CH209508A - Process for the preparation of an aminoarylsulfone. - Google Patents
Process for the preparation of an aminoarylsulfone.Info
- Publication number
- CH209508A CH209508A CH209508DA CH209508A CH 209508 A CH209508 A CH 209508A CH 209508D A CH209508D A CH 209508DA CH 209508 A CH209508 A CH 209508A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- aminoarylsulfone
- production
- sulfone
- methylamine
- Prior art date
Links
Description
Verfahren zur Herstellung eines Aminoarylsulfons. Vorliegendes Patent bezieht sich auf ein Verfahren zur Herstellung eines Aminaaryl- sulfons, dadurch gekennzeichnet, dass man 4-Chlorphenylmethylsulfon mit Methylamin kondensiert.
Das so erhaltene, bisher unbekannte 4 Methylaminophenylmethylsulfon kristallisiert aus Alkohol in farblosen Nädelchen vom Schmelzpunkt<B>128-1290</B> C und soll als Zwischenprodukt zur Herstellung von Farb stoffen und Heilmitteln Verwendung finden. Beispiel: 10 Teile 4-Chlorphenylmethylsulfon wer den mit 80 Teilen einer 25 o/oigen wässerigen Methylaminlösung in einem Druckgefäss etwa 20 Stunden auf 195-200o C erhitzt. Nach dem Erkalten filtriert man das gebildete Umsetzungsprodukt ab, wäscht es mit Wasser und trocknet es.
Process for the preparation of an aminoarylsulfone. The present patent relates to a process for the preparation of an amine aryl sulfone, characterized in that 4-chlorophenylmethyl sulfone is condensed with methylamine.
The previously unknown 4-methylaminophenylmethylsulfone obtained in this way crystallizes from alcohol in colorless needles with a melting point of <B> 128-1290 </B> C and is intended to be used as an intermediate for the production of dyes and medicinal products. Example: 10 parts of 4-chlorophenylmethylsulfone are heated with 80 parts of a 25% aqueous methylamine solution in a pressure vessel at 195-200 ° C. for about 20 hours. After cooling, the reaction product formed is filtered off, washed with water and dried.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE209508X | 1937-10-22 | ||
CH200367T | 1938-09-26 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH209508A true CH209508A (en) | 1940-04-15 |
Family
ID=25723461
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH209508D CH209508A (en) | 1937-10-22 | 1938-09-26 | Process for the preparation of an aminoarylsulfone. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH209508A (en) |
-
1938
- 1938-09-26 CH CH209508D patent/CH209508A/en unknown
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