CH193252A - Process for the production of an acidic wool dye. - Google Patents
Process for the production of an acidic wool dye.Info
- Publication number
- CH193252A CH193252A CH193252DA CH193252A CH 193252 A CH193252 A CH 193252A CH 193252D A CH193252D A CH 193252DA CH 193252 A CH193252 A CH 193252A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye
- production
- acidic
- greenish blue
- wool
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B17/00—Azine dyes
- C09B17/04—Azine dyes of the naphthalene series
Description
<B>Zusatzpatent</B> zum Hauptpatent Nr. 189649. Verfahren zur Herstellung eines sauren Wollfarbstoffes. Gegenstand vorliegenden Patentes ist ein Verfahren zur Herstellung eines sauren Woll- farbstoffes, das dadurch gekennzeichnet ist, dass man den Farbstoff der Formel:
EMI0001.0004
mit einem sulfonierenden Mittel behandelt.
Der neue Farbstoff, der zwei Sulfo- gruppen im Molekül enthält, löst sich in kon zentrierter Schwefelsäure grün, in Wasser klar grünstichig blau und färbt Wolle in klaren grünstichig blauen Tönen von guter Licht- und Alkaliechtheit. Beispiel: Der nach bekannten Methoden hergestellte Farbstoff der Formel:
EMI0001.0011
wird zwecks Sulfonierung in die fünffache Menge 80 % igen Oleums eingetragen und mehrere Stunden auf<B>80"</B> erhitzt, bis eine Probe in wässeriger Natriumacetatlösung klar löslich ist..Die Aufarbeitung erfolgt in üblicher Weise durch Ausgiessen auf Eis, Filtration und Überführung in das Natron salz. Der erhaltene Farbstoff enthält zwei Sulfogruppen im Molekül.
Er färbt Wolle in klaren grünstichig blauen Tönen von guter Licht- und Alkaliechtheit. In konzentrierter Schwefelsäure löst er sich grün, in Wasser klar grünstichig blau.
<B> Additional patent </B> to main patent No. 189649. Process for the production of an acidic wool dye. The subject of the present patent is a process for the preparation of an acidic wool dye, which is characterized in that the dye of the formula:
EMI0001.0004
treated with a sulfonating agent.
The new dye, which contains two sulfo groups in the molecule, dissolves green in concentrated sulfuric acid, clear greenish blue in water and dyes wool in clear greenish blue shades of good lightfastness and alkali fastness. Example: The dye with the formula:
EMI0001.0011
For the purpose of sulfonation, five times the amount of 80% oleum is added and heated to <B> 80 "for several hours until a sample is clearly soluble in aqueous sodium acetate solution. Working up is carried out in the usual way by pouring onto ice, filtration and conversion into the sodium salt. The dye obtained contains two sulfo groups in the molecule.
It dyes wool in clear greenish blue tones with good lightfastness and alkali fastness. In concentrated sulfuric acid it dissolves green, in water it dissolves clear greenish blue.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH189649T | 1936-04-11 | ||
CH193252T | 1936-04-11 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH193252A true CH193252A (en) | 1937-09-30 |
Family
ID=25721832
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH193252D CH193252A (en) | 1936-04-11 | 1936-04-11 | Process for the production of an acidic wool dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH193252A (en) |
-
1936
- 1936-04-11 CH CH193252D patent/CH193252A/en unknown
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