CH191752A - Process for the preparation of an acidic chromating dye of the anthraquinone series. - Google Patents

Process for the preparation of an acidic chromating dye of the anthraquinone series.

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Publication number
CH191752A
CH191752A CH191752DA CH191752A CH 191752 A CH191752 A CH 191752A CH 191752D A CH191752D A CH 191752DA CH 191752 A CH191752 A CH 191752A
Authority
CH
Switzerland
Prior art keywords
dye
preparation
anthraquinone series
acidic
chromating
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH191752A publication Critical patent/CH191752A/en

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Description

  

  Verfahren zur Darstellung eines sauren     Chromierungsfarbstoffes    der     Anthrachinonreihe.       Gegenstand     ,dieses    Zusatzpatentes     ist    ein  Verfahren zur Darstellung eines sauren     Chro-          mierungsfarbs.toffes    der     Anthrachinonreihe,          welches        dadurch        gekennzeichnet    ist,     daZ    man  1-     amino-4-bromanthrachinon    -2     -sulfosaures     Natrium mit     3'-Amino-4'-methoxybenzyl-4-          oxy-3-m,

  ethyl-5-carboxyphenylsulfon    konden  siert.  



  <I>Beispiel:</I>  12     Gewichtsteile        1-a,mino-4-bromanthra-          chinon-2-sulfosaures    Natrium     werden    mit 15       Gewichtsteilen    3'-     Amina-4'-methoxybenzyl-          4-oxy-,3-methyl-5-carboxyphenylsulfon    der  folgenden Formel:

    
EMI0001.0023     
    7     Gewichtsteile        calc.Soda    und 1     Gewichts-          teil        Kupferchlorür    in 160     Gewichtsteilen          Wasser        ca.    5     Stunden    zum Sieden     erhitzt.     



  Der     entstandene    Farbstoff färbt nach  seiner Isolierung und     Reinigung        Wolle    in    blauen Tönen, welche sich durch     Nachchro-          mieren        unter    Übergang in eine     grünstickigere          Nuance    in     ihren        EChthelten    wesentlich     ver-          bessseren        lassen.  



  Process for the preparation of an acidic chromating dye of the anthraquinone series. The subject of this additional patent is a process for the preparation of an acidic chromating agent of the anthraquinone series, which is characterized in that 1-amino-4-bromoanthraquinone -2-sulfonic acid is sodium with 3'-amino-4'-methoxybenzyl-4 - oxy-3-m,

  ethyl-5-carboxyphenyl sulfone condenses.



  <I> Example: </I> 12 parts by weight of 1-a, mino-4-bromanthraquinone-2-sulfonic acid sodium are mixed with 15 parts by weight of 3'-amina-4'-methoxybenzyl-4-oxy-, 3-methyl- 5-carboxyphenyl sulfone of the following formula:

    
EMI0001.0023
    Heat 7 parts by weight of soda ash and 1 part by weight of copper chloride in 160 parts by weight of water to the boil for about 5 hours.



  After it has been isolated and cleaned, the resulting dye dyes wool in blue tones, which can be significantly improved by re-chroming with a transition to a greener shade.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Darstellung eines sauren Chromierungsfarbstoffes der Anthrachinon- reihe,dadurch gekennzeichnet, @dass, man 1- amino-4-bromanthrachinon-2,- sulfosaures Na trium mit 3'-Amino-4'-methoxybenzyl-4-oxy- 3-methyl-5-carboxyphenylsulfdn kondensiert. Der so erhaltene Farbstoff färbt Wolle in blauen Tönen, welche durch Na, PATENT CLAIM: Process for the preparation of an acidic chromating dye of the anthraquinone series, characterized in that, 1-amino-4-bromoanthraquinone-2, - sulfonic acid sodium with 3'-amino-4'-methoxybenzyl-4-oxy-3 -methyl-5-carboxyphenylsulfdn condensed. The dye obtained in this way dyes wool in blue tones, which by Na, chchroMie- ren in eine grünstickigere Nuance von guten Echth-eitscigenschaften übergehen. UNTERANSPRUCH: Verfahren nach Patentanspruch, dadurch gekennzeichnet, dass man die Kondensation .der Reaktionskomponenten durch Erhitzen in Wasser in Gegenwart von Natriumcarbonat und Kupferchlorür bewirkt. Chromium changes into a greener shade of good real-life properties. SUBCLAIM: Process according to claim, characterized in that the condensation of the reaction components is effected by heating in water in the presence of sodium carbonate and copper chloride.
CH191752D 1934-12-22 1935-12-19 Process for the preparation of an acidic chromating dye of the anthraquinone series. CH191752A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE191752X 1934-12-22
DE231035X 1935-10-23
CH188888T 1935-12-19

Publications (1)

Publication Number Publication Date
CH191752A true CH191752A (en) 1937-06-30

Family

ID=27177768

Family Applications (1)

Application Number Title Priority Date Filing Date
CH191752D CH191752A (en) 1934-12-22 1935-12-19 Process for the preparation of an acidic chromating dye of the anthraquinone series.

Country Status (1)

Country Link
CH (1) CH191752A (en)

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