019-03-15 | 索理思科技公司 | 生物聚合物施胶剂 |
| CA3024526A1 (en) * | 2016-06-07 | 2017-12-14 | Fpinnovations | Antimicrobial lignin composition derived from wood biomass |
| CN106750362B (zh) * | 2016-11-30 | 2019-06-11 | 海南金海浆纸业有限公司 | 一种木质素的分级方法 |
| CA3043474A1 (en) | 2016-12-02 | 2018-06-07 | Jesse L. Paris | Wax-organic extender emulsion and method for manufacture thereof |
| PT3592802T (pt) | 2017-03-09 | 2024-02-05 | Fpinnovations | Processo para produzir um copolímero de lenhina aniónico sob condições aquosas ácidas |
| CN110892005A (zh) | 2017-03-09 | 2020-03-17 | Fp创新研究所 | 在酸水溶液条件下生产阳离子木质素共聚物的工艺 |
| FI129362B (fi) * | 2017-05-16 | 2021-12-31 | Andritz Oy | Menetelmä kemiallisen massan tuottamiseksi |
| CN109485871B (zh) * | 2017-09-09 | 2021-03-05 | 中国石油化工股份有限公司 | 一种高活性酶解木质素及其制备方法 |
| CN108455754B (zh) * | 2018-02-24 | 2022-01-07 | 北京林业大学 | 一种水热酸解用于处理植物原料预水解液的方法 |
| WO2019165443A1 (en) * | 2018-02-26 | 2019-08-29 | The Texas A&M University System | Lignin fractionation and fabrication for quality carbon fiber |
| WO2019241413A1 (en) * | 2018-06-12 | 2019-12-19 | Domtar Paper Company, Llc | Methods and processes for lignin isolation/extraction |
| WO2019241408A1 (en) * | 2018-06-12 | 2019-12-19 | Domtar Paper Company, Llc | Methods and processes for lignin isolation/extraction |
| AT521179B1 (de) | 2018-06-15 | 2019-11-15 | Papierholz Austria Gmbh | Verfahren zur Isolierung von Lignin aus einem alkalischen Prozessstrom |
| CN109054045B (zh) * | 2018-08-13 | 2021-05-07 | 南京工业大学 | 一种亚微米木质素的制备方法 |
| JP6662423B1 (ja) * | 2018-09-06 | 2020-03-11 | 日本製紙株式会社 | リグニンを分離する方法 |
| FI129347B (en) | 2018-10-23 | 2021-12-15 | Teknologian Tutkimuskeskus Vtt Oy | Extraction of valuable components from bark |
| EP3693508A1 (en) | 2019-02-08 | 2020-08-12 | Scitech-service OY | Method for lignin production |
| CN110372883B (zh) * | 2019-08-14 | 2021-01-01 | 南京工业大学 | 一种从黑液中提取木质素和硅酸的方法 |
| CA3091213A1 (en) | 2019-08-26 | 2021-02-26 | Walker Industries Holdings Limited | Aqueous wax emulsions and dispersions and uses thereof |
| US12515989B2 (en) | 2019-08-26 | 2026-01-06 | Walker Industries Holdings Limited | Wax dispersion composition containing lignin for imparting water resistance to gypsum |
| SE2050074A1 (en) * | 2020-01-28 | 2021-01-29 | Soedra Skogsaegarna Ekonomisk Foerening | Process for producing one, or more, compounds |
| EP4132899A4 (en) * | 2020-03-03 | 2024-10-09 | Casad, Robert C. | HIGH-SOLID ALKALINE OXIDATION AND BIOMETHANE CONVERSION OF RESIDUAL LIGNIN |
| JP2021155661A (ja) * | 2020-03-30 | 2021-10-07 | 日本製紙株式会社 | ソーダリグニンの分離方法 |
| US11866456B2 (en) * | 2020-07-14 | 2024-01-09 | Liquid Lignin Company | Process for treating lignin |
| CN111771454B (zh) * | 2020-08-24 | 2023-09-12 | 山东农业大学 | 一种基于造纸黑液制备的水稻耐盐种子包衣组分及其应用方法 |
| US20240052530A1 (en) * | 2020-08-25 | 2024-02-15 | The Texas A&M University System | Lignin Fractionation and Fabrication for Quality Carbon Fiber |
| RU2756631C1 (ru) * | 2020-10-12 | 2021-10-04 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Санкт-Петербургский государственный университет промышленных технологий и дизайна" | Способ удаления лигноуглеводного комплекса из черного щелока производства сульфатной целлюлозы (3 варианта) |
| SE545888C2 (en) * | 2021-07-15 | 2024-03-05 | Suncarbon Ab | Treating black liquor with bio-oil acids for lignin recovery |
| WO2023015325A1 (en) * | 2021-08-06 | 2023-02-09 | Lignorganic (Pty) Ltd | System and method for obtaining lignin and carboxylic acid from byproducts of pulping processes |
| JP2023168903A (ja) * | 2022-05-16 | 2023-11-29 | 日華化学株式会社 | クラフトリグニンの精製方法 |
| WO2024187276A1 (en) * | 2023-03-14 | 2024-09-19 | Fpinnovations | Improved process for the extraction of kraft lignin from hardwood and eucalyptus black liquors |
| CN116715865A (zh) * | 2023-04-21 | 2023-09-08 | 天津科技大学 | 一种提高麦草生物化学机械浆废液木素产品质量的方法 |
