CH211021A - Process for the production of a new azo dye. - Google Patents

Process for the production of a new azo dye.

Info

Publication number
CH211021A
CH211021A CH211021DA CH211021A CH 211021 A CH211021 A CH 211021A CH 211021D A CH211021D A CH 211021DA CH 211021 A CH211021 A CH 211021A
Authority
CH
Switzerland
Prior art keywords
azo dye
new azo
production
blue
new
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH211021A publication Critical patent/CH211021A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/10Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
    • C09B29/12Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group of the benzene series
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/10Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
    • C09B29/18Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides
    • C09B29/20Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides of the naphthalene series

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung eines neuen     Azofarbstoffes.       Es wurde gefunden, dass ein neuer     Azo-          farbstoff    hergestellt werden kann, wenn man       diazotiertes        4-(2'-Methyl)-phenoxyacetyl-          amino-2,5-diäthoxy-l-aminobenzol    mit     2,3-          Oxynaphtoesäure-3'-pyrenolid    vereinigt.  



  Der neue     Azofarbstoff    bildet ein blaues,  in Wasser unlösliches Pulver. Auf geeigne  ten Substraten, wie z. B. Baumwolle, her  gestellt, färbt er diese in sehr echten, insbe  sondere auch lichtechten blauen Tönen.         Beispiel     34,6 Teile     4-(2'-Methyl)-phenoxyacetyl-          a.mino-2,5-diäthoxy-l-aminobenzol        (:

  1/1o        Mol)     werden wie üblich     diazotiert    und in eine Lö  sung von 38,8 Teilen     2,3-Oxynaphtoesäure-3'-          pyrenolid        (1/,o        Mol),    100 Teilen     Natrium-          hydroxydlösung    von 36       Be,    15 Teilen Na-         triumacetat    und 2000 Teilen Wasser ein  getragen. Der gebildete Farbstoff fällt so  fort aus. Er wird     abfiltriert,    mit Wasser ge  waschen und getrocknet.



  Process for the production of a new azo dye. It has been found that a new azo dye can be prepared if diazotized 4- (2'-methyl) -phenoxyacetylamino-2,5-diethoxy-1-aminobenzene with 2,3-oxynaphthoic acid-3'-pyrenolide united.



  The new azo dye forms a blue, water-insoluble powder. On appro priate substrates such. B. cotton, made ago, he dyes them in very real, in particular special lightfast blue tones. Example 34.6 parts of 4- (2'-methyl) -phenoxyacetyl-a.mino-2,5-diethoxy-1-aminobenzene (:

  1/10 mol) are diazotized as usual and in a solution of 38.8 parts of 2,3-oxynaphthoic acid-3'-pyrenolide (1 /, o mol), 100 parts of sodium hydroxide solution of 36 Be, 15 parts of Na trium acetate and 2000 parts of water. The dye formed precipitates immediately. It is filtered off, washed ge with water and dried.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Azofarbstoffes, dadurch gekennzeichnet, dass man diazotiertes 4-(2'-Methyl)-phenoxy- acetylamino-2,5-diäthoxy-l-aminobenzol mit 2,3-Oxynaphthoesäure-3'-pyrenolid vereinigt. Der neue Azofarbstoff bildet ein blaues, in Wasser unlösliches Pulver. Auf geeigne ten Substraten, wie z. B. Baumwolle, her gestellt, färbt er diese in sehr echten, ins besondere auch lichtechten blauen Tönen. PATENT CLAIM: Process for the preparation of a new azo dye, characterized in that diazotized 4- (2'-methyl) -phenoxy-acetylamino-2,5-diethoxy-1-aminobenzene is combined with 2,3-oxynaphthoic acid-3'-pyrenolide. The new azo dye forms a blue, water-insoluble powder. On appro priate substrates such. B. cotton, made ago, he dyes them in very real, especially lightfast blue tones.
CH211021D 1937-06-02 1937-06-02 Process for the production of a new azo dye. CH211021A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH208951T 1937-06-02
CH211021T 1937-06-02

Publications (1)

Publication Number Publication Date
CH211021A true CH211021A (en) 1940-08-15

Family

ID=25724635

Family Applications (1)

Application Number Title Priority Date Filing Date
CH211021D CH211021A (en) 1937-06-02 1937-06-02 Process for the production of a new azo dye.

Country Status (1)

Country Link
CH (1) CH211021A (en)

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