CH183587A - Process for the preparation of an amine oxide. - Google Patents

Process for the preparation of an amine oxide.

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Publication number
CH183587A
CH183587A CH183587DA CH183587A CH 183587 A CH183587 A CH 183587A CH 183587D A CH183587D A CH 183587DA CH 183587 A CH183587 A CH 183587A
Authority
CH
Switzerland
Prior art keywords
ethyl
octa
decenyl
oxide
cyclohexylamine
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH183587A publication Critical patent/CH183587A/en

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Description

  

  Verfahren zur Herstellung eines     Aminozydes.       Es wurde gefunden, dass man ein neues       Aminoxyd    - das     0kta-8,9-decenyl-äthyl-          cyclohexyla.minoxyd    - erhält, wenn man das       Okta-8,9-decenyl-äthyl-cyclohexylamin    mit  solchen Oxydationsmitteln behandelt, die       superoxydisch    gebundenen Sauerstoff ent  halten.  



  Das     Okta-8,9-decenyl-äthyl-cyclohexyl-          aminoxyd    bildet ein     hellgefärbtes    Öl, das in  Wasser, fetten Ölen und Mineralölen löslich  ist. Die verdünnten wässerigen Lösungen des       01ta-8,9-decenyl-äthyl-cyclohexylaminoxydes     besitzen hervorragende     kapillaraktive    Eigen  schaften, so dass dieses     Produkt    ein wert  volles     Hilfsmittel    für die Textilindustrie dar  stellt.  



  <I>Beispiel:</I>  38 Teile     Okta-8-9-decenyl-äthyl-cyclo-          hexylamin    werden in 240     Volumteilen     Aceton gelöst, mit 19 Teilen einer Wasser  stoffsuperoxydlösung von 30     Volumprozent     versetzt, und während 40 bis 50 Stunden auf  60 bis 65   erhitzt. Nach dem     Abdestillieren     des     Acetons    und des Wassers im Vakuum  bei<B>60'</B> erhält man .das Oxyd des Okta-8,9-         decenyl-äthyl-cyclohexylamins    als hellge  färbtes dickflüssiges Öl. Es ist in Wasser,  fetten Ölen und Mineralölen klar löslich. Die  stark schäumenden wässerigen Lösungen be  sitzen hervorragende     kapillaraktive    Eigen  schaften.



  Process for the preparation of an amino acid. It has been found that a new amine oxide - the octa-8,9-decenyl-ethyl-cyclohexyla.minoxyd - is obtained if the octa-8,9-decenyl-ethyl-cyclohexylamine is treated with such oxidizing agents, the superoxide bound oxygen contain.



  The octa-8,9-decenyl-ethyl-cyclohexylamine oxide forms a light colored oil that is soluble in water, fatty oils and mineral oils. The dilute aqueous solutions of 01ta-8,9-decenyl-ethyl-cyclohexylamine oxide have excellent capillary-active properties, so that this product is a valuable aid for the textile industry.



  <I> Example: </I> 38 parts of octa-8-9-decenyl-ethyl-cyclohexylamine are dissolved in 240 parts by volume of acetone, 19 parts of a hydrogen peroxide solution of 30% by volume are added, and the mixture is increased to 60% over 40 to 50 hours heated to 65. After the acetone and the water have been distilled off in vacuo at <B> 60 '</B>, the oxide of octa-8,9-decenyl-ethyl-cyclohexylamine is obtained as a light-colored, viscous oil. It is clearly soluble in water, fatty oils and mineral oils. The highly foaming aqueous solutions have excellent capillary-active properties.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines Amin- oxydes - des Okta-8,9-decenyl-äthyl-cyclo- hexylaminoxydes -, dadurch gekennzeich net, dass man das Okta-8-9-.decenyl-äthyl- cyclohexylamin mit solchen Oxydationsmit teln behandelt, die superoxydisch gebundenen Sauerstoff enthalten. Das Okta-8,9-decenyl-.äthyl-cyclohexyl- aminoxyd bildet ein hellgefärbtes 01, das in Wasser, fetten Ölen und Mineralölen löslich ist. PATENT CLAIM: Process for the production of an amine oxide - the octa-8,9-decenyl-ethyl-cyclohexylamine oxide - characterized in that the octa-8-9-decenyl-ethyl-cyclohexylamine is treated with such oxidizing agents containing superoxide bound oxygen. The octa-8,9-decenyl-ethyl-cyclohexylamine oxide forms a light-colored oil that is soluble in water, fatty oils and mineral oils. Die verdünnten wässerigen Lösungen des Okta-8,9-.deoenyl-äthyl-cyelohexylaminoxydes besitzen hervorragende kapillaraktive Eigen schaften, so dass dieses Produkt ein wertvolles Hilfsmittel für die Textilindustrie .darstellt. The dilute aqueous solutions of octa-8,9-.deoenyl-ethyl-cyelohexylamine oxide have excellent capillary-active properties, making this product a valuable tool for the textile industry.
CH183587D 1935-07-04 1935-07-04 Process for the preparation of an amine oxide. CH183587A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH175351T 1935-07-04
CH183587T 1935-07-04

Publications (1)

Publication Number Publication Date
CH183587A true CH183587A (en) 1936-04-15

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ID=25719671

Family Applications (1)

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CH183587D CH183587A (en) 1935-07-04 1935-07-04 Process for the preparation of an amine oxide.

Country Status (1)

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CH (1) CH183587A (en)

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