CH265757A - Process for the preparation of a new mercury compound. - Google Patents
Process for the preparation of a new mercury compound.Info
- Publication number
- CH265757A CH265757A CH265757DA CH265757A CH 265757 A CH265757 A CH 265757A CH 265757D A CH265757D A CH 265757DA CH 265757 A CH265757 A CH 265757A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- mercury compound
- new mercury
- ethylmercurithio
- new
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 229940100892 mercury compound Drugs 0.000 title description 3
- 150000002731 mercury compounds Chemical class 0.000 title description 3
- 238000002360 preparation method Methods 0.000 title description 2
- 239000013078 crystal Substances 0.000 claims description 3
- 239000000645 desinfectant Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 229940100890 silver compound Drugs 0.000 claims 1
- 150000003379 silver compounds Chemical class 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- PQSBRHXGVPVYFJ-UHFFFAOYSA-N 4-(dimethylamino)benzenethiol Chemical compound CN(C)C1=CC=C(S)C=C1 PQSBRHXGVPVYFJ-UHFFFAOYSA-N 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- VUQUOGPMUUJORT-UHFFFAOYSA-N methyl 4-methylbenzenesulfonate Chemical compound COS(=O)(=O)C1=CC=C(C)C=C1 VUQUOGPMUUJORT-UHFFFAOYSA-N 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/10—Mercury compounds
- C07F3/12—Aromatic substances containing mercury
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung einer neuen Quecksilberverbindung. Gegenstand des vorliegenden Patentes ist ein Verfahren zur Herstellung einer neuen Quecksilberverbindung, das dadurch gekenn zeichnet ist, dass man p-Äthylmereurithio- dimethylanilin mit p-Toluolsulfosäuremethyl- ester umsetzt.
Das so erhaltene p-Äthylmercurithio-phenyl- ti-imethylammonium-p-toluolstilfonat. bildet in Wasser lösliche, gelbliche Kristalle und soll als Desinfektionsmittel Verwendung finden. Beispiel: 10 Teile p-;lthylniercurithio-dimetli3-lani- lin (erhalten durch Umsetzung von Äthylqueek- silberhydro:
cyd mit einer alkoholischen Lö sung von p-Mercapto-dimethylanilin) werden mit 5 Teilen p-Toluolstilfosäuremethylester in 100 Teilen Methanol versetzt und während einer Stunde am Rückfluss gekocht. Nach dem Abkühlen, Versetzen mit Äther und Ausfrie ren bei -100 erhält man p-Äthylmercurithio- phenyl-trimethy lammonium - pl-toltiolsulfonat in Form von in Wasser löslichen Kristallen.
Process for the preparation of a new mercury compound. The subject matter of the present patent is a process for the production of a new mercury compound which is characterized in that p-ethylmereurithio-dimethylaniline is reacted with p-toluenesulfonic acid methyl ester.
The p-ethylmercurithio-phenyl-ti-imethylammonium-p-toluene stilfonate thus obtained. forms yellowish crystals that are soluble in water and should be used as a disinfectant. Example: 10 parts of p-; ethylniercurithio-dimetli3-laniline (obtained by reacting ethylqueek silver hydro:
cyd with an alcoholic solution of p-mercapto-dimethylaniline) are mixed with 5 parts of methyl p-toluene-stilfoate in 100 parts of methanol and refluxed for one hour. After cooling, adding ether and freezing out at -100, p-ethylmercurithiophene- yltrimethy lammonium-p-toltenol sulfonate is obtained in the form of water-soluble crystals.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH257579T | 1944-08-04 | ||
| CH265757T | 1944-08-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH265757A true CH265757A (en) | 1949-12-15 |
Family
ID=25730082
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH265757D CH265757A (en) | 1944-08-04 | 1944-08-04 | Process for the preparation of a new mercury compound. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH265757A (en) |
-
1944
- 1944-08-04 CH CH265757D patent/CH265757A/en unknown
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