CH265755A - Process for the preparation of a new mercury compound. - Google Patents
Process for the preparation of a new mercury compound.Info
- Publication number
- CH265755A CH265755A CH265755DA CH265755A CH 265755 A CH265755 A CH 265755A CH 265755D A CH265755D A CH 265755DA CH 265755 A CH265755 A CH 265755A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- mercury compound
- new mercury
- new
- dimethylaniline
- Prior art date
Links
- 229940100892 mercury compound Drugs 0.000 title claims description 4
- 150000002731 mercury compounds Chemical class 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title description 2
- 239000000645 desinfectant Substances 0.000 claims description 2
- VAYGXNSJCAHWJZ-UHFFFAOYSA-N dimethyl sulfate Chemical compound COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- QLAJNZSPVITUCQ-UHFFFAOYSA-N 1,3,2-dioxathietane 2,2-dioxide Chemical compound O=S1(=O)OCO1 QLAJNZSPVITUCQ-UHFFFAOYSA-N 0.000 description 1
- PQSBRHXGVPVYFJ-UHFFFAOYSA-N 4-(dimethylamino)benzenethiol Chemical compound CN(C)C1=CC=C(S)C=C1 PQSBRHXGVPVYFJ-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- JLTDJTHDQAWBAV-UHFFFAOYSA-N N,N-dimethylaniline Chemical compound CN(C)C1=CC=CC=C1 JLTDJTHDQAWBAV-UHFFFAOYSA-N 0.000 description 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N N-phenyl amine Natural products NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- WGJDWRPHMYVQFO-UHFFFAOYSA-M propylmercury(1+) hydroxide Chemical compound [OH-].C(CC)[Hg+] WGJDWRPHMYVQFO-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/10—Mercury compounds
- C07F3/12—Aromatic substances containing mercury
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung einer neuen Quecksilberverbindung. Gegenstand des vorliegenden Patentes ist ein Verfahren zur Herstellung einer netten Quecksilberverbindung, das dadurch gekenn zeichnet ist, dass man p-Propylmercuritliio- dimethylanilin mit Dimethylsulfat umsetzt.
Das so erhaltene p-Propylinercurithio- phenyl-trimethyl-ammonittin-methosulfat ist ein gelbliches, in Wasser lösliches Öl und soll als Desinfektionsmittel Verwendung finden. <I>Beispiel:</I> <B>3,8</B> Teile p-Propylmercurithio-dimet.hyl.- anilin (erhalten durch Umsetzung von Pro pylquecksilberhydroxyd mit einer alkoholi schen Lösung von p-Mercapto-dimethylanilin) werden in wenig Alkohol gelöst und mit 1 Vol.-Teil Diniethylsulfat versetzt und wäh rend einer Stunde am Rückfluss gekocht.
Nach dem Abkühlen, Versetzen mit. Äther und Aus frieren bei -100 erhält man das in Wasser lösliche p - Propylmereurithio - pheny 1- trime- tliyl-ammonium-methosulfat als gelbliches Öl.
Process for the preparation of a new mercury compound. The subject of the present patent is a process for the production of a nice mercury compound which is characterized in that p-propylmercuritliio dimethylaniline is reacted with dimethyl sulfate.
The p-propylinercurithiophenyl-trimethyl-ammonittine-methosulfate obtained in this way is a yellowish, water-soluble oil and is said to be used as a disinfectant. <I> Example: </I> <B> 3.8 </B> parts of p-propylmercurithio-dimet.hyl.- aniline (obtained by reacting propylmercury hydroxide with an alcoholic solution of p-mercapto-dimethylaniline) dissolved in a little alcohol and treated with 1 part by volume of diniethyl sulfate and refluxed for one hour.
After cooling, add. Ether and freeze out at -100, the water-soluble p-propylmereurithio-pheny-1-trimethylammonium methosulphate is obtained as a yellowish oil.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH257579T | 1944-08-04 | ||
CH265755T | 1944-08-04 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH265755A true CH265755A (en) | 1949-12-15 |
Family
ID=25730080
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH265755D CH265755A (en) | 1944-08-04 | 1944-08-04 | Process for the preparation of a new mercury compound. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH265755A (en) |
-
1944
- 1944-08-04 CH CH265755D patent/CH265755A/en unknown
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