| CN116425998A (zh) * | 2023-04-21 | 2023-07-14 | 天津科技大学 | 一种高效分离麦草生物化学机械浆废液中木素的方法 |
| WO2025043331A1 (en) * | 2023-08-25 | 2025-03-06 | Red Leaf Sustainable Ip Corp. | Apparatus and methods for extracting lignin from non-wood black liquor |
| CA3252920A1 (en) | 2024-07-26 | 2026-03-01 | Walker Industries Holdings Limited | Method for imparting water resistance to gypsum |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2406867A (en) * | 1943-12-31 | 1946-09-03 | Smith Paper Mills Ltd Howard | Method of treating lignocellulosic material |
| GB664811A (en) * | 1944-08-21 | 1952-01-16 | Smith Paper Mills Ltd Howard | Improvements in the recovery of lignin from black liquor |
| SE8204365L (sv) * | 1981-07-23 | 1983-01-24 | Domtar Inc | Sett for behandling av restlut fran en alkalisk massakokningsprocess av lignocellulosamaterial |
| US4521336A (en) | 1984-04-16 | 1985-06-04 | Westvaco Corporation | Process for preparing lignosulfonates |
| US4764597A (en) * | 1987-06-15 | 1988-08-16 | Westvaco Corporation | Method for methylolation of lignin materials |
| CA1335976C (en) * | 1989-05-31 | 1995-06-20 | Mahmoud Kamran Azarniouch | Recovery of naoh and other values from spent liquors and bleach plant effluents |
| US20030041982A1 (en) * | 2001-08-31 | 2003-03-06 | Prior Eric S. | Organic biomass fractionation process |
| WO2006038072A1 (ja) * | 2004-09-07 | 2006-04-13 | K.I. System Co., Ltd. | 黒液の処理方法 |
| SE0402201D0 (sv) * | 2004-09-14 | 2004-09-14 | Stfi Packforsk Ab | Method for separating lignin from black liquor |
| SE0402437D0 (sv) * | 2004-10-07 | 2004-10-07 | Stfi Packforsk Ab | Method for separating lignin from a lignin containing liquid/slurry |
| US7699958B2 (en) * | 2006-11-27 | 2010-04-20 | Ut-Battelle, Llc | Method for improving separation of carbohydrates from wood pulping and wood or biomass hydrolysis liquors |
| WO2009104995A1 (en) * | 2008-02-21 | 2009-08-27 | Lignoboost Ab | A method for separating lignin from black liquor, a lignin product, and use of a lignin product for the production of fuels or materials |
| WO2011037967A2 (en) | 2009-09-25 | 2011-03-31 | Lake Michael A | Process for recovering lignin |
-
2011
- 2011-05-31 CA CA2799798A patent/CA2799798C/en active Active
- 2011-05-31 US US13/118,666 patent/US8771464B2/en active Active
- 2011-05-31 WO PCT/CA2011/000654 patent/WO2011150508A1/en not_active Ceased
- 2011-05-31 PT PT117890178T patent/PT2576662T/pt unknown
- 2011-05-31 JP JP2013512709A patent/JP5898677B2/ja active Active
- 2011-05-31 BR BR112012030594A patent/BR112012030594A2/pt active IP Right Grant
- 2011-05-31 PL PL11789017T patent/PL2576662T3/pl unknown
- 2011-05-31 ES ES11789017T patent/ES2854725T3/es active Active
- 2011-05-31 CN CN201180027562.XA patent/CN103154097B/zh active Active
- 2011-05-31 EP EP11789017.8A patent/EP2576662B1/en active Active
-
2012
- 2012-11-30 CL CL2012003376A patent/CL2012003376A1/es unknown
-
2014
- 2014-05-22 US US14/284,558 patent/US8940130B2/en active Active
- 2014-12-16 US US14/571,907 patent/US9091023B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| US9091023B2 (en) | 2015-07-28 |
| EP2576662B1 (en) | 2020-11-18 |
| BR112012030594A2 (pt) | 2016-08-16 |
| US8940130B2 (en) | 2015-01-27 |
| WO2011150508A1 (en) | 2011-12-08 |
| CN103154097B (zh) | 2017-01-18 |
| CN103154097A (zh) | 2013-06-12 |
| EP2576662A4 (en) | 2014-09-03 |
| JP2013527339A (ja) | 2013-06-27 |
| PL2576662T3 (pl) | 2021-09-27 |
| EP2576662A1 (en) | 2013-04-10 |
| ES2854725T3 (es) | 2021-09-22 |
| US20140256920A1 (en) | 2014-09-11 |
| JP5898677B2 (ja) | 2016-04-06 |
| US20150096697A1 (en) | 2015-04-09 |
| US8771464B2 (en) | 2014-07-08 |
| US20110297340A1 (en) | 2011-12-08 |
| PT2576662T (pt) | 2021-02-16 |
| CA2799798A1 (en) | 2011-12-08 |
| CA2799798C (en) | 2015-01-20 |
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