CH193257A - Process for the production of an acidic wool dye. - Google Patents
Process for the production of an acidic wool dye.Info
- Publication number
- CH193257A CH193257A CH193257DA CH193257A CH 193257 A CH193257 A CH 193257A CH 193257D A CH193257D A CH 193257DA CH 193257 A CH193257 A CH 193257A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye
- production
- acidic
- wool dye
- acidic wool
- Prior art date
Links
- 210000002268 wool Anatomy 0.000 title claims description 7
- 230000002378 acidificating effect Effects 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 239000000975 dye Substances 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000003513 alkali Substances 0.000 description 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 1
- 238000006277 sulfonation reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B17/00—Azine dyes
- C09B17/04—Azine dyes of the naphthalene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. <B>189649.</B> Verfahren zur Herstellung eines sauren Wollfarbstoffes. Gegenstand vorliegenden Patentes ist ein Verfahren zur Herstellung eines sauren Wollfarbstoffes, das dadurch gekennzeichnet ist, dass man den Farbstoff der Formel:
EMI0001.0003
mit einem sulfonierenden Mittel behandelt.
Der neue Farbstoff, der zwei Sulfogrup- pen im Molekül enthält, färbt Wolle in sehr klaren, grünstichig blauen Tönen von guter Licht- und Alkaliechtheit. <I>Beispiel:</I> Der Farbstoff der Formel:
EMI0001.0009
wird zwecks Sulfonierung in die fünffache Menge 30%igen Oleums eingetragen und mehrere Stunden auf<B>80'</B> erhitzt, bis eine Probe in wässeriger Natriumacetatlösung klar löslie,11 ist.
Die Aufarbeitung erfolgt in üblicher Weise durch Ausgiessen auf Eis, Filtration und Überführung in das Natron- salz. Der erhaltene Farbstoff enthält zwei Suliogruppen im Molekül. Er färbt Wolle in sehr klaren, grünstichig blauen Tönen von guter Licht- und Alkaliechtheit,
Additional patent to main patent no. <B> 189649. </B> Process for the production of an acidic wool dye. The present patent relates to a process for the preparation of an acidic wool dye, which is characterized in that the dye of the formula:
EMI0001.0003
treated with a sulfonating agent.
The new dye, which contains two sulfo groups in the molecule, dyes wool in very clear, greenish blue tones with good light and alkali fastness. <I> Example: </I> The dye of the formula:
EMI0001.0009
For the purpose of sulfonation, five times the amount of 30% oleum is added and heated to <B> 80 '</B> for several hours until a sample is clearly soluble in aqueous sodium acetate solution 11.
Working up is carried out in the customary manner by pouring onto ice, filtration and conversion into the sodium salt. The dye obtained contains two sulio groups in the molecule. It dyes wool in very clear, greenish blue tones with good light and alkali fastness,
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH193257T | 1936-04-11 | ||
| CH189649T | 1936-04-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH193257A true CH193257A (en) | 1937-09-30 |
Family
ID=25721837
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH193257D CH193257A (en) | 1936-04-11 | 1936-04-11 | Process for the production of an acidic wool dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH193257A (en) |
-
1936
- 1936-04-11 CH CH193257D patent/CH193257A/en unknown
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