CL2010001387A1 - Procedimientos para la produccion de esteres de alquilo a partir de una reaccion de transesterificacion de alcohol y trigliceridos en un reactor multi-zona; y reactor tubular usado en dichos procedimientos. - Google Patents

Procedimientos para la produccion de esteres de alquilo a partir de una reaccion de transesterificacion de alcohol y trigliceridos en un reactor multi-zona; y reactor tubular usado en dichos procedimientos.

Info

Publication number
CL2010001387A1
CL2010001387A1 CL2010001387A CL2010001387A CL2010001387A1 CL 2010001387 A1 CL2010001387 A1 CL 2010001387A1 CL 2010001387 A CL2010001387 A CL 2010001387A CL 2010001387 A CL2010001387 A CL 2010001387A CL 2010001387 A1 CL2010001387 A1 CL 2010001387A1
Authority
CL
Chile
Prior art keywords
procedures
zone
alcohol
biodiesel
entry
Prior art date
Application number
CL2010001387A
Other languages
English (en)
Inventor
Michael Ashley Tom
Original Assignee
Renewable Energy Group Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Renewable Energy Group Inc filed Critical Renewable Energy Group Inc
Publication of CL2010001387A1 publication Critical patent/CL2010001387A1/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2405—Stationary reactors without moving elements inside provoking a turbulent flow of the reactants, such as in cyclones, or having a high Reynolds-number
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/19—Esters ester radical containing compounds; ester ethers; carbonic acid esters
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/0004—Processes in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00168—Controlling or regulating processes controlling the viscosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00186—Controlling or regulating processes controlling the composition of the reactive mixture
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

Abstract

LAS RELACIONES DE UN PROCEDIMIENTO PARA LA PRODUCCIÓN DE BIODIESEL A PARTIR DE UNA REACCIÓN DE TRANS-ESTERIFICACIÓN DE ALCOHOL Y TRIGLICÉRIDOS EN UN REACTOR TUBULAR DE MULTI-ZONA SE DIVULGAN. ÉSTER DE ALQUILO Y GLICERINA SON FORMADOS A PARTIR DE REACTANTES EN UNA MEZCLA DE REACCIÓN MIENTRAS LA MEZCLA DE REACCIÓN FLUYE A TRAVÉS DE LAS ZONAS. LAS ZONAS INCLUYEN UNA ZONA DE ENTRADA, UNA ZONA DE SALIDA, Y UNA ZONA INTERMEDIA ENTRE LAS ZONAS DE ENTRADA Y SALIDA. LAS ZONAS SON CARACTERIZADAS POR PROPIEDADES FÍSICAS TALES COMO LA VISCOSIDAD, DENSIDAD, COMPOSICIÓN, Y RÉGIMEN DE FLUJO. LAS ZONAS DE ENTRADA E INTERMEDIAS INCLUYEN MEZCLADORES ESTÁTICOS QUE REALIZAN UN MEZCLADO ESTRUCTURADO QUE AUMENTA LA CONVERSIÓN Y EL RENDIMIENTO. EL GRADO DE MEZCLADO PROPORCIONADO POR LOS MEZCLADORES ES DIFERENTE EN LAS ZONAS PARA DAR CUENTAS DE LAS DIFERENCIAS EN LAS PROPIEDADES FÍSICAS. ADICIONALMENTE, LA CORRIENTE DEL PRODUCTO DEL REACTOR ES PASADA A TRAVÉS DE UN AGLUTINADOR PARA AUMENTAR EL TAMAÑO DE GOTA DE LA FASE DISPERSA DE GLICERINA, PARA FACILITAR TANTO LA RÁPIDA SEPARACIÓN DE LA FASE DE GLICERINA DESDE LA FASE DE BIODIESEL, Y AUMENTAR LA CONVERSIÓN Y EL RENDIMIENTO EN UN DECANTADOR.
CL2010001387A 2008-06-09 2010-12-09 Procedimientos para la produccion de esteres de alquilo a partir de una reaccion de transesterificacion de alcohol y trigliceridos en un reactor multi-zona; y reactor tubular usado en dichos procedimientos. CL2010001387A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US6005308P 2008-06-09 2008-06-09
US12/345,470 US8865080B2 (en) 2008-06-09 2008-12-29 Devices, processes and methods for the production of lower alkyl esters

Publications (1)

Publication Number Publication Date
CL2010001387A1 true CL2010001387A1 (es) 2011-05-13

Family

ID=41399016

Family Applications (2)

Application Number Title Priority Date Filing Date
CL2010001387A CL2010001387A1 (es) 2008-06-09 2010-12-09 Procedimientos para la produccion de esteres de alquilo a partir de una reaccion de transesterificacion de alcohol y trigliceridos en un reactor multi-zona; y reactor tubular usado en dichos procedimientos.
CL2014002318A CL2014002318A1 (es) 2008-06-09 2014-08-29 Procedimiento para la separación de ésteres de alquilo (divisional de solicitud n° 1387-2010)

Family Applications After (1)

Application Number Title Priority Date Filing Date
CL2014002318A CL2014002318A1 (es) 2008-06-09 2014-08-29 Procedimiento para la separación de ésteres de alquilo (divisional de solicitud n° 1387-2010)

Country Status (9)

Country Link
US (1) US8865080B2 (es)
CN (1) CN102099441B (es)
AU (1) AU2009257739B2 (es)
BR (1) BRPI0915080B1 (es)
CA (1) CA2727244C (es)
CL (2) CL2010001387A1 (es)
HK (1) HK1158678A1 (es)
MY (1) MY155241A (es)
WO (1) WO2009152016A2 (es)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8562841B1 (en) * 2009-03-23 2013-10-22 James Philip Hygate Glycerine-biodiesel continuous flow separator and methodology of use
US8420841B2 (en) * 2009-09-15 2013-04-16 Texas Tech University System Methods and systems to produce biodiesel fuel
US8802878B2 (en) * 2010-09-14 2014-08-12 Kyent Chin Process for the production of fatty acid methyl esters from variable feedstock using heterogeneous catalysts
BR112015009114B1 (pt) * 2012-10-22 2024-02-20 Applied Research Associates, Inc Processo para aprimorar uma carga de alimentação orgânica, e, sistema de reator hidrotérmico
US10774272B2 (en) * 2013-11-26 2020-09-15 Phillips 66 Company Sequential mixing process for improved desalting
US10392568B2 (en) * 2013-11-26 2019-08-27 Phillips 66 Company Sequential mixing system for improved desalting
US20160001255A1 (en) 2014-07-03 2016-01-07 Chevron U.S.A. Inc. Novel reactor for ionic liquid catalyzed alkylation based on motionless mixer
WO2020247515A1 (en) * 2019-06-03 2020-12-10 Ewo Solutions Llc Additives for enhancement of oil flow

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5514820A (en) * 1989-09-29 1996-05-07 Henkel Kommanditgesellschaft Auf Aktien Continuous process for the production of lower alkyl esters
US6174501B1 (en) 1997-10-31 2001-01-16 The Board Of Regents Of The University Of Nebraska System and process for producing biodiesel fuel with reduced viscosity and a cloud point below thirty-two (32) degrees fahrenheit
US20030032826A1 (en) 2001-07-20 2003-02-13 The Board Of Regents Of The University Of Nebraska Transesterification process for production of biodiesel
KR100556337B1 (ko) * 2002-02-05 2006-03-03 주식회사 가야에너지 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법
US7420072B2 (en) * 2006-05-05 2008-09-02 Orbitek, Inc. Apparatus and method for producing biodiesel fuel
BRPI0602511A (pt) 2006-07-05 2008-02-26 Etruria Ind De Fibras E Fios S reator e processo para produção de biodiesel
EP1884559A1 (en) 2006-07-26 2008-02-06 Vlaamse Instelling Voor Technologisch Onderzoek (Vito) Novel method for producing biodiesel using an immobilised catalyst
GB0620925D0 (en) 2006-10-20 2006-11-29 Renewable Holdings Ltd Biodiesel synthesis

Also Published As

Publication number Publication date
CA2727244C (en) 2017-02-07
MY155241A (en) 2015-09-30
CN102099441B (zh) 2015-03-25
AU2009257739B2 (en) 2015-03-26
WO2009152016A2 (en) 2009-12-17
AU2009257739A1 (en) 2009-12-17
BRPI0915080B1 (pt) 2018-06-19
HK1158678A1 (en) 2012-07-20
US20090300973A1 (en) 2009-12-10
CA2727244A1 (en) 2009-12-17
WO2009152016A3 (en) 2010-03-11
BRPI0915080A2 (pt) 2015-10-27
CL2014002318A1 (es) 2015-02-06
CN102099441A (zh) 2011-06-15
US8865080B2 (en) 2014-10-21

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